This product can be produced in large scale in our factory 1, Good appearance :colorless liquid 2, High purity,99%; 3, Related compound: Impurity Piperazine <0.1%; Appearance:colorless to light yellow liquid Storage:2-8 ℃ Application:key chemi
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
DayangChem exported this product to many countries and regions at best price in China. If you are looking for the product’s supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product specifica
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryProduct Name: 1-Acetylpiperazine Synonyms: N-ACETYLPIPERAZINE;AKOS BB-5737;1-ACETYLPIPERAZINE;1-PIPERAZIN-1-YL-ETHANONE;acetylpiperazine;N-Acetylpiperazine97%;N-Acetylpiperazine,99%;n-acetyl p
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiry★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support ★.Shortest delivery time . Appearance:Refer to COA Storage:Store in dry, cool and ventilated place Package:Acc
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:13889-98-0
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inquiry1-Acetylpiperazine CAS:13889-98-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inter
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiry1. Customs clearance 1) By Express: Normally there is no specical need for the recipient to clear the customs. If the customs has an objection,our rich experienced and professional group will help you clear the customs. 2) By Air and by Sea: Our
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:13889-98-0
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providing h
Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
Product Name: 1-Acetylpiperazine CAS: 13889-98-0 MF: C6H12N2O MW: 128.17 EINECS: 237-659-0 Mol File: 13889-98-0.mol 1-Acetylpiperazine Structure 1-Acetylpiperazine Chemical Properties Melting point 31-34 °C (lit.) Boiling
Cas:13889-98-0
Min.Order:1 Gram
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:13889-98-0
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inquiryWe Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiryN-acetylpiperidine
Conditions | Yield |
---|---|
With hydrogenchloride In ethyl acetate | 100% |
With trifluoroacetic acid In dichloromethane at 25℃; for 0.5h; | 88.8% |
Acidic conditions; |
piperazine
1-acetyl-2,3,4,6,7,8-hexahydropyrrolo[1,2-a]pyrimidinium tetraphenylborate
N-acetylpiperidine
Conditions | Yield |
---|---|
In acetonitrile at 80℃; for 1h; Inert atmosphere; | 99% |
piperazine
1,3-diacetyl-5-methyl-2-oxo-2,3-dihydro-1H-imidazole-4-carboxylic acid ethyl ester
N-acetylpiperidine
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1.3h; | 94% |
piperazine
1,3-diacetyl-1,3-dihydro-benzoimidazol-2-one
N-acetylpiperidine
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 0.333333h; | 93% |
Conditions | Yield |
---|---|
With acetic acid at 60℃; for 0.0666667h; Sonication; Irradiation; | 90% |
With water; sodium acetate |
piperazine
1,3-diacetyl-4,5-dimethylimidazolin-2(1H)-one
N-acetylpiperidine
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 2.5h; | 88% |
piperazine
1,3-diacetyl-2,3-dihydro-1H-imidazol-2-one
N-acetylpiperidine
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 2.5h; | 85% |
Conditions | Yield |
---|---|
With pyridine; aluminum oxide at 77 - 80℃; for 0.5h; microwave irradiation; | 75% |
In dichloromethane at 0℃; for 5h; | 20% |
With acetic acid |
N-Acetylimidazole
piperazine dihydrochloride
