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Synthetic route

: bis(η3-allyl)nickel(II)

: 7783-55-3
trifluorophosphane

: 13859-65-9
tetrakis(trifluorophosphine)nickel

Conditions

Conditions	Yield
In neat (no solvent) 29% excess PF3 condensed onto Ni(allyl)2 and reagents allowed to react at 25°C for 1.5 h; react. mixt. fractionated, Ni(PF3)4 recovered in -80°C trap;	58%

: 13463-39-3, 71564-36-8
tetracarbonyl nickel

: 7783-55-3
trifluorophosphane

: 13859-65-9
tetrakis(trifluorophosphine)nickel

Conditions

Conditions	Yield
In neat (no solvent)
In neat (no solvent)
In neat (no solvent) High Pressure; react. of (Ni(CO)4) with PF3 at 150 °C under pressure;;
In neat (no solvent) High Pressure; react. of (Ni(CO)4) with PF3 at 150 °C under pressure;;
In melt passing PF3 into liq. (Ni(CO)4) for a longer period of time (carefully raising temp. to 71 °C);;	>99

: 13463-39-3, 71564-36-8
tetracarbonyl nickel

: 7783-55-3
trifluorophosphane

A: 13859-65-9
tetrakis(trifluorophosphine)nickel

B: 14219-40-0
NiCO(PF3)3

C: 14264-32-5
Ni(trifluorophosphine)(CO)3

D: 13859-78-4
Ni(CO)2(PF3)2

Conditions

Conditions	Yield
In neat (no solvent) at higher temp.;;
In neat (no solvent) at higher temp.;;
In neat (no solvent) at 0 - 71°C;;

...Expand

: 1271-28-9
nickelocene

: 13859-65-9
tetrakis(trifluorophosphine)nickel

Conditions

Conditions	Yield
With trifluorophosphane 100°C/30 at;
With trifluorophosphane 60°C/5 d; closed tube;
With PF3 100°C/30 at;
With PF3 60°C/5 d; closed tube;

: 7440-02-0
nickel

: 13859-65-9
tetrakis(trifluorophosphine)nickel

Conditions

Conditions	Yield
With PF3 In methyl cyclohexane absence of air and moisture; condensing Ni-vapour into methylcyclohexanecontg. excess of PF3 and cycloheptatriene (-130°C); IR and mass spectroscopy;

: 7440-02-0
nickel

: 7783-55-3
trifluorophosphane

: 13859-65-9
tetrakis(trifluorophosphine)nickel

Conditions

Conditions	Yield
In neat (no solvent) High Pressure; treating Ni-powder (prepd. by thermal decompn. of Ni-oxalate in N2- or H2-stream) in rotary autoclave (Cu-impeller) with PF3 (350 atm) for 42 h at 100 °C;; distilling off PF3 at -100 °C, further react. with PF3 for 16 h at 100 °C and 180 atm;;
In neat (no solvent) treating Ni (prepd. by decompn. of (Ni(CO)4)) at 100 °C for several weeks with PF3;;
In neat (no solvent) treating Ni (prepd. by decompn. of (Ni(CO)4)) at 100 °C for several weeks with PF3;;
In neat (no solvent) High Pressure; treating Ni-powder (prepd. by thermal decompn. of Ni-oxalate in N2- or H2-stream) in rotary autoclave (Cu-impeller) with PF3 (350 atm) for 42 h at 100 °C;; distilling off PF3 at -100 °C, further react. with PF3 for 16 h at 100 °C and 180 atm;;

: 14219-40-0
NiCO(PF3)3

: 7783-55-3
trifluorophosphane

: 13859-65-9
tetrakis(trifluorophosphine)nickel

Conditions

Conditions	Yield
In neat (no solvent) react. with PF3 above 70 °C;;

: 36421-86-0
tetrakis(phosphorustrichloride)nickel(0)

: 7783-55-3
trifluorophosphane

: 13859-65-9
tetrakis(trifluorophosphine)nickel

Conditions

Conditions	Yield
In neat (no solvent) byproducts: PCl3; heating (Ni(PCl3)4) with excess of PF3 in closed tube for 24 h on steam bath, cooling react. tube with liq. N2 after the react. is finished and distilling off PF3 at -115 °C (vac.), raising temp. to 0 °C;; sepg. upper layer of PCl3 from (Ni(PF3)4), fractional distillation in high vac. with addn. of SbF3 and traces of SbF5;;

