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inquiry2,4,6-Tri-tert-butylphenol CAS:732-26-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
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inquiryProduct name: 2,4,6-Tri-Tert-Butylphenol CAS No.:732-26-3 Molecule Formula:C18H30O Molecule Weight:262.43 Purity: 98% Package: 180kg/drum Description:White or light yellow crystalline powder Manufacture Standards:Enterprise Standard
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2,4,6-tri-tert-butylphenoxyl
A
2,4,6-tri-tert-butylphenoxol
Conditions | Yield |
---|---|
With [hydrogen(diethyl ether)][tetra[3,5-bis(trifluoromethyl)phenyl]borate] | A 50% B 100% |
2,4,6-tri-tert-butyl phenoxyl radical
A
2,4,6-tri-tert-butylphenoxol
Conditions | Yield |
---|---|
In [D3]acetonitrile at -30℃; for 0.116667h; | A 100% B n/a C n/a D n/a |
Conditions | Yield |
---|---|
With 2,4,6-tri-tert-butylphenoxyl | A 20% B 90% |
2,4,6-tri-tert-butylphenoxyl
A
2,4,6-tri-tert-butylphenoxol
Conditions | Yield |
---|---|
With [hydrogen(diethyl ether)][tetra[3,5-bis(trifluoromethyl)phenyl]borate] | A 65% B 85% |
4-bromo-2,4,6-tri-tert-butyl-2,5-cyclohexadiene-1-one
2,4,6-tri-tert-butylphenoxol
Conditions | Yield |
---|---|
In isopropyl alcohol for 1h; Heating; | 80% |
With picoline In ethylene glycol at 110℃; for 1h; | 80% |
4-Phenylurazole
2,4,6-tri-tert-butylphenoxyl
A
2,4,6-tri-tert-butylphenoxol
Conditions | Yield |
---|---|
In benzene at 25℃; for 7h; | A n/a B 78% |
2,4,6-tri-tert-butylphenoxyl
mofebutazone
A
2,4,6-tri-tert-butylphenoxol
Conditions | Yield |
---|---|
In benzene at 25℃; for 2.5h; | A 50% B 78% |
oxirane
2,6-di-tert-butylphenol
A
2,4,6-tri-tert-butylphenoxol
B
2-(3,5-di-t-butyl-4-hydroxyphenyl)ethanol
C
2,6-di-tert-butyl-4,4-bis(2-hydroxyethyl)cyclohexa-2,5-dien-1-one
D
ethylene glycol 2-(3,5-di-tert-butyl-4-hydroxyphenyl)-ethyl ether
Conditions | Yield |
---|---|
With tin(IV) chloride In Trichloroethylene at -10 - 10℃; | A 4% B 75% C n/a D n/a |
{Fe4S4(S-2,4,6-(i-Pr)3C6H2)4}(3-)
2,4,6-tri-tert-butylphenoxyl
B
2,4,6-tri-tert-butylphenoxol
Conditions | Yield |
---|---|
With [hydrogen(diethyl ether)][tetra[3,5-bis(trifluoromethyl)phenyl]borate] | A 75% B 50% |
tert-butyl alcohol
phenol
A
para-tert-butylphenol
B
2,4-di-tert-Butylphenol
C
2,4,6-tri-tert-butylphenoxol
Conditions | Yield |
---|---|
With carbon tetrabromide at 175℃; for 6h; Sealed tube; | A 24% B 67% C 9% |
2,6-di-tert-butylphenol
2,4,6-tri-tert-butylphenoxyl
A
2,4,6-tri-tert-butylphenoxol
B
3,5,3',5'-tetra-tert-butyl-4,4'-diphenoquinone
Conditions | Yield |
---|---|
With triethylamine In benzene Product distribution; varying time-interval before addition of reag.; varying amount of reag.; | A 66% B 29% C 44% D 25% |
With triethylamine In benzene at 6 - 8℃; Further byproducts given; | A 66% B 29% C 42% D 25% |