A
N-acetylpiperidine
B
1,4-diacetylpiperazine
Conditions | Yield |
---|---|
In ethanol; water at 20℃; for 6.16667h; | A 70% B n/a |
Conditions | Yield |
---|---|
In water at 55℃; for 24h; | 69% |
With acetonitrile |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water at 55 - 60℃; | 35% |
N,N-bis-cyanomethyl-acetamide
N-acetylpiperidine
Conditions | Yield |
---|---|
With ethanol; nickel Hydrogenation; |
piperazine
S-phenyl thioacetate
A
N-acetylpiperidine
B
thiophenol
Conditions | Yield |
---|---|
In water at 15 - 45℃; Rate constant; Thermodynamic data; Mechanism; ionic strength 0.2 M and 0.6 M (KCl), ΔH(excit.), ΔS(excit.), structure-reactivity correlations in the aminolysis; |
piperazine
1-acetylsulfanyl-4-nitro-benzene
A
N-acetylpiperidine
B
para-nitrobenzenethiol
Conditions | Yield |
---|---|
In water at 25℃; Rate constant; Mechanism; ionic strength 0.2 M (KCl), structure-reactivity correlations in the aminolysis; |
piperazine
2,4-dinitrophenyl acetate
A
N-acetylpiperidine
B
2,4-Dinitrophenol
Conditions | Yield |
---|---|
In water at 25℃; Rate constant; Mechanism; |
piperazinium
S-phenyl thioacetate
A
N-acetylpiperidine
B
thiophenol
Conditions | Yield |
---|---|
In water at 25℃; Rate constant; Mechanism; ionic strength 0.6 M and 0.8 M (KCl), pH 6.0; other pH, structure-reactivity correlations in the aminolysis; |
piperazinium
1-acetylsulfanyl-4-nitro-benzene
A
N-acetylpiperidine
B
para-nitrobenzenethiol
Conditions | Yield |
---|---|
In water at 25℃; Rate constant; Mechanism; ionic strength 0.2 M (KCl), structure-reactivity correlations in the aminolysis; |
1-(4-benzylpiperazin-1-yl)ethan-1-one
N-acetylpiperidine
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In methanol at 20℃; |
piperazine
4-nitrophenol acetate
A
N-acetylpiperidine
B
4-nitro-phenol
Conditions | Yield |
---|---|
With sodium bis(2-ethylhexyl)-sulfosuccinate In 2,2,4-trimethylpentane at 25℃; Kinetics; Further Variations:; Solvents; |
piperazine
acetic acid
A
N-acetylpiperidine
B
1,4-diacetylpiperazine
Conditions | Yield |
---|---|
at 130℃; for 1h; microwave irradiation; | A 57 % Chromat. B 43 % Chromat. |
at 200℃; for 1h; microwave irradiation; | A 27 % Chromat. B 73 % Chromat. |
piperazine
N-Acetylimidazole
piperazine dihydrochloride
A
N-acetylpiperidine
B
1,4-diacetylpiperazine
Conditions | Yield |
---|---|
Stage #1: piperazine; piperazine dihydrochloride In water for 0.0833333h; Stage #2: N-Acetylimidazole With sodium chloride In water for 0.5h; Stage #3: With sodium hydroxide In water chemoselective reaction; |
Conditions | Yield |
---|---|
In ethanol; water at 25℃; pH=5.07; Kinetics; Mechanism; Concentration; pH-value; |
Conditions | Yield |
---|---|
In ethanol; water at 25℃; pH=9.56; Kinetics; Mechanism; Concentration; pH-value; Solvent; |
Conditions | Yield |
---|---|
In ethanol; water at 25℃; pH=6.2; Kinetics; Mechanism; Concentration; pH-value; Solvent; aq. phosphate buffer; |
N-acetylpiperidine
Conditions | Yield |
---|---|
With TEA In N,N-dimethyl-formamide at 23℃; for 24h; | 100% |
3-[2-(pyridin-2-ylamino)-thiazol-5-ylsulfanyl]-benzoic acid
N-acetylpiperidine
Conditions | Yield |
---|---|
With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In tetrahydrofuran | 100% |
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; |
6-(2-hydroxyethyl)-2-(methylthio)-4-pyrimidinyl 4-methyl-1-benzenesulfonate
N-acetylpiperidine
Conditions | Yield |
---|---|
In tetrahydrofuran at 70℃; for 48h; | 100% |
