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inquiryBIS(DICYCLOHEXYLPHOSPHINO)METHANE Basic information Product Name: BIS(DICYCLOHEXYLPHOSPHINO)METHANE Synonyms: METHYLENEBIS(DICYCLOHEXYLPHOSPHINE);BIS(DICYCLOHEXYLPHOSPHINO)METHANE;1,2-Bis(dicyclohexylphosphino)methane;Bis(dicyclohexylphosphino
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inquiryBis(dicyclohexylphosphino)methane Application:Bis(dicyclohexylphosphino)methane
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inquirybis-diphenylphosphinomethane
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
With Nb(OC6H3Ph2-2,6)2(CH2C6H4-4Me)3; hydrogen In cyclohexane at 100℃; under 62057.8 Torr; for 96h; | 96% |
With hydrogen In cyclohexane; water | 96% |
Conditions | Yield |
---|---|
at 70℃; for 12h; | 95% |
dicyclohexylphosphane
1,2-dibromomethane
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
Stage #1: dicyclohexylphosphane With cesiumhydroxide monohydrate In N,N-dimethyl-formamide at 20℃; for 1h; Molecular sieve; Inert atmosphere; Stage #2: 1,2-dibromomethane In N,N-dimethyl-formamide at 20℃; for 38h; Inert atmosphere; Molecular sieve; | 85% |
chlorodicyclohexylphosphane
C13H24LiP
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
In tetrahydrofuran at -78 - 20℃; | 83% |
Conditions | Yield |
---|---|
at 240℃; for 0.333333h; Substitution; | 80% |
bis-diphenylphosphinomethane
A
bis(dicyclohexylphosphino)methane
C
CyPCH2PPh2
Conditions | Yield |
---|---|
With n-butyllithium; hydrogen; tris(2,6-diisopropylphenoxy) dichloroniobium(V) In hexane; benzene at 60℃; under 62057.8 Torr; Kinetics; |
cyclohexyl chloride
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: Mg / diethyl ether / 2.5 h / Heating 2: PCl3 / diethyl ether 3: diethyl ether; pentane 4: tert-BuLi / heptane 5: 83 percent / tetrahydrofuran / -78 - 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: Mg / diethyl ether / 2.5 h / Heating 2: PCl3 / diethyl ether 3: 83 percent / tetrahydrofuran / -78 - 20 °C View Scheme |
dicyclohexylmethylphosphine
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tert-BuLi / heptane 2: 83 percent / tetrahydrofuran / -78 - 20 °C View Scheme |
cyclohexylmagnesiumchloride
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: PCl3 / diethyl ether 2: diethyl ether; pentane 3: tert-BuLi / heptane 4: 83 percent / tetrahydrofuran / -78 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: PCl3 / diethyl ether 2: 83 percent / tetrahydrofuran / -78 - 20 °C View Scheme |
chlorodicyclohexylphosphane
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: diethyl ether; pentane 2: tert-BuLi / heptane 3: 83 percent / tetrahydrofuran / -78 - 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: diethyl ether / 2 h / 0 - 20 °C / Inert atmosphere 2: ethylmagnesium bromide / tetrahydrofuran / 0 - 20 °C 3: 12 h / 70 °C View Scheme |
diethyl-dicyclohexylphosphino-amine
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ethylmagnesium bromide / tetrahydrofuran / 0 - 20 °C 2: 12 h / 70 °C View Scheme |
dichloromethane
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
In methanol; toluene to a methanol-soln. of CoCl2*6H2O was added a toluene-soln. of diphosphine, the soln. was stirred for 12 h; stripped to dryness, dissolved in degased CH2Cl2, placed in a freezer; elem. anal.; | 99.2% |
(dimethyl sulfoxide)(2,6-diphenylpyridinate(2-))platinum(II)
bis(dicyclohexylphosphino)methane
[Pt2((C6H4)2C5H3N)2(μ-bis(dicyclohexylphosphino)methane)]
Conditions | Yield |
---|---|
In chloroform mixt. stirred for 12 h under N2 at room temp.; soln. evapd. to dryness; purifn. by chromy. (Al, CH2Cl2 as eluent); elem. anal.; | 99% |
Conditions | Yield |
---|---|
In toluene (N2); addn. of phosphine to palladium complex in toluene, stirring at 20 °C for 5 min; decantation, washing with petroleum ether, drying under vac.; | 98% |
dichloromethane
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
In toluene (N2); addn. of phosphine soln. in toluene to a soln. of palladium complex in toluene, stirring for 12 h at room temp.; filtration, washing with petroleum ether, recrystn. (CH2Cl2-ether) at -25 °C; elem. anal.; | 96% |
copper(l) iodide
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
In acetone mixt. of Cu and P compds. in acetone stirred for 2 h at room temp.; filtered, recrystd. from CH2Cl2/Et2O, elem. anal.; | 95% |
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
Stage #1: [(AuCl)2{μ-(N-butylimidazol-N-yl-2-ylidene)2(CH2)}]; bis(dicyclohexylphosphino)methane In dichloromethane at 20℃; for 3h; Stage #2: ammonium hexafluorophosphate In dichloromethane; acetonitrile at 20℃; for 0.5h; | 95% |
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
In methanol; toluene stirred, 12 h; elem. anal.; | 94% |