With triethylamine In benzene at 6 - 8℃; | A 66% B 29% C 42% D 25% |
2,4,6-tri-tert-butylphenoxyl
2-(4-methoxy-phenyl)-2,3-dihydro-phthalazine-1,4-dione
A
2,4,6-tri-tert-butylphenoxol
B
2,3-Dihydro-2-(4-methoxyphenyl)-3-(1,3,5-tri-tert-butyl-4-oxocyclohexa-2,5-dien-1-yl)phthalazin-1,4-dion
Conditions | Yield |
---|---|
With magnesium sulfate; potassium carbonate In chlorobenzene Yield given; | A n/a B 65% |
With magnesium sulfate; potassium carbonate In chlorobenzene Yields of byproduct given; | A n/a B 65% |
3,5-Lutidine
4-bromo-2,4,6-tri-tert-butyl-2,5-cyclohexadiene-1-one
A
2,4,6-tri-tert-butylphenoxol
B
2,4-di-tert-butyl-6-chlorophenol
C
C21H29NO
D
2-(1,3,5-tri-tert-butyl-4-oxo-2,5-cyclohexadien-1-oxy)ethanol
Conditions | Yield |
---|---|
In ethylene glycol at 110℃; for 1h; Further byproducts given; | A 8% B n/a C 60% D 15% |
2,4,6-tri-tert-butylphenoxyl
2-phenyl-2,3-dihydro-phthalazine-1,4-dione
A
2,4,6-tri-tert-butylphenoxol
B
2,3-Dihydro-2-phenyl-3-(1,3,5-tri-tert-butyl-4-oxocyclohexa-2,5-dien-1-yl)phthalazin-1,4-dion
Conditions | Yield |
---|---|
With magnesium sulfate; potassium carbonate In chlorobenzene Yield given; | A n/a B 60% |
With magnesium sulfate; potassium carbonate In chlorobenzene Yields of byproduct given; | A n/a B 60% |
2-Methylcyclopentane-1,3-dione
2,4,6-tri-tert-butylphenoxyl
A
2,4,6-tri-tert-butylphenoxol
B
2,4,6-tri-tert-butyl-4-hydroxy-2,5-cyclohexadienone
Conditions | Yield |
---|---|
In benzene at 25℃; for 9h; | A 54% B 58% C 32% |
2,4,6-tri-t-butyl-4-nitrocyclohexa-2,5-dien-1-one
A
2,6-Di-tert-butyl-1,4-benzoquinone
B
2,4,6-tri-tert-butylphenoxol
C
3,5-di-tert-butyl-o-benzoquinone
D
2,4,6-tri-tert-butyl-4-hydroxy-2,5-cyclohexadienone
Conditions | Yield |
---|---|
In methanol at 30℃; for 70h; Further byproducts given; | A 3% B 13% C 18% D 58% |
2,4,6-tri-t-butyl-4-nitrocyclohexa-2,5-dien-1-one
A
2,4,6-tri-tert-butylphenoxol
B
3,5-di-tert-butyl-o-benzoquinone
C
2,4,6-tri-tert-butyl-4-hydroxy-2,5-cyclohexadienone
D
2,4-di-t-butyl-4,6-dimethoxycyclohexa-2,5-dienone
Conditions | Yield |
---|---|
In methanol at 30℃; for 70h; Further byproducts given; | A 13% B 18% C 58% D 6% |
tert-butylmercury chloride
potassium 2,4-di-tert-butylphenolate
2,4,6-tri-tert-butylphenoxol
Conditions | Yield |
---|---|
With 18-crown-6 ether In N,N,N,N,N,N-hexamethylphosphoric triamide at 35 - 40℃; for 2h; Irradiation; | 58% |
With 18-crown-6 ether In N,N,N,N,N,N-hexamethylphosphoric triamide at 35 - 40℃; for 2h; Product distribution; Irradiation; presence of (t-Bu)2NO free radical trap; in DMSO; | 58% |
methanol
2,4,6-tri-t-butyl-4-nitrocyclohexa-2,5-dien-1-one
A
2,4,6-tri-tert-butylphenoxol
B
3,5-di-tert-butyl-o-benzoquinone
C
2,4,6-tri-tert-butyl-4-hydroxy-2,5-cyclohexadienone
D