N-acetylpiperidine
3-(Chloromethyl)benzoyl chloride
4-Acetyl-1-(3-chloromethyl)benzoylpiperazine
Conditions | Yield |
---|---|
In dichloromethane | 100% |
N-acetylpiperidine
C11H10N2O2S2
1-{4-[5-(2-amino-thiazol-5-ylsulfanyl)-2-methyl-benzoyl]-piperazin-1-yl}-ethanone
Conditions | Yield |
---|---|
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide | 100% |
N-acetylpiperidine
Conditions | Yield |
---|---|
100% |
Conditions | Yield |
---|---|
In benzene at 90℃; | 100% |
N-acetylpiperidine
(S)-Propylene oxide
(2S)-1-(4-acetylpiperazin-1-yl)propan-2-ol
Conditions | Yield |
---|---|
In methanol at 80℃; for 4h; | 100% |
N-acetylpiperidine
4-fluorostyrene oxide
1-{4-[2-(4-fluoro-phenyl)-2-hydroxy-ethyl]-piperazin-1-yl}-ethanone
Conditions | Yield |
---|---|
100% |
N-acetylpiperidine
2-(tert-butoxycarbonylamino)ethyl bromide
tert-butyl 2-(4-acetylpiperazin-1-yl)ethylcarbamate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 16h; Reflux; | 100% |
With triethylamine In dichloromethane for 16h; Reflux; | 100% |
With triethylamine In dichloromethane for 16h; Reflux; | 100% |
N-acetylpiperidine
6-chloro-pyridine-2-carbonitrile
Conditions | Yield |
---|---|
In acetonitrile at 150℃; for 1h; Microwave irradiation; | 100% |
N-acetylpiperidine
1-(4-chlorophenyl)-1H-pyrazole-4-carbaldehyde
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In methanol at 20℃; under 3102.97 Torr; for 6h; | 100% |
N-acetylpiperidine
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In dichloromethane at 15℃; for 18h; | 100% |
N-acetylpiperidine
tert-butyl (2S)-2-[((2S)-2-{[(benzyloxy)carbonyl]amino}-4-methylpentanoyl)amino]-3-(4-hydroxyphenyl)propanoate
bis(trichloromethyl) carbonate
Conditions | Yield |
---|---|
Stage #1: tert-butyl (2S)-2-[((2S)-2-{[(benzyloxy)carbonyl]amino}-4-methylpentanoyl)amino]-3-(4-hydroxyphenyl)propanoate; bis(trichloromethyl) carbonate With N-ethyl-N,N-diisopropylamine In tetrahydrofuran; ethanol; dichloromethane at 20℃; for 4h; Stage #2: N-acetylpiperidine With N-ethyl-N,N-diisopropylamine In tetrahydrofuran; dichloromethane for 18h; | 99% |
N-acetylpiperidine
3-(6-bromo-quinazolin-4-yl)-benzoic acid
1-{4-[3-(6-bromo-quinazolin-4-yl)-benzoyl]-piperazine-1-yl}-ethanone
Conditions | Yield |
---|---|
Stage #1: 3-(6-bromo-quinazolin-4-yl)-benzoic acid With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 0.166667h; Stage #2: N-acetylpiperidine In dichloromethane at 20℃; for 2h; | 99% |
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine In ethyl acetate at 20℃; | 90% |
Stage #1: 3-(6-bromo-quinazolin-4-yl)-benzoic acid With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 0.166667h; Stage #2: N-acetylpiperidine In dichloromethane at 20℃; for 2h; | 3.03 mg |
Stage #1: 3-(6-bromo-quinazolin-4-yl)-benzoic acid With 5-bromo-2-ethoxy-3-trifluoromethyl-pyridine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate In dichloromethane at 20℃; for 0.166667h; Stage #2: N-acetylpiperidine In dichloromethane at 20℃; for 2h; | |
Stage #1: 3-(6-bromo-quinazolin-4-yl)-benzoic acid With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 0.166667h; Stage #2: N-acetylpiperidine In dichloromethane at 20℃; for 2h; |
N-acetylpiperidine
ortho-nitrofluorobenzene
1-(4-(2-nitrophenyl)piperazin-1-yl)ethanone
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 17h; | 99% |
With potassium carbonate In N,N-dimethyl-formamide at 25 - 50℃; for 17h; | 99% |
Conditions | Yield |
---|---|