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
In ethanol Ar-atmosphere; refluxing for 1 h; evapn., recrystn. (hot EtOH/PhCl=1:1, slow cooling, then standing overnight; two crops), collection (filtration), washing (cold EtOH), drying (vac.); | 94% |
Conditions | Yield |
---|---|
With ortho-difluorobenzene In dichloromethane at 20℃; for 0.5h; Inert atmosphere; Schlenk technique; Sealed tube; | 94% |
bis(cycloocta-1,5-diene)rhodium(I) tetrakis[3,5-bis(trifluoromethyl)phenyl]-borate
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
In dichloromethane at -78 - 20℃; for 16h; Glovebox; Inert atmosphere; Schlenk technique; | 93% |
Conditions | Yield |
---|---|
In hexane N2; equimolar amounts; 1h;; filtration; solvent concentration; crystn. at -40 ° C;; | 92% |
silver(I) hexafluorophosphate
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
In dichloromethane soln. in CH2Cl2 was stirred at 40°C for 5 h; pptn. by Et2O, recrystn. by diffusion of Et2O into a CH2Cl2 soln.; elem. anal.; | 92% |
[(η(5)-C5H5)Fe(CO)(μ-CN)2Cu(CH3CN)2]2
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
In dichloromethane; acetonitrile all manipulations under Ar atm.; soln. of org. compd. in CH2Cl2 slowly added to soln. of complex in MeCN, stirred for 30 min at ambient temp.; solvent removed in vac.; | 92% |
silver trifluoromethanesulfonate
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
In dichloromethane ssoln. in CH2Cl2 was stirred for 6 h; pptn. by Et2O, recrystn. by diffusion of Et2O into an acetonitrile soln.; elem. anal.; | 90% |
cis-(tungsten tetracarbonyl bipiperidine)
bis(dicyclohexylphosphino)methane
[W(CO)4(bis(dicyclohexylphosphino)methane)]
Conditions | Yield |
---|---|
In dichloromethane (N2); reflux of PCy2CH2PCy2 and W(CO)4(NHC5H10)2 in CH2Cl2 for 4.5 h; cooling, filtration, addn. of MeOH; placing of mixt. in the freezer; removal of cryst., concn. of soln. on rotary evaporator; cooling in the freezer; crystn., elem. anal.; | 90% |
bis(dicyclohexylphosphino)methane
((C6H11)2PCH2P(C6H11)2O)Co(NO3)2
Conditions | Yield |
---|---|
In methanol; dichloromethane; toluene to a methanol soln. of Co-salt was added a toluene-soln. of diphosphine,CH2Cl2 was added to the soln., stirred for 12 h; stripped to dryness, dissolved in degased CH2Cl2, allowed to slow evapn.; elem. anal.; | 89.4% |
tetrakis(acetonitrile)copper(I) perchlorate
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
In acetone mixt. of Cu and P compds. in acetone stirred for 1 h at room temp.; solvent removed, Et2O added, recrystd. from CH2Cl2/Et2O, elem. anal.; | 89% |
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
In dichloromethane at -78 - 20℃; for 16h; Glovebox; Inert atmosphere; Schlenk technique; | 89% |
bis(acetonitrile)dichloroplatinum(II)
dichloromethane
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
In dichloromethane stirring of CH2Cl2 soln. of Pt(NCMe)2Cl2 (1 equiv.) and PCy2CH2PCy2 (2 equiv.) for 48 h; concd., filtration, drying in vac., elem. anal.; | 88% |
(tetrahydrothiophene)gold(I) chloride
bis(dicyclohexylphosphino)methane
[Au2(bis(dicyclohexylphosphanyl)methane)Cl2]
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 0.5h; Inert atmosphere; Schlenk technique; | 87% |
In tetrahydrofuran stoichiometric amounts of Au-complex and phosphine in THF; pptn. with pentane, vac.-filtered; |
tetrakis(actonitrile)copper(I) hexafluorophosphate
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
In acetone mixt. of Cu and P compds. in acetone stirred for 1 h at room temp.; solvent removed, Et2O added, recrystd. from CH2Cl2/Et2O, elem. anal.; | 86% |
dichloromethane
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
In toluene byproducts: CO; (N2); reflux of toluene soln. of Fe2(CO)6(SCH2CH2CH2S) and PCy2CH2PCy2 for 16 h; cooling to room temp., removal of volatiles by rotary evapn., washing with hexane; drying; dissolving in min. of CH2Cl2; chromy. on alumina; eluting with Et2O:hexane (1:9); elem. anal.; | 84% |
bis(dicyclohexylphosphino)methane
(((C6H11)2P)2CH2)Rh(OC(CF3))2CH
Conditions | Yield |
---|---|
In tetrahydrofuran Ar-atmosphere; slow phosphine soln. addn.; crystn.; elem. anal.; | A 82% B n/a |
2,6-di-tert-butylphenol
bis(dicyclohexylphosphino)methane
Conditions | Yield |
---|---|
In toluene under Ar; toluene soln. of phosphine and substituted phenol (molar ratio 1:2) added to neat Zn compd.; stirred for 0.5 h; volatiles stripped away in vac.; | 82% |
bis(dicyclohexylphosphino)methane
(bis(dicyclohexylphosphino)methane)dimethylpalladium(II)
Conditions | Yield |
---|---|
In benzene at room temp.; characterized spectroscopically and by single crystal X-ray diffraction; | 82% |
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