As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for t
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inquiryProduct description: Product name 2,6-Di-tert-butylphenol CAS number 128-39-2 Assay ≥99% Appearance White solid Capacity 1000mt/year Application Rubber antioxidant, fuel stab
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryProduct Name: 2,6-Di-tert-butylphenol Synonyms: Hitec4701;Isonox 103;Isonox103;Lowinox 001;Phenol, 2,6-bis(t-butyl);Phenol, 2,6-di-tert-butyl-;phenol,2,6-bis(1,1-dimethylethyl)-;Phenol,2,6-di-tert-butyl- CAS: 128-39-2 MF: C14H22O MW: 206.32 EI
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inquiryAbout Product Details
Cas:128-39-2
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inquiryProName:2,6-Di-tert-butylphenol CasNo:128-39-2 Molecular Formula:C14H22O Appearance:White solid Application:Rubber antioxidant, fuel stabilizer, U... DeliveryTime:Immediately PackAge:25kg/drum Port:Shanghai or Qingdao ProductionCapacity:100
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time pr
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inquiryName: 2,6-Di-tert-butylphenol Synonyms: 2,6-Di-(tert-butyl)phenol CAS:128-39-2 MF: C14H21KO Appearance: white powder Storage:Store in cool and dry place, away from sun light. Package: 25kgs/drum Application: Rubber Antioxidant Transportation:By se
We are leading fine chemicals supplier in China and Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediat
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inquiryAppearance:Colorless transparent liquid Storage:R.T Package:180kg/Barrel Application:Used in the preparation of antioxidant 2,6-di-tert-butyl-p-cresol, rubber antioxidant, cresol-formaldehyde resin and plasticizer, used as a disinfectant in medicine
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryProduct Name: 2,6-Di-tert-butylphenol CAS: 128-39-2 MF: C14H22O MW: 206.32 EINECS: 204-884-0 Mol File: 128-39-2.mol 2,6-Di-tert-butylphenol Structure 2,6-Di-tert-butylphenol Chemical Properties Melting point 34-37 °C(lit.)
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inquiryE2,6-Di-tert-butylphenol CAS:128-39-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
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inquirySuperiority We can customize and synthesize products that other suppliers may not be able to provide. Advantage cof, mof ligand manufacturer Product Detail bes
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inquiryPacking: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:white powder/ Refer to COA Storage:Refer to COA
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Appearance:white powder Storage:Store in a cool,dry place and keep away from direct strong light Package:as customer request Application:Use only for laboratory research Transportation:Sea,Air,DHL/TNT/FEdex/UPS/EMS Port:QINGDAO
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:128-39-2
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquirySuperior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediates Tr
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermediat
Cas:128-39-2
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:128-39-2