2,4-di-t-butyl-4,6-dimethoxycyclohexa-2,5-dienone
Conditions | Yield |
---|---|
at 30℃; for 70h; Further byproducts given; | A 13% B 18% C 56% D 6% |
2,6-di-tert-butylphenol
2,4,6-tri-tert-butylphenoxyl
A
2,4,6-tri-tert-butylphenoxol
B
3,5,3',5'-tetra-tert-butyl-4,4'-diphenoquinone
C
3,3’,5,5’-tetra-tert-butyl-[1,1‘-biphenyl]-2,4’-diol
D
4,4'-dihydroxy-3,3',5,5'-tetra-tert-butylbiphenyl
Conditions | Yield |
---|---|
With trifluoroacetic acid In benzene Product distribution; varying time-interval before addition of reag.; | A 56% B 17% C 56% D 24% |
With trifluoroacetic acid In benzene at 6 - 8℃; for 0.25h; | A 56% B 17% C 56% D 24% |
2,4,6-tri-tert-butylphenoxyl
2-(4-nitrophenyl)-1,4-phthalazinediones
A
2,4,6-tri-tert-butylphenoxol
B
2,3-Dihydro-2-(4-nitrophenyl)-3-(1,3,5-tri-tert-butyl-4-oxocyclohexa-2,5-dien-1-yl)phthalazin-1,4-dion
Conditions | Yield |
---|---|
With magnesium sulfate; potassium carbonate In chlorobenzene Yields of byproduct given; | A n/a B 55% |
tert-butyl alcohol
phenol
A
para-tert-butylphenol
B
2-tert-Butylphenol
C
2,4-di-tert-Butylphenol
D
2,4,6-tri-tert-butylphenoxol
Conditions | Yield |
---|---|
With carbon tetrabromide at 175℃; for 6h; Sealed tube; | A 39% B 2% C 55% D 5% |
With carbon tetrabromide at 175℃; for 6h; Reagent/catalyst; Temperature; Sealed tube; | A 39% B 4% C 52% D 5% |
With carbon tetrabromide at 175℃; for 6h; Concentration; Time; Sealed tube; | A 41% B 8% C 44% D 2% |
Conditions | Yield |
---|---|
With uranyl nitrate hydrate; water; trifluoroacetic acid In nitromethane for 60h; Irradiation; | 55% |
4-Phenylphenol
4-chloro-2,4,6-tri-tert-butylcyclohexa-2,5-dienone
A
2,4,6-tri-tert-butylphenoxol
Conditions | Yield |
---|---|
With α-picoline at 110℃; for 2h; 1b : 5i : α-picoline = 1 : 2 : 2; Further byproducts given; | A 52% B 7% |
4-Fluorophenol
4-chloro-2,4,6-tri-tert-butylcyclohexa-2,5-dienone
A
2,4,6-tri-tert-butylphenoxol
B
2,4,6-tri-tert-butyl-4-hydroxy-2,5-cyclohexadienone
Conditions | Yield |
---|---|
With α-picoline at 110℃; for 2h; 1b : 5e : α-picoline = 1 : 2 : 2; Further byproducts given; | A 18% B 3% C 51% |
4-bromo-phenol
4-chloro-2,4,6-tri-tert-butylcyclohexa-2,5-dienone
A
2,4,6-tri-tert-butylphenoxol
B
2,4,6-tri-tert-butyl-4-hydroxy-2,5-cyclohexadienone
C
2,4-di-tert-butyl-6-chlorophenol
D
2-(4-Bromo-phenoxy)-4,6-di-tert-butyl-phenol
Conditions | Yield |
---|---|
With α-picoline at 110℃; for 2h; 1b : 5h : α-picoline : 1 : 2 : 2; | A 29% B 8% C 13% D 51% |
2-methyl-but-2-ene
isobutene
phenol
A
para-tert-butylphenol
B
2-tert-Butylphenol
C
4-t-amylphenol
D
2,4-di-tert-Butylphenol
E
2,4,6-tri-tert-butylphenoxol
F
2,4-di-tert-amylphenol
G
2-t-butyl-4-(1,1-dimethylpropyl)-phenol
H
4-tert-butyl-2-(1,1-dimethyl-propyl)-phenol
Conditions | Yield |
---|---|
