Conditions | Yield |
---|---|
In tetrahydrofuran at -5 - 0℃; for 1h; | 83% |
Conditions | Yield |
---|---|
With PEG-400; aluminum oxide; sodium hydroxide; water 1.) MeOH, r.t., 30 min, 2.) r.t., 1 h; | 79% |
With triethylamine In diethyl ether at 20℃; for 12h; | 68% |
With copper; sodium carbonate; toluene |
Conditions | Yield |
---|---|
With pyridine |
Conditions | Yield |
---|---|
With ethanol |
Conditions | Yield |
---|---|
With trichlorothiophosphine; ethanol |
4-(4-nitrophenoxy)butanoic acid
diethyl phosphorochloridothioate
parathion
Conditions | Yield |
---|---|
With diethylene glycol | |
With hexamethylenetetramine; chlorobenzene | |
With chlorobenzene at 120℃; | |
With water at 95 - 100℃; | |
With ethanol |
Conditions | Yield |
---|---|
In ethanol for 1h; Heating; Yield given; |
Conditions | Yield |
---|---|
With 3,3-dimethyldioxirane In dichloromethane; acetone for 0.0833333h; Ambient temperature; | 100% |
With 3,3-dimethyldioxirane In dichloromethane; acetone for 0.0833333h; Ambient temperature; other phosphorothioates, also with phosphine sulfides; | 100% |
With perfluro-cis-2-n-butyl-3-n-propyloxaziridine In various solvent(s) at -30℃; for 6h; | 90% |
Conditions | Yield |
---|---|
With sodium hydroxide In cyclohexane at 50℃; for 144h; | 55% |
parathion
A
Diethyl phosphate
B
para-nitro-phenylphosphonate diethylique
C
phosphonic acid diethyl ester
Conditions | Yield |
---|---|
With magnesium monoperoxyphthalate hexahydrate In water at 25℃; for 24h; | A 28% B 38% C 29% |
Conditions | Yield |
---|---|
at 170℃; |
parathion
thiophosphoric acid S-ethyl ester-O,O'-bis-(4-nitro-phenyl ester)
parathion
Conditions | Yield |
---|---|
With hydrogenchloride; zinc anschliessenden Diazotieren und Kuppeln mit N-<1>Naphthyl-aethylendiamin-dihydrochlorid; |
parathion
thiophosphoric acid O-ethyl ester-O'-(4-nitro-phenyl ester); silver-salt
Conditions | Yield |
---|---|
With ethanol; silver nitrate; acetonitrile |
ethene
parathion
O-Aethyl-O-<-p-nitro-phenyl>-S-<2-chloraethyl>-phosphorothionat
Conditions | Yield |
---|---|
(i) SO2Cl2, benzene, (ii) /BRN= 1730731/; Multistep reaction; |
Conditions | Yield |
---|---|
With hydrogenchloride; zinc; sodium nitrite In ethanol; water |
Conditions | Yield |
---|---|
With sodium hypochlorite; bis(hydroxyethyl)cetylmethyl ammonium bromide at 25℃; Rate constant; reaction in presence of other reagents possessing positive chlorine, other surfactants; influence of temperature, pH, surfactant concentration; | |
With rat liver microsomes Enzyme kinetics; Further Variations:; Reaction partners; dearylation; Enzymatic reaction; | |
With sodium hydroxide; β‐cyclodextrin at 25℃; Kinetics; Further Variations:; Reagents; Hydrolysis; |
Conditions | Yield |
---|---|
With water; palladium (II) ion In various solvent(s) at 25℃; |
Conditions | Yield |
---|---|
With Cu(ClO)4(N,N,N',N'-tetramethylethylene diamine) In methanol; water at 35℃; Rate constant; Mechanism; Thermodynamic data; var. Cu(II) diamine complexes; Ea, ΔG(excit.), ΔH(excit.), ΔS(excit.); | |
With sodium perchlorate; cycloplatinated aryl ketoxime In acetonitrile at 25℃; pH=8.5; Kinetics; Further Variations:; Catalysts; pH-values; | |
With N-2-hydroxyethylpiperazine-N'-2-ethanesulfonic acid; recombinant bacterial organophosphorous hydrolase In methanol Enzyme kinetics; |
parathion
O,O-diethyl O-(4-nitrosophenyl) thiophosphate
Conditions | Yield |
---|---|
With iron In methanol at 15℃; pH=5.9; Kinetics; Reduction; |
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