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inquiryProduct name: 2,6-Di-Tert-Butylphenol CAS No.:128-39-2 Molecule Formula:C14H22O Molecule Weight:206.32 Purity: 98% Package: 180kg/drum Description:White or light yellow crystalline powder Manufacture Standards:Enterprise Standard
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
tert-butyl (2,6-di-tert-butylphenyl)carbonate
2,6-di-tert-butylphenol
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane for 3h; Product distribution; Heating; deprotection; | 89% |
Conditions | Yield |
---|---|
With decarboxylase at 25℃; for 15h; pH=6.5; Enzymatic reaction; | 84.1% |
Conditions | Yield |
---|---|
With lithium; ethylenediamine In tetrahydrofuran at -10℃; for 0.5h; | 82% |
tert-butyl alcohol
phenol
A
para-tert-butylphenol
B
2,6-di-tert-butylphenol
C
2-tert-Butylphenol
Conditions | Yield |
---|---|
With aluminium(III) phenoxide In various solvent(s) at 130℃; for 2h; | A 9.4% B 1.8% C 70.4% |
4-bromo-2,6-di-tert-butylphenol
bicyclo[2.2.1]hepta-2,5-diene
A
2,6-di-tert-butylphenol
Conditions | Yield |
---|---|
With ammonium formate; palladium diacetate; triphenylphosphine In N,N-dimethyl-formamide at 90℃; for 24h; Heck Reaction; Schlenk technique; Inert atmosphere; | A 20% B 68% |
isobutene
phenol
A
para-tert-butylphenol
B
2,6-di-tert-butylphenol
C
t-butyl phenyl ether
D
2-tert-Butylphenol
E
2,4-di-tert-Butylphenol
Conditions | Yield |
---|---|
2-phenoxy-1,2-thialuminolane at 110℃; for 3h; Product distribution; Mechanism; other catalysts, other time, other temperature; | A 1.23% B 4.97% C 0.8% D 66.67% E 2.37% |
isobutene
phenol
A
2,6-di-tert-butylphenol
B
t-butyl phenyl ether
C
2-tert-Butylphenol
D
2,4-di-tert-Butylphenol
Conditions | Yield |
---|---|
2-phenooxy-1,2-thialuminolane at 110℃; for 3h; Further byproducts given; | A 4.97% B 0.8% C 66.67% D 2.37% |
potassium 2,6-di-tert-butylphenolate
A
2,6-di-tert-butylphenol
Conditions | Yield |
---|---|
Stage #1: C23H26N2*BF4(1-)*H(1+); potassium 2,6-di-tert-butylphenolate In dimethyl sulfoxide for 0.0166667h; Stage #2: With ammonium hydroxide In dimethyl sulfoxide pH=10; | A 26% B 64% |
carbon dioxide
2,6-di-tert-butyl-anisole
A
2,6-di-tert-butylphenol
B
1,3-di-tert-butylbenzene
C
2,6-di-tert-butylbenzoic acid
Conditions | Yield |
---|---|
Stage #1: 2,6-di-tert-butyl-anisole With 4,4'-di-tert-butylbiphenyl; lithium In tetrahydrofuran at 20℃; for 1.55h; Inert atmosphere; Stage #2: carbon dioxide In tetrahydrofuran for 0.5h; Heating; | A 7% B 30% C 63% |
4-bromo-2,6-di-tert-butyl-2,5-cyclohexadienone
A
2,6-di-tert-butylphenol
B
2,6-Di-tert-butyl-1,4-benzoquinone
C
3,5,3',5'-tetra-tert-butyl-4,4'-diphenoquinone
D
2,6-Di-tert-butyl-4-iodophenol
E
4-bromo-2,6-di-tert-butylphenol
F
2,6-Di-t-butyl-4-methoxyphenol
Conditions | Yield |
---|---|
With iodine In methanol; water at 35℃; for 0.0833333h; Product distribution; | A 5% B 18% C 7% D 1% E 62% F 6% |
tert-butyl alcohol
phenol
A
para-tert-butylphenol
B
2,6-di-tert-butylphenol
C
2-tert-Butylphenol
D
2,4-di-tert-Butylphenol
Conditions | Yield |
---|---|
With carbon tetrabromide at 175℃; for 6h; Sealed tube; | A 33% B 3% C 9% D 49% |
With 3-methyl-1-(4-sulfobutyl)imidazol-3-ium methanesulfonate at 70℃; for 2h; Temperature; Sealed tube; | |
