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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

Phosphorothioic acid,O,O,O-triethyl ester

Cas:126-68-1

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

O,O,O-TRIETHYLPHOSPHOROTHIOATE CAS:126-68-1

Cas:126-68-1

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Phosphorothioic acid,O,O,O-triethyl ester

Cas:126-68-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

O,O,O-TRIETHYLPHOSPHOROTHIOATE

Cas:126-68-1

Min.Order:1 Kilogram

FOB Price: $60.0 / 80.0

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

O,O,O-TRIETHYLPHOSPHOROTHIOATE

Cas:126-68-1

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Product Name: O,O,O-TRIETHYLPHOSPHOROTHIOATE Synonyms: O,O,O-triethylthiophosphate;Phosphine sulfide, triethoxy-;Phosphorothioic acid, O,O,O-triethyl ester;phosphorothioicacid,o,o,o-triethylester;riethyl phosphorothioate;Thiophosphoric acid, tri-

126-68-1---O,O,O-TRIETHYLPHOSPHOROTHIOATE

Cas:126-68-1

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Xi`an Eastling Biotech Co., Ltd.

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou

O,O,O-TRIETHYLPHOSPHOROTHIOATE

Cas:126-68-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Antimex Chemical Limied

Phosphorothioic acid,O,O,O-triethyl esterAppearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:Used in Synthesis, Pharmaceuticals and other fields Transportation:Sea/air/courier

Phosphorothioic acid,O,O,O-triethyl ester

Cas:126-68-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Guangdong Juda Chemical Industrial Co.,Limited

Appearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China

O,O,O-TRIETHYLPHOSPHOROTHIOATE CAS No.126-68-1

Cas:126-68-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

Phosphorothioic acid,O,O,O-triethyl ester cas 126-68-1Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

Phosphorothioic acid,O,O,O-triethyl ester cas 126-68-1

Cas:126-68-1

Min.Order:0

Negotiable

Type:Other

inquiry

Shanghai Yuanye Bio-Technology Co., Ltd.

Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.Appearance:White powder Storage:keep sealed and keep from direct light Package:According client's requirements Application:pharmaceutica

O,O,O-TRIETHYLPHOSPHOROTHIOATE manufacturer

Cas:126-68-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

O,O,O-TRIETHYLPHOSPHOROTHIOATE

Cas:126-68-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Changzhou Extraordinary Pharmatech co.,LTD

Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa

O,O,O-Triethylphosphorothioate

Cas:126-68-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Jilin haofei import and export trade Co.,Ltd

Price, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right

Phosphorothioic acid,O,O,O-triethyl ester CAS NO.126-68-1

Cas:126-68-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai Run-Biotech Co., Ltd.

Shanghai, Run-Biotech Co., Ltd is a leading domestic pharmaceutical, biopharmaceutical, and health care products R & D outsourcing services company. As an innovation-driven and customer-focused company, Run Biotech provides a broad and integrated por

O,O,O-TRIETHYLPHOSPHOROTHIOATE

Cas:126-68-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Finetech Industry Limited

FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the O,O,O-TRIETHYLPHOSPHOROTHIOATE, CAS:126-68-1 with the most competitive price and the

O,O,O-TRIETHYLPHOSPHOROTHIOATE

Cas:126-68-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai PotentPharm Science and Technology Co.,Ltd

1 good quality, better price and bettter service;2 Timely delivery;3 100% refunded if parcel is t delivered or poor quality.We will try to satisfy you upon receipt of your reply. I hope that we can become a long-term cooperative partner. Application:

Phosphorothioic acid,O,O,O-triethyl ester

Cas:126-68-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Debye Scientific

Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen

O,O,O-Triethylphosphorthioate

Cas:126-68-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

yuyongmei

YUYONGMEI was established in Aug,1999, located in the industrial park of Nanjing University of Technology, It is a private enterprises in Jiangsu Province with 1200 square meters’ R&D center. Our R&D center has a well-equipped synthetic laboratory a