Stage #1: isobutene; phenol; Fulcat 22B catalyst at 130 - 140℃; for 1.5h; Inert atmosphere; Stage #2: 2-methyl-but-2-ene at 130℃; for 3.25h; | A 50.8% B 1.4% C 15.3% D 17.6% E 0.3% F 1.3% G 10.7% H 10.7% |
4-chloro-2,4,6-tri-tert-butylcyclohexa-2,5-dienone
A
2,4,6-tri-tert-butylphenoxol
B
2,4,6-tri-tert-butyl-4-hydroxy-2,5-cyclohexadienone
C
2,4-di-tert-butyl-6-chlorophenol
Conditions | Yield |
---|---|
With α-picoline; ortho-cresol at 110℃; for 2h; | A 50% B 1% C 7% D 6% |
4-chloro-2,4,6-tri-tert-butylcyclohexa-2,5-dienone
ortho-cresol
A
2,4,6-tri-tert-butylphenoxol
B
2,4,6-tri-tert-butyl-4-hydroxy-2,5-cyclohexadienone
C
2,4-di-tert-butyl-6-chlorophenol
Conditions | Yield |
---|---|
With α-picoline at 110℃; for 2h; 1b : 5b : α-picoline = 1 : 2 : 2; | A 50% B 1% C 7% D 6% |
NH-pyrazole
4-bromo-2,4,6-tri-tert-butyl-2,5-cyclohexadiene-1-one
A
2,4,6-tri-tert-butylphenoxol
B
2,6-Di-tert-butyl-4-pyrazol-1-yl-phenol
C
2,4-Di-tert-butyl-6-pyrazol-1-yl-phenol
D
2,4,6-Tri-tert-butyl-4-pyrazol-1-yl-cyclohexa-2,5-dienone
Conditions | Yield |
---|---|
at 110℃; for 24h; Further byproducts given; | A 49% B 21% C 21% D 2% |
2,4,6-tri-tert-butylphenoxol
2,4,6-tri-tert-butylphenoxyl
Conditions | Yield |
---|---|
With iodine; ethylenediamine; potassium iodide In methanol other base; | 100% |
With iodine; ethylenediamine; potassium iodide In methanol | 100% |
With 5,10,15-tris(pentafluorophenyl)corrole iron(IV) chloride; 3-chloro-benzenecarboperoxoic acid In acetonitrile at 25℃; Kinetics; Concentration; | 99.92% |
phosgene
2,4,6-tri-tert-butylphenoxol
2,4,6-tri(tert-butyl)phenyl carbonochloridate
Conditions | Yield |
---|---|
With n-butyllithium at 0℃; | 100% |
With n-butyllithium In 1,2-dimethoxyethane at 0℃; | 98% |
Stage #1: 2,4,6-tri-tert-butylphenoxol With sodium hydride In tetrahydrofuran Metallation; Stage #2: phosgene With N,N-dimethyl-aniline In toluene at 0 - 20℃; for 2.5h; Acylation; | 75% |
2,4,6-tri-tert-butylphenoxol
Conditions | Yield |
---|---|
With tert.-butylnitrite at 20℃; for 0.166667h; | 100% |
2,4,6-tri-tert-butylphenoxol
2,4,6-tri-tert-butyl phenoxyl radical
Conditions | Yield |
---|---|
With [Ru(III)(dmp-)(TPA)](2+) In acetonitrile at 19.84℃; Kinetics; Concentration; Reagent/catalyst; Time; | 100% |
With [MnII(2-[bis(pyridin-2-ylmethyl)]amino-N-quinolin-8-yl-acetamidate)(OMe)](1+) In acetonitrile at 50℃; Mechanism; Activation energy; Solvent; Inert atmosphere; | 75% |
Conditions | Yield |
---|---|
With sodium hydride In dimethylsulfoxide-d6 at 20℃; for 1h; | 99% |
Stage #1: 2,4,6-tri-tert-butylphenoxol With ethyl [2]alcohol; sodium for 10h; Stage #2: With water-d2 Further stages.; | 97% |
Stage #1: 2,4,6-tri-tert-butylphenoxol With sodium hydride In dimethylsulfoxide-d6 Stage #2: With water-d2 In dimethylsulfoxide-d6 Further stages.; | 90% |
Conditions | Yield |
---|---|