With 1-(4-sulfonic acid)butylpyridinium methane sulfonate at 80℃; for 2h; Reagent/catalyst; Sealed tube; | |
With N-(4-sulfonic acid)butyl triethylammonium methane sulfonate at 80℃; for 2h; Catalytic behavior; Kinetics; Temperature; Reagent/catalyst; Sealed tube; |
tertiary butyl chloride
ortho-isobornylphenol
A
2,6-di-tert-butylphenol
Conditions | Yield |
---|---|
With montmorillonite KSF In dichloromethane for 5h; Reflux; | A 7% B 32% C 48% D n/a |
tert-butyl alcohol
phenol
A
para-tert-butylphenol
B
2,6-di-tert-butylphenol
C
2-tert-Butylphenol
D
2,4-di-tert-Butylphenol
E
2,4,6-tri-tert-butylphenoxol
Conditions | Yield |
---|---|
With carbon tetrabromide at 150℃; for 6h; Sealed tube; | A 9% B 10% C 20% D 39% E 14% |
With carbon tetrabromide at 175℃; for 6h; Sealed tube; | A 6% B 13% C 16% D 34% E 25% |
With tetrachloromethane at 175℃; for 6h; Sealed tube; | A 17% B 4% C 21% D 23% E 7% |
With Bromoform at 175℃; for 6h; Sealed tube; | A 21% B 1% C 21% D 22% E 1% |
3,5-di-tert-butyl-4-hydroxybenzyl alcohol
2-pentyl-4,6-bis-trichloromethyl-[1,3,5]triazine
A
2,6-di-tert-butylphenol
B
4,4'-Methylenebis(2,6-di-tert-butylphenol)
C
2,6-Di-tert-butyl-4-(4-pentyl-6-trichloromethyl-[1,3,5]triazin-2-yloxymethyl)-phenol
Conditions | Yield |
---|---|
With triethylamine In 1,4-dioxane at 60℃; for 4h; | A 0.55 g B 0.35 g C 38% |
3,5-di-tert-butyl-4-hydroxybenzyl alcohol
A
2,6-di-tert-butylphenol
B
4,4'-Methylenebis(2,6-di-tert-butylphenol)
C
2,6-Di-tert-butyl-4-(4-phenyl-6-trichloromethyl-[1,3,5]triazin-2-yloxymethyl)-phenol
Conditions | Yield |
---|---|
With 2-phenyl-4,6-bis-trichloromethyl-[1,3,5]triazine; triethylamine In 1,4-dioxane at 60℃; for 4h; | A 0.55 g B 0.35 g C 32% |
3,5-di-tert-butyl-4-hydroxybenzyl alcohol
2-phenyl-4,6-bis-trichloromethyl-[1,3,5]triazine
A
2,6-di-tert-butylphenol
B
4,4'-Methylenebis(2,6-di-tert-butylphenol)
C
2,6-Di-tert-butyl-4-(4-phenyl-6-trichloromethyl-[1,3,5]triazin-2-yloxymethyl)-phenol
Conditions | Yield |
---|---|
With triethylamine In 1,4-dioxane at 60℃; for 4h; | A 0.55 g B 0.35 g C 32% |
dioxomolybdenum(VI) dichloride
lithium 2,6-di-tert-butylphenolate
B
2,6-di-tert-butylphenol
C
3,5,3',5'-tetra-tert-butyl-4,4'-diphenoquinone
Conditions | Yield |
---|---|
In acetonitrile MoO2Cl2 soln. in CH3CN was added to LiO(2,6-t-Bu2C6H3) soln. in CH3CN and mixt. was stirred for 1 h; solvent was removed in vacuo, solved in pentane, filtered and placed in-35°C freezer for 2 days; elem. anal.; | A 31% B n/a C n/a |
2,6-di-tert-butyl-4-methyl-phenol
phenol
A
p-cresol
B
para-tert-butylphenol
C
2-tert-Butyl-4-methylphenol
D
2,6-di-tert-butylphenol
E
2-tert-Butylphenol
F
2,4-di-tert-Butylphenol
Conditions | Yield |
---|---|
C24H20ClNbO4 at 140℃; for 3h; Product distribution; Rate constant; Mechanism; also with 2-methylphenol, other catalysts, other products; | A 14% B 8% C 30.5% D 2% E 20% F 15% |
2,6-di-tert-butyl-4-diazo-2,5-cyclohexadien-1-one
A
2,6-di-tert-butylphenol
B
3,5,3',5'-tetra-tert-butyl-4,4'-diphenoquinone
C
4,4'-dihydroxy-3,3',5,5'-tetra-tert-butylbiphenyl
Conditions | Yield |
---|---|
With cyclohexane In pyridine for 3h; Heating; Further byproducts given. Title compound not separated from byproducts; | A n/a B n/a C n/a D 29% |
ethanol
benzene-1,2-diol
A
2,6-di-tert-butylphenol
