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inquiryNickelous oxide Basic information Product Name: Nickelous oxide Synonyms: NICKEL(II) OXIDE;NICKEL(II) OXIDE, BLACK;NICKEL (II) OXIDE (GREEN);NICKEL MONOXIDE;NICKELO
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inquiryMolecular formula : NiO The molecular weight: Traits: Green powder Use: Mainly used in magnetic materials, electronic components materials, enamel, ceramic coating, gray glass materials, nickel salt, nickel catalyst materials Packing: in 25
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inquiryNickel Oxide CAS: 1313-99-1 Specification NiO % min 76.5 78 Co % max 0.15 0.03 Cu % max 0.05 0.01 Fe % max
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Product Name: Nickel(II) oxide CAS: 1313-99-1 MF: NiO MW: 74.69 EINECS: 215-215-7 Mol File: 1313-99-1.mol Nickel(II) oxide Structure Nickel(II) oxide Chemical Properties Melting point 1960 °C density 6.67 g/mL at 25 &d
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Conditions | Yield |
---|---|
In melt Kinetics; byproducts: KCl, NO2, O2; mixt. of K salt/Ni salt (8/1) heated up to 500°C with a rate of 150°C/h, cooled in furnace; washed with H2O, insol. residue filtered off; elem. anal.; | 100% |
Conditions | Yield |
---|---|
In melt Kinetics; byproducts: LiCl, NO2, O2; mixt. of Li salt/Ni salt (8/1) heated up to 500°C with a rate of 150°C/h, cooled in furnace; washed with H2O, insol. residue filtered off; elem. anal.; | 100% |
Conditions | Yield |
---|---|
In melt Kinetics; byproducts: NaCl, NO2, O2; mixt. of Na salt/Ni salt (8/1) heated up to 500°C with a rate of 150°C/h, cooled in furnace; washed with H2O, insol. residue filtered off; elem. anal.; | 100% |
Conditions | Yield |
---|---|
In melt Kinetics; byproducts: KNO3, NO2, O2; mixt. of K salt/Ni salt (8/1) heated up to 500°C with a rate of 150°C/h, cooled in furnace; washed with H2O, insol. residue filtered off; elem. anal.; | 100% |
Conditions | Yield |
---|---|
In melt Kinetics; byproducts: LiNO3, NO2, O2; mixt. of Li salt/Ni salt (8/1) heated up to 500°C with a rate of 150°C/h, cooled in furnace; washed with H2O, insol. residue filtered off; elem. anal.; | 100% |
Conditions | Yield |
---|---|
In melt Kinetics; byproducts: NaNO3, NO2, O2; mixt. of Na salt/Ni salt (8/1) heated up to 500°C with a rate of 150°C/h, cooled in furnace; washed with H2O, insol. residue filtered off; elem. anal.; | 100% |
1-(2-mercaptoethyl)-3,5-dimethylpyrazole
A
nickel(II) oxide
B
[NiCl3(NC(CH3)CHC(CH3)NCH2CH2SSCH2CH2NC(CH3)CHC(CH3)NH)]
Conditions | Yield |
---|---|
With triethyl orthoformate; O2 In acetonitrile vac. line and Schlenk technique; soln. of Ni compd. in CH3CN was added dropwise to soln. of ligand and triethyl orthoformate in CH3CN; soln. waskept in presence of O2 for 3 d; filtered; solvent evapd.; elem. anal.; | A n/a B 96% |
Conditions | Yield |
---|---|
With Dimethylglyoxime; nitric acid In ethanol; ammonia; water byproducts: NH4F; addn. of aq. NH4OH to Ni(PF3)4, cooling with liquid nitrogen, mixing for 15 min, addn. of HNO3, adjusting pH to 7-8 by addn. of NH4OH, heating to 80°C, pptg. by addn. of alcoholicammoniacal soln. of dimethylglyoxime; filtn., heating at 850°C; | 92% |
Conditions | Yield |
---|---|
In solid byproducts: LiCl; under N2; Li2O and metal halide ground together, added to glass ampoule, sealed under vacuum, sonicated (ultrasound) for 10 min, wrapped in glss wool, placed in oven at 450°C for 10 h; removed from oven, allowed to cool to room temp., trituration with THF for 10 h, ppt. and cloudy THF layer formed, evapn.of THF filtrate produced Li salt; or metal oxides washed with H2O for 10 min to remove Li salt; | 75% |
In neat (no solvent, solid phase) byproducts: LiCl; |
Conditions | Yield |
---|---|