In diethyl ether at 20℃; | 99% |
2,4,6-tri-tert-butylphenoxol
trimethylaluminum
methylaluminum bis(2,4,6-tri-tert-butylphenoxide)
Conditions | Yield |
---|---|
In hexane (Ar); std. Schlenk technique; soln. of Me3Al in hexane was slowly added over 5 min to stirred soln. of phenol in hexane; soln. was stirred at 25°C for 1 h; evapd. in vac. overnight; | 98% |
In hexane; dichloromethane hexane soln. of AlMe3 added to CH2Cl2 soln. of organic compound at room temp.; stirred for 1 h at room temp.;; no further purifn.; used as CH2Cl2 soln.;; |
[(2,4,6-tri-tert-butylphenyl)NP][GaCl4]
2,4,6-tri-tert-butylphenoxol
Conditions | Yield |
---|---|
In dichloromethane absence of moisture; pptn. on slow addn. of 1 equiv. substituted phenol to Ga-complex (over 10 min); elem. anal.; | 98% |
Conditions | Yield |
---|---|
With copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; 4,4'-di-tert-butyl-2,2'-bipyridine In toluene at 20℃; for 20h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With perchloric acid; lead dioxide In water; acetone at 25℃; | 97% |
With (2,9-dimethyl-1,10-phenanthroline)Fe(II)(benzoylformate)2; oxygen In acetonitrile at 20℃; for 20h; Reagent/catalyst; | 90% |
With 1-chloro-2,2,6,6-tetramethylpiperidine In benzene for 20h; Heating; | 55% |
2,4,6-tri-tert-butylphenoxol
2,4,6-tri-tert-butyl-4-hydroperoxycyclohexa-2,5-dienone
Conditions | Yield |
---|---|
With oxygen; thiamine diphosphate In tetrachloromethane Irradiation; | 97% |
With 2,8-dibromo-5,5-difluoro-1,3,7,9-tetramethyl-10-phenyl-5H-dipyrrolo[1,2-c:2′,1′-f ][1,3,2]diazaborinin-4-ium-5-uide; oxygen In 1,4-dioxane for 6h; Irradiation; | 92% |
With oxygen In toluene Mechanism; Thermodynamic data; further solvents; ΔH(activ.), ΔS(activ.); | |
With potassium hydroxide; oxygen In ethanol |
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane at -78 - 20℃; for 2.5h; | 96% |
decamethylsamarocene(II) bis(tetrahydrofurane)
2,4,6-tri-tert-butylphenoxol
Conditions | Yield |
---|---|
In toluene Ar-atmosphere; stirring (room temp., 3 h); evapn., washing (toluene); elem. anal.; | 96% |
2,4,6-tri-tert-butylphenoxol
2,4,6-Tri-tert-butylcyclohexanon
Conditions | Yield |
---|---|
With hydrogen; nickel | 95% |
With nickel at 195 - 235℃; under 110326 Torr; Hydrogenation; |
2,4,6-tri-tert-butylphenoxol
acetic anhydride
2,4,6-tri-tert-butylphenyl acetate
Conditions | Yield |
---|---|
With silica gel-supported phosphotungstic acid In chloroform at 62℃; for 1h; | 95% |
With sulfuric acid at 35 - 40℃; | 36% |
2,4,6-tri-tert-butylphenoxol
acetic acid
4-Acetoxy-2,4,6-tri-tert-butylcyclohexa-2,5-dien-1-one
Conditions | Yield |
---|---|
With 3-(morpholin-4-yl)propyl modified polystyrene In acetonitrile Electrochemical reaction; | 95% |
With lead(IV) acetate |
2,4,6-tri-tert-butylphenoxol