B
2,4-diisopropylphenol
C
2,5-diethyl phenol
Conditions | Yield |
---|---|
With perrhenic acid anhydride at 320℃; for 6h; Inert atmosphere; Sealed tube; | A 5.8% B 10.1% C 5.2% |
((CH3)3SiCH2)2Ta(CSi(CH3)3)2Ta(OC6H3(C4H9)2)2
A
tetramethylsilane
B
Ta(OC6H3-t-BuCMe2CH2)2(CH2SiMe3)
C
2,6-di-tert-butylphenol
Conditions | Yield |
---|---|
In (2)H8-toluene heated at 150°C in a sealed NMR tube for 5-10 h; not isolated ((1)H NMR data); yield of the cyclometallated complex increases when thermolysis is carried out in the presence of 2 or more equiv of 2,6-t-Bu2C6H3OH; | A n/a B 5% C n/a |
Conditions | Yield |
---|---|
With sodium hydroxide; aluminum nickel; ethanol |
Conditions | Yield |
---|---|
With sodium hydroxide; aluminum nickel; ethanol | |
With ammonia; potassium |
Conditions | Yield |
---|---|
With aluminium(III) phenoxide | |
With aluminium(III) phenoxide |
Conditions | Yield |
---|---|
With aluminium(III) phenoxide |
2-tert-Butylphenol
2,4,6-tri-tert-butylphenoxol
A
2,6-di-tert-butylphenol
B
2,4-di-tert-Butylphenol
Conditions | Yield |
---|---|
sulfuric acid at 110℃; for 4h; Equilibrium constant; Product distribution; other temperature, other time; | |
at 80 - 180℃; Equilibrium constant; |
Conditions | Yield |
---|---|
sulfuric acid at 180℃; for 7h; Equilibrium constant; Product distribution; other catalysis, other temperature, other time; |
2,6-Di-tert-butyl-1,4-benzoquinone
A
2,6-di-tert-butylphenol
B
3,5,3',5'-tetra-tert-butyl-4,4'-diphenoquinone
Conditions | Yield |
---|---|
With oxygen; N-(2-aminoethyl)-N'-{2-[(2-aminoethyl)amino]ethyl}ethane-1,2-diamine In methanol; water at 35℃; Equilibrium constant; Mechanism; Rate constant; other catalysts are also investigated; |
3,5,3',5'-tetra-tert-butyl-4,4'-diphenoquinone
A
2,6-di-tert-butylphenol
B
2,6-Di-tert-butyl-1,4-benzoquinone
Conditions | Yield |
---|---|
With oxygen; N-(2-aminoethyl)-N'-{2-[(2-aminoethyl)amino]ethyl}ethane-1,2-diamine In methanol; water at 35℃; Equilibrium constant; Mechanism; Rate constant; other catalysts are also investigated; |
Conditions | Yield |
---|---|
With potassium hydroxide; iodine In methanol for 0.25h; | 100% |
With 2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate; potassium hydrogencarbonate In water; acetonitrile for 1h; | 100% |
With oxygen; pyridine; copper(I) In methanol at 60℃; for 6h; | 100% |
2,6-di-tert-butylphenol
2,6-Di-tert-butyl-4-iodophenol
Conditions | Yield |
---|---|
With bis(2,4,6-trimethylpyridine)iodine(I) hexafluorophosphate In dichloromethane for 0.0833333h; Ambient temperature; | 100% |
With tetrabutylammomium bromide; iodine; oxygen; copper(II) nitrate In water at 80℃; under 760.051 Torr; for 6h; Green chemistry; regioselective reaction; | 89% |
With aluminum oxide; periodic acid In 1,4-dioxane for 3h; Heating; | 78% |
Conditions | Yield |
---|---|
With pyridine; oxygen; Co(babp) In toluene at 20℃; under 760 Torr; for 24h; Mechanism; Product distribution; other reaction temperatures and times, without solvent, with 4-methylpyridine, 4-(dimethylamino)pyridine or 1-azabicyclo<2.2.2>octane, re-use of catalyst; | 100% |
With pyridine; oxygen; Co(babp) In toluene at 20℃; under 760 Torr; for 24h; | 100% |
With cobalt(II); oxygen In N,N-dimethyl-formamide for 1h; | 100% |