: 36421-86-0
tetrakis(phosphorustrichloride)nickel(0)

: 7783-55-3
trifluorophosphane

A: 13859-65-9
tetrakis(trifluorophosphine)nickel

B: 7719-12-2, 52843-90-0
phosphorus trichloride

Conditions

Conditions	Yield
In neat (no solvent) react. at >100°C and 50-100 atm in a pressure pipe;;
In neat (no solvent) react. at >100°C and 50-100 atm in a pressure pipe;;

...Expand

: 15689-05-1
tetrakis(tribromophosphine)nickel(0)

: 7783-55-3
trifluorophosphane

: 13859-65-9
tetrakis(trifluorophosphine)nickel

Conditions

Conditions	Yield
In neat (no solvent) react. at >100°C and 50-100 atm in a pressure pipe;;
In neat (no solvent) react. at >100°C and 50-100 atm in a pressure pipe;;
In neat (no solvent) byproducts: PBr3; heating (Ni(PBr3)4) with excess of PF3 in closed tube for 24 h on steam bath, cooling react. tube with liq. N2 after the react. is finished and distilling off PF3 at -115 °C (vac.), raising temp. to 0 °C;; sepg. upper layer of PBr3 from (Ni(PF3)4), fractional distillation in high vac. with addn. of SbF3 and traces of SbF5;;

: 13463-39-3, 71564-36-8
tetracarbonyl nickel

: 7783-55-3
trifluorophosphane

A: 13859-65-9
tetrakis(trifluorophosphine)nickel

B: 14219-40-0
NiCO(PF3)3

Conditions

Conditions	Yield
In neat (no solvent) treating (Ni(CO)4) for 100 h with PF3 at 40 °C;;	A 0% B n/a

...Expand

: 1271-28-9
nickelocene

: 7783-55-3
trifluorophosphane

: 13859-65-9
tetrakis(trifluorophosphine)nickel

Conditions

Conditions	Yield
In neat (no solvent) heating Ni(C5H5)2 and PF3 for several days in closed tube to 65 °C;;
In neat (no solvent) heating Ni(C5H5)2 and PF3 for several days in closed tube to 65 °C;;

: nickel(II) iodide

: 7783-55-3
trifluorophosphane

: 13859-65-9
tetrakis(trifluorophosphine)nickel

Conditions

Conditions	Yield
With copper In neat (no solvent) High Pressure; react. of NiI2 and Cu-powder with PF3 (110 atm) at 100 °C for 24 h;; condensing excess PF3 and (Ni(PF3)4) into Schlenk-tube, evapg. PF3 at -100 °C, distilling (Ni(PF3)4);;
With Cu In neat (no solvent) High Pressure; react. of NiI2 and Cu-powder with PF3 (110 atm) at 100 °C for 24 h;; condensing excess PF3 and (Ni(PF3)4) into Schlenk-tube, evapg. PF3 at -100 °C, distilling (Ni(PF3)4);;

: 36421-86-0
tetrakis(phosphorustrichloride)nickel(0)

: 7783-56-4
antimony(III) fluoride

: 13859-65-9
tetrakis(trifluorophosphine)nickel

Conditions

Conditions	Yield
antimony pentafluoride In neat (no solvent) react. of (Ni(PCl3)4) with SBF3 in presence of catalytic amt. of SbF5;;
antimony pentafluoride In neat (no solvent) react. of (Ni(PCl3)4) with SBF3 in presence of catalytic amt. of SbF5;;

: 14219-40-0
NiCO(PF3)3

A: 13859-65-9
tetrakis(trifluorophosphine)nickel

B: 13463-39-3, 71564-36-8
tetracarbonyl nickel

Conditions

Conditions	Yield
In neat (no solvent)

: 14986-57-3
potassium fluorosulphinate

: 36421-86-0
tetrakis(phosphorustrichloride)nickel(0)