Phosphorothioic acid,O,O,O-triethyl ester

Cas:126-68-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

NEOCHEMA

O,O,O-Triethylphosphorothioate

Phosphorothioic acid,O,O,O-triethyl ester

Cas:126-68-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

triethyl phosphite
122-52-1

triethyl phosphite

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

Conditions
ConditionsYield
With N,N'-dimethylthioperoxydicarbamic acid In acetonitrile at 20℃;99%
With N-Bromosuccinimide; triphenylsilanethiol In benzene for 1h;93%
With propylene sulphide; [ReOCl3(OPPh3)(SMe2)] In dichloromethane for 0.333333h; Ambient temperature;85%
diphenyl-4,5 dithiole-1,3 thiones-2
17534-37-1

diphenyl-4,5 dithiole-1,3 thiones-2

A

tetraphenyl-[2,2']bi[1,3]dithiolylidene
23780-79-2

tetraphenyl-[2,2']bi[1,3]dithiolylidene

B

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

Conditions
ConditionsYield
With triethyl phosphite In acetonitrile for 16h; Irradiation;A 91%
B n/a
N-(chlorosulfanyl)morpholine
2958-89-6

N-(chlorosulfanyl)morpholine

triethyl phosphite
122-52-1

triethyl phosphite

A

Diethyl 4-morpholidophosphate
37097-43-1

Diethyl 4-morpholidophosphate

B

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

C

O,O-diethyl S-morpholino phosphorothioate
56341-75-4

O,O-diethyl S-morpholino phosphorothioate

Conditions
ConditionsYield
6-13 deg C then rt., 4 h;A 81%
B 4%
C 15%
6-13 deg C then rt., 4 h;A 23%
B 7%
C 70%
at 6 - 13℃;A 9%
B 7%
C 10.7 g
sodium ethanolate
141-52-6

sodium ethanolate

diethyl phosphorochloridothioate
2524-04-1

diethyl phosphorochloridothioate

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

Conditions
ConditionsYield
In ethanol at 20℃; for 14h;78.2%
diisopropoxyphosphinothionyl tert-butylamino trisulfide
76289-06-0

diisopropoxyphosphinothionyl tert-butylamino trisulfide

triethyl phosphite
122-52-1

triethyl phosphite

A

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

B

diisopropoxyphosphinothionyl tert-butylamino disulfide
76276-34-1

diisopropoxyphosphinothionyl tert-butylamino disulfide

Conditions
ConditionsYield
In diethyl ether at 0℃; for 0.25h;A 78%
B 63.5%
dicyclohexyl-carbodiimide
538-75-0

dicyclohexyl-carbodiimide

O,O'-diethyl thiophosphoric acid
2465-65-8

O,O'-diethyl thiophosphoric acid

A

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

B

O,O,S-triethyl phosphorothioate
1186-09-0

O,O,S-triethyl phosphorothioate

C

tetraethyl thiopyrophosphate
645-78-3

tetraethyl thiopyrophosphate

D

1,3-dicyclohexylthiourea
1212-29-9

1,3-dicyclohexylthiourea

Conditions
ConditionsYield
In diethyl ether for 240h; Mechanism; Product distribution; Ambient temperature; solvent: acetonitrile;A n/a
B n/a
C 45%
D 77%
O,O'-diethyl thiophosphoric acid
2465-65-8

O,O'-diethyl thiophosphoric acid

A

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

B

O,O,S-triethyl phosphorothioate
1186-09-0

O,O,S-triethyl phosphorothioate

C

tetraethyl thiopyrophosphate
645-78-3

tetraethyl thiopyrophosphate

D

1,3-dicyclohexylthiourea
1212-29-9

1,3-dicyclohexylthiourea

Conditions
ConditionsYield
With dicyclohexyl-carbodiimide In diethyl ether for 240h; Ambient temperature;A n/a
B n/a
C 45%
D 77%
ethanol
64-17-5

ethanol

O-phenyl> O,O-diethyl phosphorothioate
106259-91-0

O-phenyl> O,O-diethyl phosphorothioate

A

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

B

O-(o-aminophenyl) O,O-diethyl phosphorothioate
106259-89-6

O-(o-aminophenyl) O,O-diethyl phosphorothioate

Conditions
ConditionsYield
for 10h; Heating;A 69%
B 71%
3-phenylethanoic dithioperoxyanhydride
15088-78-5