With C32H36ClNO2P2Ru; hydrogen In tetrahydrofuran at 120℃; under 30402 Torr; for 20h; Autoclave; Green chemistry; | 99% |
With Au-TiO2; hydrogen In N,N-dimethyl acetamide at 140℃; for 5h; | 98% |
With dmap; hydrogen; copper diacetate In tetrahydrofuran at 90℃; under 60804.1 Torr; for 12h; Sealed tube; chemoselective reaction; | 80 %Chromat. |
N-acetylpiperidine
ethyl 7-chloro-1-ethyl-1,4-dihydro-4-oxo-1,8-naphthyridine-3-carboxylate
ethyl 7-(4-acetyl-1-piperazinyl)-1-ethyl-1,4-dihydro-4-oxo-1,8-naphthyridine-3-carboxylate
Conditions | Yield |
---|---|
In ethanol for 3h; Heating; | 98.1% |
N-acetylpiperidine
(5S)-5-(tert-butyldiphenylsiloxymethyl)-2(5H)-furanone
Conditions | Yield |
---|---|
In tetrahydrofuran for 24h; Ambient temperature; | 98% |
N-acetylpiperidine
ethyl acetoacetate
malononitrile
6-amino-2,4-dihydro-3,4-dimethyl-4-(piperazin-1-yl)pyrano[2,3-c]pyrazole-5-carbonitrile
Conditions | Yield |
---|---|
With hydrazine hydrate; heptakis(6-amino-6-deoxy)-β-cyclodextrin at 20℃; for 0.0166667h; Neat (no solvent); | 98% |
N-acetylpiperidine
Conditions | Yield |
---|---|
Stage #1: N-acetylpiperidine; methyl 4-(((3R,5S)-4-(3-formylbenzyl)-3,5-dimethylpiperazin-1-yl)methyl)benzoate In dichloromethane at 20℃; for 1h; Stage #2: With sodium tris(acetoxy)borohydride In dichloromethane at 20℃; for 17h; | 97.7% |
N-acetylpiperidine
3-chloro-4-fluoronitrobenzene
1-acetyl-4-(2-chloro-4-nitrophenyl)piperazine
Conditions | Yield |
---|---|
at 55℃; for 1h; | 97% |
With pyridine at 60℃; for 2h; Substitution; condensation; | 53% |
With potassium carbonate In dimethyl sulfoxide at 90℃; for 4h; |
N-acetylpiperidine
N-[4-(2-bromo-ethoxy)-3-(2-methyl-2H-pyrazol-3-yl)-phenyl]-3-methoxy-benzamide
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 0.333333h; Microwave irradiation; | 97% |
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 0.333333h; Microwave irradiation; |
benzoxazole
N-acetylpiperidine
1-(4-(benzo[d]oxazol-2-yl)piperazin-1-yl)ethan-1-one
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; 1-(n-butyl)pyridinium iodide; acetic acid In water; acetonitrile at 20℃; for 3.5h; Green chemistry; | 97% |
Stage #1: benzoxazole; N-acetylpiperidine With N-iodo-succinimide; dihydrogen peroxide; acetic acid In water; acetonitrile at 20℃; for 6h; Stage #2: With sodium carbonate In water; ethyl acetate; acetonitrile Saturated solution; | 90% |
With dihydrogen peroxide; tetra-(n-butyl)ammonium iodide; acetic acid In water; acetonitrile at 20℃; for 3h; | 83% |
With copper acetylacetonate; oxygen In 5,5-dimethyl-1,3-cyclohexadiene at 140℃; for 14h; | 82% |
Multi-step reaction with 2 steps 1: neat (no solvent) / 1 h / 60 °C 2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane / 0.5 h / 25 °C View Scheme |
Conditions | Yield |
---|---|
Stage #1: methanol; N-acetylpiperidine With Ag/TiO2 at 25℃; under 760.051 Torr; for 10h; UV-irradiation; Stage #2: With hydrogenchloride In diethyl ether at 25℃; for 12h; | 97% |
N-acetylpiperidine
3-(Dimethylaminomethyl)indole
3-[(4-acetylpiperazin-1-yl)methyl]-1H-indole
Conditions | Yield |
---|---|
In toluene Reflux; | 97% |
Conditions | Yield |
---|---|
In 1-methyl-pyrrolidin-2-one at 100℃; for 2h; | 97% |
N-acetylpiperidine
N-(5-((dibenzylamino)methyl)-4-oxo-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-2-yl)octanamide
Conditions | Yield |
---|---|
In tetrahydrofuran; methanol at 75℃; for 24h; Sealed tube; | 97% |
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