Stage #1: nickel(II) sulfate hexahydrate With ethanol; sodium hydroxide In water Stage #2: With sodium carbonate In water at 80℃; for 24h; Stage #3: air at 450℃; for 2h; Calcination; | 46.9% |
nickel(II) oxide
Conditions | Yield |
---|---|
Stage #1: C7H3NO4(2-)*Ni(2+)*2H2O*C10H14N4 at 115 - 198℃; Stage #2: at 325 - 490℃; Pyrolysis; | 24.2% |
A
nickel(II) oxide
Conditions | Yield |
---|---|
In neat (no solvent) stoich. amts. reactants mixed, fired (890°C, N2 or O2/N2); X-ray diffraction; | A 20% B n/a |
nickel(II) oxide
Conditions | Yield |
---|---|
Stage #1: [Ni(homophthalate)(N,N-dimethylethylenediamine)2(H2O)]·H2O at 32 - 150℃; Stage #2: at 150 - 326℃; Stage #3: at 312 - 435℃; | 16% |
Stage #1: [Ni(homophthalate)(N,N-dimethylethylenediamine)2(H2O)]·H2O at 32 - 150℃; Stage #2: at 150 - 326℃; Stage #3: at 312 - 435℃; |
nickel(II) oxide
Conditions | Yield |
---|---|
Stage #1: [Ni(3,14-diethyl-2,6,13,17-tetraazatricyclo[14,4,01.18,07.12]docosane)(NCS)2] at 284 - 573℃; Inert atmosphere; Stage #2: at 573℃; Inert atmosphere; | 15.1% |
nickel(II) oxide
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) byproducts: ethane, H2O, CO; TG, heating in the range of 20-600 °C; at 172.91 loss of ethane and water of hydration; at 357.15 °C loss of CH2COOH, H2N, N2NCHCONH, and C6H4OH; at 458.53 °C loss of CO, C3S, and H2O; | 15% |
nickel(II) oxide
Conditions | Yield |
---|---|
Stage #1: [Ni(3,14-diethyl-2,6,13,17-tetraazatricyclo[14,4,01.18,07.12]docosane)(cyclopropanedicarboxylic acid)2] at 236 - 523℃; Inert atmosphere; Stage #2: at 523℃; Inert atmosphere; | 10.5% |
nickel(II) oxide
Conditions | Yield |
---|---|
Stage #1: [Ni(diclofenac)2(2-pyridineethanol)2] at 30 - 261℃; Stage #2: at 261 - 436℃; | 8.51% |
lithium acetate dihydrate
nickel(II) acetate tetrahydrate
A
nickel(II) oxide
C
lithium carbonate
Conditions | Yield |
---|---|
In water mixt. stirred, heated at 120 °C to remove water, heated at 250 °C for 24 h or at 370 °C for 24 h; detd. by XRD; |
nickel(II) oxide
Conditions | Yield |
---|---|
In neat (no solvent) decomposition at 300 - 350°C;; | |
In neat (no solvent) decomposition at 300 - 350°C;; | |
In neat (no solvent, solid phase) Ni compd. was calcined at 800°C; |
Conditions | Yield |
---|---|
In solid byproducts: aluminium nickel alloy; ball milling of a mixt of Al and nickel salt in air; X-ray diffraction; |
nickel(II) oxide
Conditions | Yield |
---|---|
In solid heating in air (500°C); elem. anal., X-ray diffraction; |
nickel(II) oxide
Conditions | Yield |
---|---|
In solid heating in air (500°C); elem. anal., X-ray diffraction; |
nickel(II) oxide
Conditions | Yield |
---|---|
Kinetics; byproducts: HCl, H2O; other Radiation; laser irradiation; distributed as a thin layer in a metal reaction cell; detected by X-ray; | |
In water prepd. onto heated substrate kept at 350°C by spray pyrolysis technique; soln. concn. was 0.05-0.30 M; flow rate was 15 cm**3/min; deposition time was 40 s; nozzle to substrate distance was 40 cm; | |
In neat (no solvent) decompn. upon heating at red heat;; |
Conditions | Yield |
---|---|
With air; polyvinylpyrrolidone In water NiCl2*6H2O dissolved in H2O in the presence of polyvinylpyrrolidone at room temp., NaOH added under stirring, filtered, washed (H2O), dried in air, annealed in air at 573 K for 2,5 h; detd. by XRD; |
Conditions | Yield |
---|---|
With resorcinol; formaldehyde; hydrochloric acid In water byproducts: CO2; pH 1 (HCl); mixt. dried in oven at 85°C for 24 h; calcined at 700°C for 2 h under flowing Ar; heated at 700°C, maintained for 2 h under oxygen atm.; | |
With air In neat (no solvent, solid phase) Ni-contg. compd. was ground and calcined at 400°C for 2.5 h in static air; cooling to room temp.; the powder was dispersed in distd. water and stirred at 80°C for 1 h; the compd. was recovered by filtration and dried under ambient conditions; detd. by powder XRD; |
