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inquiry4-Chloro-6-ethyl-5-fluoropyrimidine CAS No.:137234-74-3 Name: 4-Chloro-6-ethyl-5-fluoropyrimidine Molecular Structure Molecular Formula: C6H6ClFN2
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inquiryGood quality Good price Promptly delivery Appearance:white powder Storage:dry dondition Package:According to the demand of customer Application:intermediate Transportation:According to the demand of customer Port:shanghai
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi
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inquiryColorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1982.html Product Name 4-Chloro-6-ethyl-5-fluoropyrimidine CAS No.
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inquiryOur company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryCAS 137234-74-3 Details Chemical Name:4-Chloro-6-ethyl-5-fluoropyrimidine CAS No.: 137234-74-3 Molecular Formula: C6H6ClFN2 Molecular Weight: 160.58 Appearance: Colorless to light yellow liquid Appearance:Colorless to light yellow liquid Storage
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inquiryWe have two GMP facilities in Hubei Province and cooperative factories in Zhejiang Province We are concentrating on the R&D and technical service of APIs and pharmaceutical intermediates FDA Approved Appearance:white Storage:Inert atmosp
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:137234-74-3
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inquiryBeluga chemical professional supply 4-Chloro-6-ethyl-5-fluoropyrimidine 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. Made in China and exp
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryProduct Name: 4-Chloro-6-ethyl-5-fluoropyrimidine Synonyms: 4-Chloro-5-fluoro-6-ethylpyriMidine;PyriMidine, 4-chloro-6-ethyl-5-fluoro-;4-chloro-6-ethyl-5-fluoropyiMidine;4-CHLORO-6-ETHYL-5-FLUOROPYRIMIDINE;6-CHLORO-4-ETHYL-5-FLUORO-1,6-DIHYDROPY
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiryAppearance:white powder Storage:Store in a cool,dry place and keep away from direct strong light Package:packaged in foil bags or tins Application:Use only for laboratory research Transportation:Sea,Air,DHL/TNT/FEdex/UPS/EMS Por
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryNewCan Biotech Limited was established in 2021 and is primarily engaged in the research, development, production, and sales of sugars, nucleosides, nucleotides, phosphorylated monomers, as well as next-generation antiviral and antitumor drug intermed
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inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
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inquiry6-ethyl-5-fluoropyrimidin-4(1H)-one
4-chloro-5-fluoro-6-ethylpyrimidine
Conditions | Yield |
---|---|
With triethylamine; trichlorophosphate In dichloromethane at 48℃; for 6h; Product distribution / selectivity; Industry scale; Heating / reflux; | 99% |
With triethylamine; trichlorophosphate In dichloromethane for 5h; Product distribution / selectivity; Heating / reflux; | 90% |
With triethylamine; trichlorophosphate In dichloromethane at 40℃; for 5.16667h; Reflux; |
6-ethyl-5-fluoro-4-hydroxypyrimidine