2,6-di-tert-butylphenol
[6-Hydroxy-2,7,8-trimethyl-2-(4,8,12-trimethyltridecyl)chroman-5-yl]methyl bromide
Conditions | Yield |
---|---|
With hydrogen bromide; zinc(II) chloride In hexane; dichloromethane at 50℃; for 4h; | 100% |
Sm(OC(=C6H6)Ph)2(O-C6H2-(t)Bu2-2,6-Me-4)(hexamethylphosphoramide)2
2,6-di-tert-butylphenol
Sm(OC(=C6H6)Ph)2(O-C6H3-(t)Bu2-2,6)(hexamethylphosphoramide)2
Conditions | Yield |
---|---|
In benzene Ar or N2-atmosphere; 2 equivs. of phenol; | 100% |
2,6-di-tert-butylphenol
C14H21Cl3OTe
Conditions | Yield |
---|---|
With tellurium tetrachloride In tetrachloromethane at 0 - 20℃; for 2h; | 100% |
With tellurium tetrachloride In tetrachloromethane at 0 - 20℃; for 2h; |
2,6-di-tert-butylphenol
Conditions | Yield |
---|---|
In benzene-d6 at 24℃; for 18h; | 100% |
2,6-di-tert-butylphenol
Conditions | Yield |
---|---|
In hexane at 20℃; | 100% |
2,6-di-tert-butylphenol
Conditions | Yield |
---|---|
In toluene at 20℃; for 18h; | 100% |
trimethylsilyl isothiocyanate
2,6-di-tert-butylphenol
3,5-di-tert-butyl-4-hydroxyphenylthiocyanate
Conditions | Yield |
---|---|
With 1-chloro-1λ3-benzo[d][1,2]iodaoxol-3(1H)-one In dichloromethane at 20℃; for 1h; | 100% |
2,6-di-tert-butylphenol
2,4,6-tris(chloromethyl)-mesitylene
1,3,5-trimethyl-2,4,6-tris-(3,5-di-tert-butyl-4-hydroxybenzyl)benzene
Conditions | Yield |
---|---|
With hydrogenchloride; 15-crown-5; 3,4,7,8-Tetramethyl-o-phenanthrolin; cadmium(II) iodide; ytterbium(III) triflate In tetrachloromethane; water at 50℃; for 10h; Catalytic behavior; Concentration; Reagent/catalyst; Temperature; Solvent; | 99.5% |
Conditions | Yield |
---|---|
Stage #1: 2,6-di-tert-butylphenol With oxygen In tert-butyl alcohol at 70℃; under 760.051 Torr; for 18h; Green chemistry; Stage #2: With hydrogen In tert-butyl alcohol at 60℃; under 760.051 Torr; for 4h; Green chemistry; | 99% |
With CuCl(OH)*TMEDA In dichloromethane at 20℃; for 2h; | 96% |
Stage #1: 2,6-di-tert-butylphenol In dichloromethane at 20℃; for 2h; Stage #2: With sodium dithionite In ethanol for 2h; Heating; | 96% |
2,6-di-tert-butylphenol
potassium 2,6-di-tert-butylphenolate
Conditions | Yield |
---|---|
With potassium hexamethylsilazane In tetrahydrofuran at 20℃; for 15h; | 99% |
With potassium tert-butylate In ethanol for 0.25h; | 92% |
With potassium hydroxide In 5,5-dimethyl-1,3-cyclohexadiene for 5h; Solvent; Reflux; Inert atmosphere; | 88.5% |
With potassium hydroxide; potassium tert-butylate |
2,6-di-tert-butylphenol
acrylic acid methyl ester
methyl 3-(4-hydroxy-3,5-di-tert-butyl)phenylpropanoate
Conditions | Yield |
---|---|
Stage #1: 2,6-di-tert-butylphenol With tri-n-butyltin acetate; zinc(II) carbonate Inert atmosphere; Heating; Stage #2: acrylic acid methyl ester at 70 - 90℃; for 1.5h; Inert atmosphere; | 99% |
With potassium tert-butylate 1) t-BuOH, 2) water, 116 deg C, 2 h; Yield given. Multistep reaction; | |
With potassium tert-butylate; water Mechanism; Rate constant; 1) t-BuOH, 2) 116 deg C; inhibiting effect of water; |
Conditions | Yield |
---|---|
With sodium methoxide-d3 at 50℃; for 24h; Methylation; Substitution; | 99% |
2,6-di-tert-butylphenol
(salen(tBu,tBu)Sc(N(SiHMe2)2)
(N,N'-bis(3,5-bis(tert-butyl)-2-oxy-benzylidene)-1,2-ethanediamine)(2,6-bis(tert-butyl)phenolato)scandium(III)