3-phenylethanoic dithioperoxyanhydride

triethyl phosphite
122-52-1

triethyl phosphite

A

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

B

phenacetyl sulfide
97754-54-6

phenacetyl sulfide

Conditions
ConditionsYield
In 1,2-dichloro-ethane at 20℃; for 0.0833333h;A 70%
B n/a
triethyl phosphite
122-52-1

triethyl phosphite

A

diethyl sulfate
64-67-5

diethyl sulfate

B

triethyl phosphate
78-40-0

triethyl phosphate

C

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

D

ethylphosphonic acid diethyl ester
78-38-6

ethylphosphonic acid diethyl ester

Conditions
ConditionsYield
With sulfur trioxide In dichloromethane at -78℃;A 2%
B 70%
C 23%
D 5%
ethanol
64-17-5

ethanol

O,O'-diethyl thiophosphoric acid
2465-65-8

O,O'-diethyl thiophosphoric acid

A

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

B

O,O,S-triethyl phosphorothioate
1186-09-0

O,O,S-triethyl phosphorothioate

Conditions
ConditionsYield
With thiamine diphosphate; diethylazodicarboxylate In benzene at 35 - 40℃; for 6h; Yield given;A n/a
B 66%
With thiamine diphosphate; diethylazodicarboxylate In benzene at 35 - 40℃; for 6h; Yields of byproduct given;A n/a
B 66%
Lawessons reagent
19172-47-5

Lawessons reagent

triethyl phosphate
78-40-0

triethyl phosphate

A

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

B

2,4,6-tris(4-methoxyphenyl)-2,4,6-trisulfanylene-1,3,5,2,4,6-trioxatriphosphinane
137171-51-8, 67218-02-4

2,4,6-tris(4-methoxyphenyl)-2,4,6-trisulfanylene-1,3,5,2,4,6-trioxatriphosphinane

Conditions
ConditionsYield
In benzene for 12h; Heating;A 61%
B n/a
1,2-epithio-3-methoxypropane
19858-14-1

1,2-epithio-3-methoxypropane

triethyl phosphite
122-52-1

triethyl phosphite

A

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

B

methylallylether
627-40-7

methylallylether

cyclohexene sulfide
286-28-2

cyclohexene sulfide

diethyl ether
60-29-7

diethyl ether

triethyl phosphite
122-52-1

triethyl phosphite

A

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

B

cyclohexene
110-83-8

cyclohexene

carbon disulfide
75-15-0

carbon disulfide

methyl-imidophosphoric acid triethyl ester
71867-67-9

methyl-imidophosphoric acid triethyl ester

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

O-ethyl dichlorothiophosphate
1498-64-2

O-ethyl dichlorothiophosphate

sodium ethanolate
141-52-6

sodium ethanolate

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

ethanol
64-17-5

ethanol

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

Conditions
ConditionsYield
With sulfur; toluene; phosphorus trichloride
With trichlorophosphate
With phosphorus(V) oxybromide
sodium ethanolate
141-52-6

sodium ethanolate

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

Conditions
ConditionsYield
With trichlorophosphate
propylene sulphide
1072-43-1

propylene sulphide

triethyl phosphite
122-52-1

triethyl phosphite

A

propene
187737-37-7

propene

B

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

ethanol
64-17-5

ethanol

sodium acetate
127-09-3

sodium acetate

diethyl phosphorochloridothioate
2524-04-1

diethyl phosphorochloridothioate

A

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

B

O,O,S-triethyl phosphorothioate
1186-09-0

O,O,S-triethyl phosphorothioate

phenylmethanethiol
100-53-8

phenylmethanethiol

triethyl phosphite
122-52-1

triethyl phosphite

A

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

B

toluene
108-88-3

toluene

Conditions
ConditionsYield
Gluehlampenlicht.Irradiation;
Diethyl disulfide
110-81-6

Diethyl disulfide

triethyl phosphite
122-52-1

triethyl phosphite

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

Conditions
ConditionsYield
With di-tert-butyl peroxide at 140℃;
Diethyl disulfide
110-81-6