: 13859-65-9
tetrakis(trifluorophosphine)nickel

Conditions

Conditions	Yield
In further solvent(s) byproducts: SO2; react. of KSO2F with (Ni(PCl3)4) under exclusion of air and moisture in m-dichlorobenzene (cooling with ice), stirring for 30 min at ambient temp. and for 2 h at 90 °C;; collecting volatile react. products in cooled U-tube (filled with KSO2F), distilling into second U-tube after evapn. of SO2, distillation of (Ni(PF3)4) in micro-column at 760 torr under N2;;
In further solvent(s) byproducts: SO2; react. of KSO2F with (Ni(PCl3)4) under exclusion of air and moisture in m-dichlorobenzene (cooling with ice), stirring for 30 min at ambient temp. and for 2 h at 90 °C;; collecting volatile react. products in cooled U-tube (filled with KSO2F), distilling into second U-tube after evapn. of SO2, distillation of (Ni(PF3)4) in micro-column at 760 torr under N2;;

Yield

In further solvent(s) byproducts: SO2; react. of KSO2F with (Ni(PCl3)4) under exclusion of air and moisture in m-dichlorobenzene (cooling with ice), stirring for 30 min at ambient temp. and for 2 h at 90 °C;; collecting volatile react. products in cooled U-tube (filled with KSO2F), distilling into second U-tube after evapn. of SO2, distillation of (Ni(PF3)4) in micro-column at 760 torr under N2;;

: 14264-32-5
Ni(trifluorophosphine)(CO)3

A: 13859-65-9
tetrakis(trifluorophosphine)nickel

B: 13463-39-3, 71564-36-8
tetracarbonyl nickel

Conditions

Conditions	Yield
In neat (no solvent)

: 13859-78-4
Ni(CO)2(PF3)2

A: 13859-65-9
tetrakis(trifluorophosphine)nickel

B: 13463-39-3, 71564-36-8
tetracarbonyl nickel

Conditions

Conditions	Yield
In neat (no solvent)

: 15024-22-3
Ni(PF2Cl)4

: 13859-65-9
tetrakis(trifluorophosphine)nickel

Conditions

Conditions	Yield
With L-Selectride In not given under inert atmosphere, other unidentified products;

: 13859-65-9
tetrakis(trifluorophosphine)nickel

: ammonium hydroxide

: 1313-99-1
nickel(II) oxide

Conditions

Conditions	Yield
With Dimethylglyoxime; nitric acid In ethanol; ammonia; water byproducts: NH4F; addn. of aq. NH4OH to Ni(PF3)4, cooling with liquid nitrogen, mixing for 15 min, addn. of HNO3, adjusting pH to 7-8 by addn. of NH4OH, heating to 80°C, pptg. by addn. of alcoholicammoniacal soln. of dimethylglyoxime; filtn., heating at 850°C;	92%

: 13859-65-9
tetrakis(trifluorophosphine)nickel

: 100-59-4
phenylmagnesium chloride

: 79268-50-1
(difluorophenylphosphane)tris(trifluorophosphane)nickel(0)

Conditions

Conditions	Yield
In diethyl ether byproducts: MgClF; ratio 1:1; 6 h, room temp., under N2; solvent evapd. in vac., the residue extracted with pentane, evapd. in vac.,;	68.4%

: 109-72-8, 29786-93-4
n-butyllithium

: 13859-65-9
tetrakis(trifluorophosphine)nickel

: 79268-37-4
(butyldifluorophosphane)tris(trifluorophosphane)nickel(0)

Conditions

Conditions	Yield
In diethyl ether byproducts: LiF; ratio 1:1; 6 h, room temp., under N2; solvent evapd. in vac., residue extracted with pentane, evapd. in vac.;	64%

: 13859-65-9
tetrakis(trifluorophosphine)nickel

: 931-51-1
cyclohexylmagnesiumchloride

: 79268-51-2
(cyclohexyldifluorophosphane)tris(trifluorophosphane)nickel(0)

Conditions

Conditions	Yield
In diethyl ether byproducts: MgClF; ratio 1:1; 6 h, room temp., under N2; solvent evapd. in vac., residue extracted with pentane, evapd. in vac.;	63.6%