Conditions | Yield |
---|---|
In hexane byproducts: HN(SiH(CH3)2)2; under Ar; phenol deriv. added to soln. of Sc complex in hexane, mixt. stirred for 2 h; evapd. under vac., crystd. from toluene; elem. anal.; | 99% |
2,6-di-tert-butylphenol
Conditions | Yield |
---|---|
In hexane byproducts: HN(SiH(CH3)2)2; under Ar; phenol deriv. added to soln. of Sc complex in hexane, mixt. stirred for 2 h; evapd. under vac., crystd. from toluene; elem. anal.; | 99% |
2,6-di-tert-butylphenol
4,4'-Dimethoxybenzhydrol
4',4''-Dimethoxy-3,5-di-tert.-butyl-4-hydroxy-triphenylmethan
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate In 1,2-dichloro-ethane at 60℃; for 4h; Green chemistry; | 99% |
Conditions | Yield |
---|---|
Stage #1: 2,6-di-tert-butylphenol; 6-bromo-2-pyrrolidinobenzaldehyde With piperidine In toluene at 120℃; for 12h; Stage #2: In ethanol at 25℃; for 0.05h; Time; | 99% |
2,6-di-tert-butylphenol
2,4-bis(3,5-di-tert-butyl-4-hydroxyphenyl)-1,3,2,4-dithiadiphosphetane-2,4-disulfide
bis(3,5-di-t-butyl-4-hydroxyphenyl)phosphinodithioic acid
Conditions | Yield |
---|---|
at 160℃; | 98.5% |
1,1-Diphenylmethanol
2,6-di-tert-butylphenol
3,5-di-tert-butyl-4-hydroxyphenyldiphenylmethane
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate In 1,2-dichloro-ethane at 60℃; for 8h; | 98% |
With tris(pentafluorophenyl)borate In 1,2-dichloro-ethane at 60℃; for 4h; Green chemistry; | 95% |
With sulfuric acid In acetic acid |
2,6-di-tert-butylphenol
3,5-di-tert-butyl-4-hydroxybenzenesulfonic acid
Conditions | Yield |
---|---|
With sulfur trioxide In nitromethane at 0℃; for 0.5h; Product distribution; | 98% |
2,6-di-tert-butylphenol
Conditions | Yield |
---|---|
With oxygen; manganese(II); iron(III); magnesium oxide; copper In benzene for 24h; Product distribution; Ambient temperature; | 98% |
With oxygen; manganese; magnesium oxide In benzene for 24h; Ambient temperature; | 98% |
With manganese(III) triacetate dihydrate; sodium hydroxide In water; acetonitrile at 25℃; for 4h; Reagent/catalyst; Solvent; Time; | 94% |
phthalimidesulfenyl chloride
2,6-di-tert-butylphenol
Conditions | Yield |
---|---|
In chloroform at 20℃; Substitution; | 98% |
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate In 1,2-dichloro-ethane at 60℃; for 4h; Green chemistry; | 98% |
With sulfuric acid; acetic acid |
2,6-di-tert-butylphenol
1-(4-chlorophenyl)-3-phenylprop-2-yn-1-ol
Conditions | Yield |
---|---|
With tin(ll) chloride In nitromethane at 40℃; for 0.166667h; | 98% |
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate In 1,2-dichloro-ethane at 60℃; for 4h; Green chemistry; | 98% |
With sulfuric acid In dichloromethane at 0 - 25℃; for 0.333333h; Inert atmosphere; Schlenk technique; |
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate In 1,2-dichloro-ethane at 60℃; for 8h; | 98% |
With tris(pentafluorophenyl)borate In 1,2-dichloro-ethane at 60℃; for 4h; Green chemistry; | 89% |
Conditions | Yield |
---|---|
Stage #1: 4-cyano-2-pyrrolidinylbenzaldehyde; 2,6-di-tert-butylphenol With piperidine In toluene at 120℃; for 12h; Stage #2: 1,1,1,3',3',3'-hexafluoro-propanol In ethanol at 25℃; for 0.833333h; | 98% |
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