Diethyl disulfide

triethyl phosphite
122-52-1

triethyl phosphite

A

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

B

O,O,S-triethyl phosphorothioate
1186-09-0

O,O,S-triethyl phosphorothioate

Conditions
ConditionsYield
at 160℃;
dibenzyl disulphide
150-60-7

dibenzyl disulphide

triethyl phosphite
122-52-1

triethyl phosphite

A

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

B

dibenzyl sulfide
538-74-9

dibenzyl sulfide

C

1,1'-(1,2-ethanediyl)bisbenzene
103-29-7

1,1'-(1,2-ethanediyl)bisbenzene

D

toluene
108-88-3

toluene

Conditions
ConditionsYield
at 60℃; Irradiation;
diethyl sulphide
352-93-2

diethyl sulphide

di-tert-butyl peroxide
110-05-4

di-tert-butyl peroxide

triethyl phosphite
122-52-1

triethyl phosphite

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

Conditions
ConditionsYield
at 140℃;
Octanethiol
111-88-6

Octanethiol

triethyl phosphite
122-52-1

triethyl phosphite

A

octane
111-65-9

octane

B

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

Conditions
ConditionsYield
unter der Einwirkung von Licht;
dibutyl disulfide
629-45-8

dibutyl disulfide

di-tert-butyl peroxide
110-05-4

di-tert-butyl peroxide

triethyl phosphite
122-52-1

triethyl phosphite

A

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

B

Isobutane
75-28-5

Isobutane

C

Dibutyl sulfide
544-40-1

Dibutyl sulfide

D

n-butane
106-97-8

n-butane

Conditions
ConditionsYield
at 140℃;
thiocyanogen
505-14-6

thiocyanogen

triethyl phosphite
122-52-1

triethyl phosphite

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

diacetyl disulfide
592-22-3

diacetyl disulfide

triethyl phosphite
122-52-1

triethyl phosphite

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

ethanol
64-17-5

ethanol

diethyl thiophosphorocyanidate
87174-50-3

diethyl thiophosphorocyanidate

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

Conditions
ConditionsYield
With potassium hydroxide In water for 0.25h;
O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

triethyl phosphate
78-40-0

triethyl phosphate

Conditions
ConditionsYield
With pyridine; trifluoroacetic anhydride for 24h;100%
With 3-chloro-benzenecarboperoxoic acid In dichloromethane for 20h;100%
With ozone In dichloromethane at -75℃;95%
aluminum(III) perchlorate hydrate

aluminum(III) perchlorate hydrate

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

Al(3+)*3(OC2H5)2POS(1-)=Al((OC2H5)2POS)3

Al(3+)*3(OC2H5)2POS(1-)=Al((OC2H5)2POS)3

Conditions
ConditionsYield
In neat (no solvent) Al(ClO4)3 dissolved in a large excess of organic compound at ambient temp., temp. increased by 1-2°C per min, precipitated at 85-90.dergree.C, mixture allowed to cool; supernatant removed, washed with anhydrous diethyl ether, stored in vac. over anhydrous CaSO4; elem. anal.;95%
In ethanol byproducts: ethyl perchlorate; dissolving metal perchlorate in ethanol/triethyl orthoformate; stirringat 50°C for 2 h; cooling to room temp.; addn. of ligand; stirring at 80-90°C; pptn. after 20-40 mins; elem. anal.;35-50
O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

A

Diethyl phosphate
598-02-7

Diethyl phosphate

B

ethylphosphonic acid diethyl ester
78-38-6

ethylphosphonic acid diethyl ester

C

phosphonic acid diethyl ester
762-04-9

phosphonic acid diethyl ester

Conditions
ConditionsYield
With magnesium monoperoxyphthalate hexahydrate In water at 25℃; for 24h;A 10%
B 81%
C 9%
[Cp(CO)2Fe(THF)]PF6

[Cp(CO)2Fe(THF)]PF6

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

(η-cyclopentadienyl)dicarbonyl(triethylthiophosphato)iron hexafluorophosphate
115565-36-1