4-chloro-5-fluoro-6-ethylpyrimidine
Conditions | Yield |
---|---|
Stage #1: 6-ethyl-5-fluoro-4-hydroxypyrimidine With triethylamine; trichlorophosphate In dichloromethane for 5.5h; Heating / reflux; Stage #2: With hydrogenchloride; water In dichloromethane at 20℃; | 95% |
With triethylamine; trichlorophosphate In dichloromethane at 40℃; for 8h; Reflux; | 90% |
With trichlorophosphate In N,N-dimethyl-formamide at 90℃; for 5h; | 90.2% |
3-(6-chloro-5-fluoropyrimidin-4-yl)-2-(2,4-difluorophenyl)-1-(1H-1,2,4-triazol-1-yl)-2-butanol
A
1-(2,4-difluorophenyl)-2-(1H-1,2,4-triazolyl)ethanone
B
4-chloro-5-fluoro-6-ethylpyrimidine
Conditions | Yield |
---|---|
With hydrogenchloride In water at 60 - 70℃; Temperature; Reagent/catalyst; Solvent; | A 88.4% B n/a |
6-Ethyl-5-fluoropyrimidin-4(3H)-one
4-chloro-5-fluoro-6-ethylpyrimidine
Conditions | Yield |
---|---|
With trichlorophosphate Heating; |
2-fluoro-3-oxopentanoic acid ethyl ester
4-chloro-5-fluoro-6-ethylpyrimidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1) MeONa, MeOH 2: POCl3 / Heating View Scheme | |
Multi-step reaction with 2 steps 1: sodium methylate / methanol / 20 h / 15 °C 2: trichlorophosphate / 3 h / 60 °C View Scheme |
4-chloro-5-fluoro-6-ethylpyrimidine
1-(4-chloro-5-fluoropyrimidin-6-yl)bromoethane
Conditions | Yield |
---|---|
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In dichloromethane at 55℃; for 16h; Temperature; | 98% |
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In dichloromethane for 12h; Reflux; | 95.1% |
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In dichloromethane for 12h; Reflux; | 95.1% |
p-Chlorothiophenol
4-chloro-5-fluoro-6-ethylpyrimidine
4-(4-chloro-phenylsulfanyl)-6-ethyl-5-fluoropyrimidine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 10 - 20℃; for 2h; | 96% |
4-chloro-5-fluoro-6-ethylpyrimidine
Methyl thiosalicylate
methyl 2-(6-ethyl-5-fluoropyrimidin-4-yl-sulfanyl)benzoate
Conditions | Yield |
---|---|
Stage #1: Methyl thiosalicylate With sodium hydride In tetrahydrofuran at 5℃; for 0.666667h; Stage #2: 4-chloro-6-ethyl-5-fluoropyrimidine In tetrahydrofuran at 20 - 25℃; | 96% |
thiophenol
4-chloro-5-fluoro-6-ethylpyrimidine
4-(phenylsulfanyl)-6-ethyl-5-fluoropyrimidine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 10℃; for 2h; | 95% |
4-chloro-5-fluoro-6-ethylpyrimidine
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 120℃; for 17.3h; Sealed tube; | 81% |
4-chloro-5-fluoro-6-ethylpyrimidine
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 120℃; for 18h; Sealed tube; | 74% |
4-chloro-5-fluoro-6-ethylpyrimidine
6-ethyl-5-fluoropyrimidine-4-thiol
Conditions | Yield |
---|---|
With sodium hydrogensulfide In acetonitrile at 48 - 52℃; for 8.75h; Product distribution / selectivity; Industry scale; | 73% |
With sodium hydrogensulfide In methanol at 50℃; for 4.25h; Product distribution / selectivity; |
1-methyl-5-mercaptotetrazole
4-chloro-5-fluoro-6-ethylpyrimidine
Conditions | Yield |
---|---|
Stage #1: 1-methyl-5-mercaptotetrazole With sodium hydride In tetrahydrofuran at 5 - 25℃; Stage #2: 4-chloro-6-ethyl-5-fluoropyrimidine In tetrahydrofuran at 5 - 25℃; | 63.4% |
4-chloro-5-fluoro-6-ethylpyrimidine
dl-α-methyl-4-pentafluorophenoxybenzylamine