[Mn(tris[(N'-tert-butylureaylato)-N-ethyl]aminato)(OH)](1-)
Conditions | Yield |
---|---|
In not given Mn-complex was reacted with ligand; | 95% |
methanol
2,4,6-tri-tert-butylphenoxol
2,4,6-tri-tert-butyl-4-methoxy-2,5-cyclohexadienone
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene In methanol at 20℃; for 0.666667h; | 94% |
With piperidine; silica gel Electrochemical reaction; | 91% |
With perchloric acid; lead dioxide for 0.133333h; | 90% |
oxalyl dichloride
2,4,6-tri-tert-butylphenoxol
(2,4,6-tri-tert-butylphenoxy)oxalyl chloride
Conditions | Yield |
---|---|
With n-butyllithium In diethyl ether; hexane at 0℃; for 0.5h; | 94% |
With n-butyllithium In hexane |
2,4,6-tri-tert-butylphenoxol
2,4,6-tri-tert-butyl-4-methoxy-2,5-cyclohexadienone
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene In methanol Ambient temperature; | 94% |
Multi-step reaction with 2 steps 1: 52 percent / Br2; KBr; pyridine / diethyl ether; H2O / 0.17 h / -20 °C 2: 94 percent / 25 °C View Scheme |
di-tert-butyl dicarbonate
2,4,6-tri-tert-butylphenoxol
Conditions | Yield |
---|---|
With dmap In dichloromethane at 20℃; | 94% |
Conditions | Yield |
---|---|
With cesium hydroxide; oxygen; triethyl phosphite In dimethyl sulfoxide at 25℃; under 760.051 Torr; for 12h; | 93% |
With C5CoN5O2(3-)*3C36H30NP2(1+); oxygen In N,N-dimethyl-formamide at 25℃; for 5h; | 90% |
With bis-[(trifluoroacetoxy)iodo]benzene In water; acetonitrile at 0℃; | 76% |
2,4,6-tri-tert-butylphenoxol
dimethylsilicon dichloride
(2,4,6-tri-tert-butylphenoxy)dimethylsilyl chloride
Conditions | Yield |
---|---|
With triethylamine In acetonitrile Heating; | 93% |
With triethylamine In acetonitrile Yield given; |
2,4,6-tri-tert-butylphenoxol
2,4,6-Trichlorophenol
4-(2',4',6'-trichlorophenoxy)2,4,6-tri-t-butyl-2,5-cyclohexadien-1-one
Conditions | Yield |
---|---|
With barium manganate In benzene for 1h; | 92% |
2,4,6-tri-tert-butylphenoxol
4-bromo-2,4,6-tri-tert-butyl-2,5-cyclohexadiene-1-one
Conditions | Yield |
---|---|
With N-Bromosuccinimide for 0.166667h; | 91% |
With [bis(acetoxy)iodo]benzene; lithium bromide In tetrahydrofuran at 20℃; for 0.5h; | 87% |
With pyridine; bromine; potassium bromide In diethyl ether; water at -20℃; for 0.166667h; | 52% |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In ethanol; water at 25℃; for 1h; Inert atmosphere; Darkness; stereoselective reaction; | 91% |
isocyanate de chlorosulfonyle
2,4,6-tri-tert-butylphenoxol
N-chlorosulfonylcarbamate de 2,4,6-tritertiobutylphenyle
Conditions | Yield |
---|---|
In diethyl ether -10 deg C then room temp., 30 min; | 90% |
2,4,6-tri-tert-butylphenoxol
4,6-di-tert-butyl-2-nitrosophenol
Conditions | Yield |
---|---|
With sulfuric acid; sodium nitrite at -10 - -5℃; for 0.25h; | 90% |
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