nickel(II) oxide
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: H2O; heated at 250-350°C; XRD; TEM; |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: H2, H2O, CO; static air atmosphere; heating up to 1273 K (heating rate 1 - 10 K/min); reaction followed by X-ray diffraction; | |
With poly(vinyl alcohol) In water aq. PVA soln. (10 wt. %) was dropped into Ni-salt soln., heating up to 50 °C for 5 h, drying at 70 .degre.C for 12 h in vac., calcined at700 °C for 120 h (240 °C/h rate); removal of org. compds. were not completed at lower temp.; | |
With hexamethylenetetramine In water heated at 100°C for 300 min in an autoclave, quenched in air at room temp., heated in air at 350-450°C for 30 min; obtained as a film; |
Conditions | Yield |
---|---|
In neat (no solvent) heating at a temp. range 230 and 350°C in N2;; | |
In neat (no solvent) heating at a temp. range 230 and 350°C in N2;; |
Conditions | Yield |
---|---|
In neat (no solvent) decomp. in air at 600 °C for 2 h; detected by XRD; |
Conditions | Yield |
---|---|
With citric acid monohydrate; air or O2 In water byproducts: CO2, H2O; La2O3/C3H4(OH)(COOH)3*H2O (1:(30-50) w/w, a few H2O droplets) heating to420-450 K (stirring), Ni-compd./H2O addn., soln. dehydration at 450 K, incineration at 620-720 K, crushing, pelletizing, firing in air or O2 at 1300 K for 24 H; XRD; |
Conditions | Yield |
---|---|
With NH4Cl In water High Pressure; heating (sealed silica tube, 375°C, 3-5 d); | 99% |
In neat (no solvent) byproducts: NiTe2O5; NiO and TeO2 were heated in a stream of N2 at 550-800 °C;; polluted with NiTe2O5:; | |
In neat (no solvent) NiO and TeO2 were heated in a stream of N2 at 550-800 °C, molten at 900°C for 20 min in goldplate covers;; pure;; |
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) heating 3:2:1 mixt. of nickel oxide, molybdenum trioxide and selenum dioxide in vac. at 710°C for 6 d; IR; | 99% |
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) mixt. of MoO3, NiO and TeO2 ground; pressed into pellet; sealed in evacuated quartz tube; heated at 720°C for 6 d; cooled to 270°C(4.5°C/h); crystals isolated; elem. anal.; | 99% |
Conditions | Yield |
---|---|
With sulfur In neat (no solvent) passing S vapor over, for 2 h at 600°C, N2 as carrier gas;; | A 5% B 90% |
With sulfur byproducts: SO2; heating at 400-800°C; ratio of products depends on the temp. of reaction; influence of reaction time is given; | |
With S byproducts: SO2; heating at 400-800°C; ratio of products depends on the temp. of reaction; influence of reaction time is given; | |
With SO2 In neat (no solvent) equilibrium, investigation of SO2-absorption with NiO-NiS-mixtures;; |
nickel(II) oxide
Conditions | Yield |
---|---|
With sulfur In neat (no solvent) S vapor, at 500°C in 2 h, at 800°C in 35 min;; | 90% |
With S In neat (no solvent) S vapor, at 500°C in 2 h, at 800°C in 35 min;; | 90% |
With hydrogen sulfide In neat (no solvent) at 600°C; NiO prepared of NiCO3 in O2 atmosphere at 650°C;; | >99 |
nickel(II) oxide
Conditions | Yield |
---|---|
With αAl2O3 In neat (no solvent) equimolar amounts of NiO and αAl2O3, at 1200°C after 20 min;; | 90% |
With γAl2O3 In neat (no solvent) reaction starts at 800°C; complete after calcination at 900°C within 15 h in air;; | >99 |
With αAl2O3 In neat (no solvent) equimolar amounts of NiO and αAl2O3, at 1200°C after 1h; slower reaction with calcinated NiO, excess of Al2O3, addition ofGa2O3 and Li2O;; | >99 |
2-pyrazylcarboxylic acid
nickel(II) oxide
water
silver(l) oxide
Conditions | Yield |
---|---|
In water High Pressure; hydrothermal react.; loading Ag2O, Re2O7, pyrazinecarboxylate, NiO, and destillated H2O inside teflon pouch, sealed, placed in vessel, heated toand kept at 140°C for 36 h; cooled to room temp. over 24 h; | 90% |
