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inquirytris(4-trifluoromethylphenyl)phosphine oxide
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
With diisobutylaluminium hydride In cyclohexane at 72℃; for 14h; | 93% |
Stage #1: tris(4-trifluoromethylphenyl)phosphine oxide With trityl tetrakis(pentafluorophenyl)borate In (2)H8-toluene at 20℃; Glovebox; Inert atmosphere; Stage #2: With phenylsilane In (2)H8-toluene at 80℃; for 6h; Glovebox; Inert atmosphere; Sealed tube; | 92% |
With [AlH3(triethylamine)] In hexane at 20℃; for 0.166667h; Inert atmosphere; Schlenk technique; | 88 %Chromat. |
With hexylsilane; trifluorormethanesulfonic acid In toluene at 70℃; for 24h; Inert atmosphere; Sealed tube; chemoselective reaction; | >= 99 %Spectr. |
With 2,6-dimethylpyridine; oxalyl dichloride; hydrogen; tris(2,6-difluorophenyl)borane triethylphosphine oxide In (2)H8-toluene at 130℃; under 3000.3 Torr; for 48h; Reagent/catalyst; | 57 %Spectr. |
p-trifluoromethylphenyl bromide
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
Stage #1: p-trifluoromethylphenyl bromide With magnesium dihydride In diethyl ether at 20℃; for 1h; Stage #2: With phosphorus trichloride In diethyl ether at 20℃; for 1h; | 72% |
Stage #1: p-trifluoromethylphenyl bromide With magnesium In diethyl ether for 2h; Reflux; Schlenk technique; Inert atmosphere; Stage #2: With phosphorus trichloride In diethyl ether at 0℃; for 1h; Reflux; Schlenk technique; Inert atmosphere; | 63% |
With phosphorus trichloride 2) Et2O, reflux, 1h; Yield given. Multistep reaction; |
(4-(trifluoromethyl)phenyl)zinc(II) bromide
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
With phosphorus trichloride In acetonitrile at 20℃; for 2h; | 53% |
p-trifluoromethylphenyl bromide
phosphorus trichloride
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
With hydrogenchloride; n-butyllithium In diethyl ether; hexane; water | 35% |
4-(trifluoromethyl)phenylmagnesium bromide
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
With phosphorus trichloride |
tris(para-trifluoromethyl)phenyl phosphine
tris(4-trifluoromethylphenyl)phosphine oxide
Conditions | Yield |
---|---|
With dihydrogen peroxide In dichloromethane; water at 20℃; for 3h; Glovebox; Inert atmosphere; | 100% |
With gold(III) complex supported on cellulose extracted from Carthamus tinctorius immobilized on nanofibrous phosphosilicate; air at 20℃; for 1h; Irradiation; | 99% |
With dihydrogen peroxide In dichloromethane; water for 0.75h; cooling; | 97% |
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In benzene at 100℃; for 6h; Inert atmosphere; Sealed tube; | 100% |
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 100% |
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
In dichloromethane under inert atm. soln. TpOs(N)Cl2 andphosphine ligand in CH2Cl2 was stirred for 1 h; soln. was concd., hexane was added, ppt. was washed with Et2O and recrystd. from CH2Cl2 and heptane; elem. anal.; | 97% |
Conditions | Yield |
---|---|
In acetone all manipulations under dry N2 atm.; 2 equiv. of P compd. added to soln.of Rh compd., stirred at room temp. (checked for completion by TLC); solvent removed in vac., isolated as crystalline solid; elem. anal.; | 97% |
copper(l) iodide
2-(diphenylphosphaneyl)-4-methylpyridine
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 12h; Inert atmosphere; Schlenk technique; Darkness; | 97% |
2-(diphenylphosphino)pyridine
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 12h; Inert atmosphere; Schlenk technique; Darkness; | 96% |
carbon dioxide
2-(trimethylsilyl)phenyl trifluoromethanesulfonate
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
With potassium fluoride; 18-crown-6 ether In tetrahydrofuran at 0 - 50℃; under 760.051 Torr; for 36h; Schlenk technique; Sealed tube; | 96% |
[RhCl(cis-cyclooctene)2]2
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
In toluene at 20℃; Inert atmosphere; | 95.1% |
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
In dichloromethane stirring ReOCl3(As(C6H5)3)2 (0.33 mmol) and P(C6H4CF3)2 (0.66 mmol) in CH2Cl2 at room temp. for 27 h; concg. in vac.; addn. of heptane;; pptn.; filtering off, washing with heptane and drying in vac.; elem. anal.;; | 95% |
tetrafluoroboric acid diethyl ether
N-(1-methoxyethyl)phthalimide
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
Stage #1: tetrafluoroboric acid diethyl ether; tris(para-trifluoromethyl)phenyl phosphine In dichloromethane at 0 - 20℃; for 2h; Stage #2: N-(1-methoxyethyl)phthalimide With sodium bromide at 95℃; for 7h; | 95% |