(η-cyclopentadienyl)dicarbonyl(triethylthiophosphato)iron hexafluorophosphate

Conditions
ConditionsYield
In dichloromethane stirring of a mixture of the THF-complex and the P-ligand in CH2Cl2 at room temp. for 36 h under N2; addn. of ether, filtn. of ppt., washing (ether), drying in vacuo, recrystn. (CH2Cl2/ether), elem. anal.;70%
O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

acetonitrile
75-05-8

acetonitrile

A

triethyl phosphate
78-40-0

triethyl phosphate

B

O,O,S-triethyl phosphorothioate
1186-09-0

O,O,S-triethyl phosphorothioate

C

bis(diethylphosphoryl)disulfide
4403-51-4

bis(diethylphosphoryl)disulfide

D

N-(ethyl)acetonitrilium tetrafluoroborate
462-35-1

N-(ethyl)acetonitrilium tetrafluoroborate

E

NO

NO

Conditions
ConditionsYield
With nitrosonium tetrafluoroborate In water 15-30 min; Further byproducts given. Yields of byproduct given;A n/a
B n/a
C 42%
D n/a
E n/a
O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

acetonitrile
75-05-8

acetonitrile

A

triethyl phosphate
78-40-0

triethyl phosphate

B

O,O,S-triethyl phosphorothioate
1186-09-0

O,O,S-triethyl phosphorothioate

C

ethanol
64-17-5

ethanol

D

bis(diethylphosphoryl)disulfide
4403-51-4

bis(diethylphosphoryl)disulfide

E

N-(ethyl)acetonitrilium tetrafluoroborate
462-35-1

N-(ethyl)acetonitrilium tetrafluoroborate

F

NO

NO

Conditions
ConditionsYield
With nitrosonium tetrafluoroborate for 0.5h;A n/a
B n/a
C n/a
D 42%
E 65 % Spectr.
F n/a
copper(II) perchlorate hydrate

copper(II) perchlorate hydrate

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

Cu(2+)*2(OC2H5)2POS(1-)=Cu((OC2H5)2POS)2

Cu(2+)*2(OC2H5)2POS(1-)=Cu((OC2H5)2POS)2

Conditions
ConditionsYield
In ethanol byproducts: ethyl perchlorate; dissolving metal perchlorate in ethanol/triethyl orthoformate; stirringat 50°C for 2 h; cooling to room temp.; addn. of ligand; stirring at 80-90°C for 2 h; elem. anal.;3%
ethyl bromide
74-96-4

ethyl bromide

O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

O,O,S-triethyl phosphorothioate
1186-09-0

O,O,S-triethyl phosphorothioate

Conditions
ConditionsYield
at 160℃;
O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

Isobutyl iodide
513-38-2

Isobutyl iodide

O,O-diethyl (S)-isobutylphosphorothioate
26629-01-6

O,O-diethyl (S)-isobutylphosphorothioate

Conditions
ConditionsYield
at 120℃; im Rohr;
O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

sodium isobutoxide
13259-29-5

sodium isobutoxide

thiophosphoric acid O-ethyl ester-O-isobutyl ester; silver salt

thiophosphoric acid O-ethyl ester-O-isobutyl ester; silver salt

Conditions
ConditionsYield
With 2-methyl-propan-1-ol bei nachfolgender Einw. von Silbernitrat;
O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

Diethyl phosphoramidate
1068-21-9

Diethyl phosphoramidate

Conditions
ConditionsYield
With diethyl ether; ammonia at 150℃;
With ethanol; ammonia at 120℃;
O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

O,O,S-triethyl phosphorothioate
1186-09-0

O,O,S-triethyl phosphorothioate

Conditions
ConditionsYield
at 200℃;
at 180℃;
With silver nitrate man setzt das erhaltene S-Silbersalz des Thiophosphorsaeure-O.O-diaethylesters mit Aethyljodid in Alkohol;
O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

sulfotep
3689-24-5

sulfotep

Conditions
ConditionsYield
With sulfuric acid
O,O,O-triethyl phosphorothioate
126-68-1

O,O,O-triethyl phosphorothioate

diethoxyoxophosphoranesulfenyl chloride
1186-08-9

diethoxyoxophosphoranesulfenyl chloride

Conditions
ConditionsYield
With tetrachloromethane; chlorine at -5℃;
With sulfuryl dichloride
With sulfuryl dichloride In benzene

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