: 931-53-3
Cyclohexyl isocyanide

: 13859-65-9
tetrakis(trifluorophosphine)nickel

A: cyclo-C6H11NCNi(PF3)3

B: (cyclo-C6H11NC)2Ni(PF3)2

Conditions

Conditions	Yield
In hexane byproducts: (cyclo-C6H11NC)(n); prepn. in n-hexane at 40-50°C;;	A 31.7% B n/a
In hexane byproducts: (cyclo-C6H11NC)(n); prepn. in n-hexane at 40-50°C;;	A 31.7% B n/a
In hexane byproducts: (CNC6H11-cyclo)(n); prepn. from Ni(PF3)4 and cyclo-C6H11NC in n-hexane at 40-50 °C;; main product is cyclo-C6H11NCNi(PF3)3;;
In hexane byproducts: (CNC6H11-cyclo)(n); prepn. from Ni(PF3)4 and cyclo-C6H11NC in n-hexane at 40-50 °C;; main product is cyclo-C6H11NCNi(PF3)3;;

...Expand

: 13859-65-9
tetrakis(trifluorophosphine)nickel

: 201230-82-2
carbon monoxide

: 13463-39-3, 71564-36-8
tetracarbonyl nickel

Conditions

Conditions	Yield
In neat (no solvent) High Pressure; prepn. from Ni(PF3)4 and CO at high pressure;;
In neat (no solvent) High Pressure; prepn. from Ni(PF3)4 and CO at high pressure;;

: 13859-65-9
tetrakis(trifluorophosphine)nickel

: 7553-56-2
iodine

: nickel(II) iodide

Conditions

Conditions	Yield
react. with I2;;

: 13859-65-9
tetrakis(trifluorophosphine)nickel

: 7726-95-6
bromine

: nickel dibromide

Conditions

Conditions	Yield
byproducts: PF3Br2; react. with Br2;;

: 13859-65-9
tetrakis(trifluorophosphine)nickel

: 115512-35-1
NiPF3(1+)

Conditions

Conditions	Yield
In gas electron impact; MS;

: 13859-65-9
tetrakis(trifluorophosphine)nickel

: 7440-02-0
nickel

Conditions

Conditions	Yield
In neat (no solvent) decompn. at elevated temp.;;

: 13859-65-9
tetrakis(trifluorophosphine)nickel

: 13463-39-3, 71564-36-8
tetracarbonyl nickel

Conditions

Conditions	Yield
With carbon monoxide In neat (no solvent) High Pressure; react. with CO at 100 °C and 350 atm;;
With CO In neat (no solvent) High Pressure; react. with CO at 100 °C and 350 atm;;

: 13859-65-9
tetrakis(trifluorophosphine)nickel

: nickel(II) sulphate

Conditions

Conditions	Yield
With H2SO4 In sulfuric acid aq. H2SO4; react. with concd. H2SO4 at elevated temp.;;

: 101-02-0
triphenyl phosphite

: 13859-65-9
tetrakis(trifluorophosphine)nickel

: 17112-33-3
Ni(P(OC6H5)3)3PF3

Conditions

Conditions	Yield
In benzene heating (Ni(PF3)4) and P(OC6H5)3 (molar ratio 1:4) for 10 h in boiling benzene, evapg. solvent and excess P(OC6H5)3 in vac.;; digesting residue with methanol, recrystn. from methanol;;
In benzene heating (Ni(PF3)4) and P(OC6H5)3 (molar ratio 1:4) for 10 h in boiling benzene, evapg. solvent and excess P(OC6H5)3 in vac.;; digesting residue with methanol, recrystn. from methanol;;

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2,7-Naphthalenedisulfonicacid, 3,6-bis[2-(2-arsonophenyl)diazenyl]-4,5-dihydroxy-, sodium salt (1:?)

13862-16-3

Silanamine,N,N-disilyl-

13863-31-5

Benzenesulfonic acid,2,2'-(1,2-ethenediyl)bis[5-[[4-[(2-hydroxyethyl)methylamino]-6-(phenylamino)-1,3,5-triazin-2-yl]amino]-,sodium salt (1:2)

13864-01-2

Lanthanum hydride(LaH3)

13864-02-3

Ceriumhydride (CeH3)

13864-03-4

Praseodymium hydride(PrH3)

13864-04-5

Neodymium hydride(NdH3)

138642-47-4

Benzonitrile,2-bromo-5-methoxy-

138642-62-3

2-Cyanophenylboronic acid

Downstream Products

7440-02-0

Risk Statements	11-23/24/25
Safety Statements	16-36/37/39

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