Conditions | Yield |
---|---|
With triethylamine; dmap In N,N-dimethyl-formamide for 8h; Substitution; Heating; |
4-chloro-5-fluoro-6-ethylpyrimidine
dl-α-methyl-4-difluoromethoxybenzylamine
Conditions | Yield |
---|---|
With triethylamine at 20℃; Substitution; |
4-chloro-5-fluoro-6-ethylpyrimidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: LDA / tetrahydrofuran 2: H2, AcONa / Pd/C / ethanol / 20 °C View Scheme |
4-chloro-5-fluoro-6-ethylpyrimidine
voriconazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: LDA / tetrahydrofuran 2: H2, AcONa / Pd/C / ethanol / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: diisopropylamine; n-butyllithium / n-heptane; hexane; tetrahydrofuran / 0.25 h / -80 - -70 °C / Inert atmosphere 1.2: 2 h / -80 - -55 °C 1.3: -70 - -10 °C 2.1: sodium acetate / ethyl acetate; water / 0.5 h / 25 - 30 °C 2.2: 25 - 30 °C / 3677.86 Torr 2.3: 0.5 h / 20 - 25 °C 3.1: acetone; methanol / 15 h / -20 - 25 °C 4.1: sodium hydroxide / dichloromethane; water / 0.25 h / pH 11 - 14 View Scheme | |
Multi-step reaction with 5 steps 1.1: diisopropylamine; n-butyllithium / n-heptane; hexane; tetrahydrofuran / 0.25 h / -80 - -70 °C / Inert atmosphere 1.2: 2 h / -80 - -55 °C 1.3: -70 - -10 °C 2.1: hydrogen; sodium acetate / palladium 10% on activated carbon / ethyl acetate; water / 25 - 30 °C / 3677.86 Torr 2.2: 0.5 h / 20 - 25 °C 2.3: 12.5 h / 25 - 30 °C 3.1: sodium hydroxide / dichloromethane; water / 0.5 h / pH 9 - 12 4.1: acetone; methanol / 15 h / -20 - 25 °C 5.1: sodium hydroxide / dichloromethane; water / 0.25 h / pH 11 - 14 View Scheme |
4-chloro-5-fluoro-6-ethylpyrimidine
3-(6-chloro-5-fluoropyrimidin-4-yl)-2-(2,4-difluorophenyl)-1-(1H-1,2,4-triazol-1-yl)-2-butanol
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran; n-heptane at -70 - -65℃; for 3 - 4h; pH=5 - 8; |
1-[2-(trifluoromethyl)-1H-pyrrolo[2,3-b]pyridine-5-yl]methanamine
4-chloro-5-fluoro-6-ethylpyrimidine
Conditions | Yield |
---|---|
Stage #1: 1-[2-(trifluoromethyl)-1H-pyrrolo[2,3-b]pyridine-5-yl]methanamine; 4-chloro-6-ethyl-5-fluoropyrimidine With N-ethyl-N,N-diisopropylamine In 1-methyl-pyrrolidin-2-one at 0℃; Stage #2: With hydrogenchloride In 1,4-dioxane; methanol |
4-chloro-5-fluoro-6-ethylpyrimidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: diisopropylamine; n-butyllithium / n-heptane; hexane; tetrahydrofuran / 0.25 h / -80 - -70 °C / Inert atmosphere 1.2: 2 h / -80 - -55 °C 1.3: -70 - -10 °C 2.1: sodium acetate / ethyl acetate; water / 0.5 h / 25 - 30 °C 2.2: 25 - 30 °C / 3677.86 Torr 2.3: 0.5 h / 20 - 25 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: diisopropylamine; n-butyllithium / n-heptane; hexane; tetrahydrofuran / 0.25 h / -80 - -70 °C / Inert atmosphere 1.2: 2 h / -80 - -55 °C 1.3: -70 - -10 °C 2.1: hydrogen; sodium acetate / palladium 10% on activated carbon / ethyl acetate; water / 25 - 30 °C / 3677.86 Torr 2.2: 0.5 h / 20 - 25 °C 2.3: 12.5 h / 25 - 30 °C 3.1: sodium hydroxide / dichloromethane; water / 0.5 h / pH 9 - 12 View Scheme | |
Multi-step reaction with 3 steps 1.1: diisopropylamine; n-butyllithium / n-heptane; hexane; tetrahydrofuran / 0.25 h / -80 - -70 °C / Inert atmosphere 1.2: 2 h / -80 - -55 °C 1.3: -70 - -10 °C 2.1: hydrogen; sodium acetate; sodium carbonate / palladium 10% on activated carbon / ethyl acetate; water / 25 - 30 °C / 3677.86 Torr 2.2: 0.5 h / 20 - 25 °C 2.3: 10 - 25 °C 3.1: potassium carbonate / dichloromethane; water / 0.5 h / pH 8 - 10 View Scheme |