nickel(II) oxide
Conditions | Yield |
---|---|
With chlorine In neat (no solvent) at 600°C, 2 h;; | 87% |
With Cl2 In neat (no solvent) at 600°C, 2 h;; | 87% |
With chlorine In neat (no solvent) in a stream of Cl2, at 700°C; reaction starts at 200°C, acceleration by addition of C;; | >99 |
Conditions | Yield |
---|---|
With hydrogen In neat (no solvent) Kinetics; 1000 h, NiO calcinated at 1000°C;; | 85% |
With H2 In neat (no solvent) Kinetics; 1000 h, NiO calcinated at 1000°C;; | 85% |
With hydrogen In neat (no solvent) Kinetics; 180°C, 70 h, NiO prepared be H2O elimination of Ni(OH)2 in vacuum;; | >99 |
Conditions | Yield |
---|---|
Kinetics; 1 h, 1200°C; | 83% |
Kinetics; 1 h, 900°C; | 23% |
Kinetics; 1300°C, 10 min.; | >99 |
nickel(II) oxide
hydrogen fluoride
water
Ni(H2O)6(2+)*VOF4(H2O)(2-)=[Ni(H2O)6][VOF4(H2O)]
Conditions | Yield |
---|---|
In hydrogen fluoride aq. HF; High Pressure; aq. HF added to mixt. of nickel oxide and vanadium oxide, water added, mixt. heated at 75-200°C for 24 h; different relative amounts of compds. used; Parr bomb cooled to 25°C at 0.1°C/min, stored for 48 h, crystals filtered off in air; | A n/a B 83% |
nickel(II) oxide
Conditions | Yield |
---|---|
With molybdenum(VI) oxide In neat (no solvent) Kinetics; at 500°C for 48 h, strating at 400°C;; | 80% |
With molybdenum(VI) oxide In neat (no solvent) depending on excess of O in NiO and temperature of preparation of NiO from Ni(OH)2;; | |
With molybdenum(VI) oxide In neat (no solvent) at 400 - 900°C acceleration by addition of Li2O, deceleration by addition of Cr2O3;; | |
With MoO3 In neat (no solvent) depending on boiling point of adsorbed gases;; | |
With MoO3 |
piperazine
nickel(II) oxide
sulfuric acid
hydrogen fluoride
water
Conditions | Yield |
---|---|
In water; ethylene glycol High Pressure; NiO was dissolved in ethylene glycol-water mixt., H2SO4 and HF were added, piperazine was added and stirred for 1 h, react. mixt. was transferred into Teflon-lined acid digestion bomb and heated at 180°C for 3days under autogenous pressure; | 80% |
nickel(II) oxide
trifluoroacetic acid
nickel(II) (tetraaqua)bis(O-trifluoroacetate)
Conditions | Yield |
---|---|
In neat (no solvent) High Pressure; mixt. heated in high pressure reactor at 150°C for 1 d; cooled; crystals were obtained from mother liquor after a few ds; elem. anal.; | 80% |
Conditions | Yield |
---|---|
at 550℃; for 72h; Sealed tube; | 76.04% |
Conditions | Yield |
---|---|
In water High Pressure; in an autoclave, at 160°C for 72 h, then at 165°C for 48 h; cooled over 10 h to room temp., filtered, washed, dried at 40°C; | 70% |
nickel(II) oxide
3,3’,5,5’-tetracarboxydiphenylmethane
water
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide High Pressure; mixt. of NiO, acid, DMF and H2O was heated in reactor at 105°C for 3 d; cooled to room temp. at rate 10°C/h; elem. anal.; | 69% |
nickel(II) oxide
piperazinium sulfate monohydrate
hydrogen fluoride
water
Conditions | Yield |
---|---|
In ethanol; water High Pressure; NiO was dispersed in EtOH-H2O mixt., piperazine sulfate and HF were added and stirred for 1 h, react. mixt. was transferred into Teflon-lined acid digestion bomb and heated at 180°C for 48 h under autogenous pressure; | 65% |
Conditions | Yield |
---|---|
In water at 180℃; Autoclave; | 55% |
Conditions | Yield |
---|---|
In water for 24h; Reflux; | 54.6% |
nickel(II) oxide
1,10-Phenanthroline
1-amino-ethane-1,1-diphosphonic acid
water
Conditions | Yield |
---|---|
In water NiO, phenathroline, CH3C(PO(OH)2)2NH2 and H2O mixed; sealed; heated at 80°C for several d; elem. anal.; | 50.6% |
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