tris(para-trifluoromethyl)phenyl phosphine
(p-cymene)OsCl2(P(p-CF3C6H4)3)
Conditions | Yield |
---|---|
In dichloromethane inert atmosphere; stirring soln. of Os-complex with 2 equivs. of phosphine for 60 min at room temp.; evapn., washing (hexane), collection (filtration), drying (vac.); elem. anal.; | 92% |
Conditions | Yield |
---|---|
Inert atmosphere; Schlenk technique; | 92% |
potassium tetrachloroplatinate(II)
tris(para-trifluoromethyl)phenyl phosphine
cis-dichlorobis{tris(4-(trifluoromethyl)phenyl)phosphane}platinum(II)
Conditions | Yield |
---|---|
In ethanol; water addn. of aq. soln. of K2(PtCl4) to hot ethanolic soln. of phosphane; stirring at room temp. for 25 h; filtering, washing with water, ethanol and ether, drying in vac. at room temp.; | 91% |
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
With phosphorus tribromide; iron (III) bromide In tetrachloromethane at 0 - 80℃; for 10h; | 91% |
chloro(1,5-cyclooctadiene)(pentamethylcyclopentadiene)ruthenium(II)
tris(para-trifluoromethyl)phenyl phosphine
(η(5)-C5Me5)RuCl(P(p-CF3C6H4)3)2
Conditions | Yield |
---|---|
In tetrahydrofuran Ar or N2-atmosphere; 2 equivs. of phosphine, stirring overnight; evapn., addn. of hexane, stirring for 20 min, collection (filtration), washing (hexanes), drying (vac.); elem. anal.; | 90% |
In tetrahydrofuran Ar or N2-atmosphere; 30°C; not sepd., enthalpy of reaction determined; |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1.5h; | 90% |
Conditions | Yield |
---|---|
With trimethylamine-N-oxide In dichloromethane; acetonitrile at 20℃; for 1h; | 90% |
iodobenzene
[RhCl(cis-cyclooctene)2]2
tris(para-trifluoromethyl)phenyl phosphine
[(p-CF3-C6H4)3P]2 bis(pivalate) rhodium(I)Ph
Conditions | Yield |
---|---|
In 1,4-dioxane in dioxane at 120°C; | 89% |
1,1'-bis-(diphenylphosphino)ferrocene
tetrakis(acetonitrile)palladium(II) tetrafluoroborate
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
In acetone; benzene for 0.166667h; Inert atmosphere; Glovebox; | 88% |
(tetrahydrothiophene)gold(I) chloride
tris(para-trifluoromethyl)phenyl phosphine
[tris(para(trifluoromethyl)phenyl)phosphine]gold(I) chloride
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1h; | 87% |
In dichloromethane |
Conditions | Yield |
---|---|
In dichloromethane for 12h; Schlenk technique; | 87% |
tris(para-trifluoromethyl)phenyl phosphine
(η(5)-C5H5)RuCl(P(p-CF3C6H4)3)2
Conditions | Yield |
---|---|
In tetrahydrofuran Ar or N2-atmosphere; 2 equivs. of phosphine, stirring overnight; evapn., addn. of hexane, stirring for 20 min, collection (filtration), washing (hexanes), drying (vac.); elem. anal.; | 86% |
In tetrahydrofuran Ar or N2-atmosphere; 30°C; not sepd., enthalpy of reaction determined; |
[(η(5)-C5H5)Re(NO)(CO)(MeCN)]BF4
tris(para-trifluoromethyl)phenyl phosphine
[(μ5-C5H5)Re(NO)(CO)(P(4-C6H4CF3)3)]BF4
Conditions | Yield |
---|---|
In butanone all manipulations under dry N2 atm.; EtCOMe added to Re complex and the phosphane, refluxed for 46 h; allowed to cool, hexane added, filtered, washed with pentane, dried in vac., elem. anal.; | 85% |
tris(para-trifluoromethyl)phenyl phosphine
Rh(CO)((CH3CO)2CH)(P(C6H4CF3)3)
Conditions | Yield |
---|---|
In dichloromethane byproducts: CO; Ar or N2-atmosphere, 30°C; elem. anal.; | 85% |
tris(para-trifluoromethyl)phenyl phosphine
[tris(para(trifluoromethyl)phenyl)phosphine]gold(I) chloride
Conditions | Yield |
---|---|
With β-thiodiglucol In methanol; dichloromethane; water under N2 or Ar using Schlenk techniques; in the dark; soln. of HAuCl4*4H2O dissolved in H2O/MeOH; cooled; soln. of β-thiodiglucol in MeOH added with stirring; soln. of org. ligand in MeOH/CH2Cl2 added; mixt. stirred overnight; MeOH added; solvent removed (vac.); recrystd. (CH2Cl2/hexane); dried (vac.); | 85% |
tris(para-trifluoromethyl)phenyl phosphine
cis-[Me2Pt(P(p-CF3C6H4)3)2]
Conditions | Yield |
---|---|
In not given byproducts: cyclooctadiene; 2 equiv. of phosphine; elem. anal.; | 84% |
1-Iodo-perfluorodecane
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
In chloroform-d1 at 20℃; for 30h; Irradiation; Sealed tube; Inert atmosphere; | 84% |
at 15 - 25℃; for 30h; Irradiation; Sealed tube; Inert atmosphere; | 61 %Spectr. |
tris(para-trifluoromethyl)phenyl phosphine
Conditions | Yield |
---|---|
With trimethylamine-N-oxide In dichloromethane; acetonitrile at 20℃; for 1h; | 84% |
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