4-chloro-5-fluoro-6-ethylpyrimidine
(2R,3S)-2-(2,4-difluorophenyl)-3-(5-fluoro-4-pyrimidinyl)-1-(1H-1,2,4-triazol-1-yl)-2-butanol (1R)-10-camphorsulfonate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: diisopropylamine; n-butyllithium / n-heptane; hexane; tetrahydrofuran / 0.25 h / -80 - -70 °C / Inert atmosphere 1.2: 2 h / -80 - -55 °C 1.3: -70 - -10 °C 2.1: sodium acetate / ethyl acetate; water / 0.5 h / 25 - 30 °C 2.2: 25 - 30 °C / 3677.86 Torr 2.3: 0.5 h / 20 - 25 °C 3.1: acetone; methanol / 15 h / -20 - 25 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: diisopropylamine; n-butyllithium / n-heptane; hexane; tetrahydrofuran / 0.25 h / -80 - -70 °C / Inert atmosphere 1.2: 2 h / -80 - -55 °C 1.3: -70 - -10 °C 2.1: hydrogen; sodium acetate / palladium 10% on activated carbon / ethyl acetate; water / 25 - 30 °C / 3677.86 Torr 2.2: 0.5 h / 20 - 25 °C 2.3: 12.5 h / 25 - 30 °C 3.1: sodium hydroxide / dichloromethane; water / 0.5 h / pH 9 - 12 4.1: acetone; methanol / 15 h / -20 - 25 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: diisopropylamine; n-butyllithium / n-heptane; hexane; tetrahydrofuran / 0.25 h / -80 - -70 °C / Inert atmosphere 1.2: 2 h / -80 - -55 °C 1.3: -70 - -10 °C 2.1: hydrogen; sodium acetate; sodium carbonate / palladium 10% on activated carbon / ethyl acetate; water / 25 - 30 °C / 3677.86 Torr 2.2: 0.5 h / 20 - 25 °C 2.3: 10 - 25 °C 3.1: potassium carbonate / dichloromethane; water / 0.5 h / pH 8 - 10 4.1: acetone; methanol / 15 h / -20 - 25 °C View Scheme |
4-chloro-5-fluoro-6-ethylpyrimidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: diisopropylamine; n-butyllithium / n-heptane; hexane; tetrahydrofuran / 0.25 h / -80 - -70 °C / Inert atmosphere 1.2: 2 h / -80 - -55 °C 1.3: -70 - -10 °C 2.1: hydrogen; sodium acetate; sodium carbonate / palladium 10% on activated carbon / ethyl acetate; water / 25 - 30 °C / 3677.86 Torr 2.2: 0.5 h / 20 - 25 °C 2.3: 10 - 25 °C View Scheme |
4-chloro-5-fluoro-6-ethylpyrimidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: diisopropylamine; n-butyllithium / n-heptane; hexane; tetrahydrofuran / 0.25 h / -80 - -70 °C / Inert atmosphere 1.2: 2 h / -80 - -55 °C 1.3: -70 - -10 °C 2.1: hydrogen; sodium acetate / palladium 10% on activated carbon / ethyl acetate; water / 25 - 30 °C / 3677.86 Torr 2.2: 0.5 h / 20 - 25 °C 2.3: 12.5 h / 25 - 30 °C View Scheme |
4-chloro-5-fluoro-6-ethylpyrimidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / dichloromethane / 16 h / Inert atmosphere; Reflux 2.1: lead; zinc; bromine / dichloromethane; tetrahydrofuran / 30 - 50 °C 2.2: 4 h / 20 - 25 °C View Scheme |
4-chloro-5-fluoro-6-ethylpyrimidine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / dichloromethane / 16 h / Inert atmosphere; Reflux 2.1: lead; zinc; bromine / dichloromethane; tetrahydrofuran / 30 - 50 °C 2.2: 4 h / 20 - 25 °C 3.1: sodium hydroxide / water; methanol / 20 - 25 °C / pH 8 - 9 3.2: 55 - 60 °C 3.3: 1 h / 40 - 45 °C View Scheme |
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