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Cas:137-03-1
Min.Order:1 Kilogram
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Min.Order:1 Gram
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Min.Order:1 Gram
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Min.Order:1 Kilogram
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2-Heptylcyclopentanone cas 137-03-1Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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Conditions | Yield |
---|---|
With tert.-butylhydroperoxide at 150 - 160℃; under 12000.9 - 13501.1 Torr; | 75% |
With (t-BuO)2 at 140 - 150℃; | 70% |
With di-tert-butyl peroxide | |
With di-tert-butyl peroxide at 140 - 160℃; Autoclave; |
2-heptyl-adipic acid
2-heptylcyclopentanone
Conditions | Yield |
---|---|
With acetic anhydride |
2-heptylidenecyclopentan-1-one
2-heptylcyclopentanone
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal | |
Ir(CO)(PPh3)2Cl at 240℃; |
1-heptyl-2-oxo-cyclopentanecarboxylic acid ethyl ester
2-heptylcyclopentanone
Conditions | Yield |
---|---|
With sulfuric acid | |
Multi-step reaction with 2 steps 1: ethanolic KOH-solution 2: acetic acid anhydride View Scheme |
2-heptylcyclopentanone
Conditions | Yield |
---|---|
In tetrahydrofuran; hydrogenchloride; hexane Yield given; |
2-heptylcyclopentanone
Conditions | Yield |
---|---|
Hydrogenation; |
2-cyclopentylidene-1,1-dimethylhydrazine
2-heptylcyclopentanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) n-BuLi / 1.) THF, hexane, -5 deg C, 1 h, 2.) THF, hexane, rt, 20 h 2: aq. HCl; tetrahydrofuran; hexane View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 91 percent / trifluoroacetic acid; benzene / 5 h / Heating 2: 1.) n-BuLi / 1.) THF, hexane, -5 deg C, 1 h, 2.) THF, hexane, rt, 20 h 3: aq. HCl; tetrahydrofuran; hexane View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium ethylate 2: ethanolic KOH-solution 3: acetic acid anhydride View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (i) aq. KOH, (ii) oxalic acid 2: H2 / Pd-C View Scheme | |
Multi-step reaction with 2 steps 1: (i) benzene, (ii) aq. HCl 2: Ir(CO)(PPh3)2Cl / 240 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: K2CO3 / acetone / Heating 2: aq. H2SO4 View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: K2CO3 / acetone / Heating 2: aq. H2SO4 View Scheme |
Conditions | Yield |
---|---|
With hydrogen at 140℃; under 26252.6 Torr; for 6.66667h; Autoclave; | 71 %Chromat. |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; magnesium monoperoxyphthalate hexahydrate In methanol; water for 24h; Ambient temperature; | 98% |
With dihydrogen peroxide; tungsten(VI) oxide In acetonitrile at 40℃; for 12h; Time; Reagent/catalyst; | 92% |
With dihydrogen peroxide; lithium acetate In water; Ethyl propionate at 110℃; for 6h; Baeyer-Villiger Oxidation; Heating / reflux; | 91% |
Conditions | Yield |
---|---|
With (S)-3,3'-bis(9-anthracenyl)-1,1′-binaphthyl-2,2′-diyl hydrogenphosphate In acetonitrile at 20℃; for 48h; enantioselective reaction; | 88% |
2-heptylcyclopentanone
A
5-dodecanolide
B
5-oxododecanoic acid
C
5-hydroxydodecanoic acid
Conditions | Yield |
---|---|
With water; dihydrogen peroxide at 40℃; for 12h; Reagent/catalyst; Baeyer-Villiger Ketone Oxidation; | A 81% B n/a C n/a |
propylene glycol
2-heptylcyclopentanone
2-methyl-6-heptyl-1,4-dioxaspiro[4.4]nonane
Conditions | Yield |
---|---|
With P0.17Mo2.4CoBr0.27O6.8 In 5,5-dimethyl-1,3-cyclohexadiene at 130℃; for 6h; | 80% |
With GdPO4*(MoO2)0.5PMo12O40 In toluene Reflux; Dean-Stark; | 80% |
Conditions | Yield |
---|---|
In benzene Heating; | 78% |
2-heptylcyclopentanone
δ-dodecalactone
Conditions | Yield |
---|---|
With dihydrogen peroxide; molybdenum(VI) oxide In water at 40℃; for 12h; Reagent/catalyst; Baeyer-Villiger Ketone Oxidation; | 78% |
Conditions | Yield |
---|---|
With Calcium tetrakis(pentafluorophenyl)borate; dihydrogen peroxide; oxalic acid In water; 1,2-dichloro-ethane at 50℃; for 10h; Reagent/catalyst; | A 65% B 23% |
2-heptylcyclopentanone
ethylene glycol
6-heptyl-1,4-dioxaspiro[4.4]nonane
Conditions | Yield |
---|---|
With chlorinated KU-23 In 5,5-dimethyl-1,3-cyclohexadiene at 130℃; for 6h; | 64% |
With GdPO4*(MoO2)0.5PMo12O40 In toluene Reflux; Dean-Stark; | 54.7% |
Conditions | Yield |
---|---|
With 2,2,6,6-tetramethyl-piperidine; trifluorormethanesulfonic acid; oxygen In m-xylene at 130℃; under 760.051 Torr; for 6h; Sealed tube; | 61% |
1.3-butanediol
2-heptylcyclopentanone
1-heptyl-7-methyl-6,10-dioxaspiro[4.5]decane
Conditions | Yield |
---|---|
With P0.17Mo2.4CoBr0.27O6.8 In 5,5-dimethyl-1,3-cyclohexadiene at 130℃; for 6h; | 59% |
Conditions | Yield |
---|---|
With sulfuric acid; aurin; oxygen In toluene at 20℃; for 24h; Schlenk technique; Irradiation; | 47% |
Conditions | Yield |
---|---|
With ammonium acetate; acetic acid In toluene for 90h; Knoevenagel Condensation; Reflux; Dean-Stark; | 37% |
1,2-diphenyl-2-methylthio-1-ethanone
2-heptylcyclopentanone
A
2-heptyl-2-(methylthio)cyclopentanone
Conditions | Yield |
---|---|
With hydridotetakis(triphenylphosphine)rhodium(I); Dimethyldisulphide; 1,2-bis-(diphenylphosphino)ethane In tetrahydrofuran at 90℃; for 3h; Inert atmosphere; regioselective reaction; | A 30% B 5% C 13% |
2-heptylcyclopentanone
A
2-heptyl-2-cyclopenten-1-one
B
(E)-2-n-heptylidenecyclopentanone
Conditions | Yield |
---|---|
With iron(III) chloride In ethanol; water for 2.5h; Heating; | A 25% B n/a |
2-heptylcyclopentanone
2-methoxymethylpyrrolidine
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 120h; Reflux; Dean-Stark; | 11% |
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