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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryProduct name: 1,6-Anhydro-Beta-D-Mannopyranose CAS No.: 14168-65-1 Molecule Formula:C6H10O5 Molecule Weight:162.14 Purity: 95.0% Package: 5kg/drum Description:White or off-white powder Manufacture Standards:Enterprise Standard TE
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiry1,6-Anhydro-beta-d-mannopyranose cas 14168-65-1Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Zhengzhou Kingorgchem Chemical Technology Co., Ltd. was founded on the basis of Organophosphorus Chemistry Lab of Institute of Chemistry Henan Academy of Sciences in 2015. The laboratory covers 600 m2 and the pilot plant covers 2000 m2. Kingorgchem i
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inquiryAt Share Chemical Company, we scrupulously abide by our policy of “Excellent Quality at a Reasonable Price”. We strive to satisfy all of our customers by providing the finest quality products supported by the finest in customer servi
United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat
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inquiryFINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 1,6-ANHYDRO-BETA-D-MANNOPYRANOSE, CAS:14168-65-1 with the most competitive price and
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Manufacturer,strong R&D,professional team Storage:Store in a cool, dry place. Store in a tightly closed container. Package:according to your requirement Application:ZhiShang Chemical is owned by ZhiShang Group, is a professional new-type chemicals en
high purity Application:Drug intermediates Materials intermediates and active molecules
D-Mannose
mannosan
Conditions | Yield |
---|---|
With p-toluenesulfonyl chloride In pyridine for 4h; Ambient temperature; | 80% |
With pyridine; p-toluenesulfonyl chloride at 20℃; for 21h; Inert atmosphere; | 48.4% |
With toluene-4-sulfonic acid In N,N-dimethyl-formamide | 20% |
6-O-p-toluenesulfonyl-D-mannopyranose
mannosan
Conditions | Yield |
---|---|
NaOH In pyridine; sodium hydroxide for 1h; Ambient temperature; | 77% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In ethanol Ambient temperature; | |
With sodium hydride In N,N-dimethyl-formamide for 15h; Ambient temperature; | |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile for 0.5h; Ambient temperature; |
1,6-anhydro-2,3,4-tri-O-benzyl-β-D-mannopyranose
A
1,6-anhydro-3-O-benzoyl-β-D-mannopyranose
B
mannosan
Conditions | Yield |
---|---|
palladium on activated charcoal In isopropyl alcohol for 4h; Heating; | A 40% B n/a |
With isopropyl alcohol; palladium on activated charcoal for 4h; Heating; | A 40% B n/a |
2,3,4-tri-O-acetyl-1,6-anhydro-β-D-mannopyranose
mannosan
Conditions | Yield |
---|---|
With methanol; barium methoxide |
D-Mannose
mannosan
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid; benzene In N,N-dimethyl-formamide |
(1R,2S,6S,7R,8R)-7-Allyloxy-4-vinyl-3,5,10,11-tetraoxa-tricyclo[6.2.1.02,6]undecane
mannosan
Conditions | Yield |
---|---|
With sodium acetate; palladium dichloride In acetic acid at 20℃; for 24h; |
1,6-anhydro-2,3-O-isopropylidene-β-D-mannopyranose
mannosan
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In methanol for 30h; Heating; |
mannosan
Conditions | Yield |
---|---|
With sulfuric acid |
Conditions | Yield |
---|---|
Stage #1: D-Mannose; p-toluenesulfonyl chloride Tosylation; Stage #2: With sodium hydroxide In water Cyclization; Further stages.; |
dianhydroaltrose
mannosan
Conditions | Yield |
---|---|
Stage #1: dianhydroaltrose With boron trifluoride diethyl etherate Stage #2: With sodium methylate In methanol |
mannosan
Conditions | Yield |
---|---|
With sodium methylate In methanol |
1,6-anhydro-2,3,4-tri-O-benzoyl-β-D-mannopyranose
mannosan
Conditions | Yield |
---|---|
With sodium methylate In methanol |
2,3-isopropylidenedioxy-D-mannono-γ-lactone
mannosan
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 61 percent / pyridine / 10 h / Ambient temperature 2: 98 percent / imidazole / dimethylformamide / 10 h / Ambient temperature 3: 90 percent / iBu2AlH / hexane; toluene / 4 h / -78 °C 4: 12 percent / NaH / dimethylformamide / 1.5 h / Ambient temperature 5: pyridinium p-toluenesulfonate / methanol / 30 h / Heating View Scheme | |
Multi-step reaction with 6 steps 1: 61 percent / pyridine / 10 h / Ambient temperature 2: 98 percent / imidazole / dimethylformamide / 10 h / Ambient temperature 3: 90 percent / iBu2AlH / hexane; toluene / 4 h / -78 °C 4: 35 percent / NaH / dimethylformamide / 1.5 h / Ambient temperature 5: 70 percent / Bu4NF / tetrahydrofuran / 0.17 h 6: pyridinium p-toluenesulfonate / methanol / 30 h / Heating View Scheme |
2,3-O-Isopropylidene-4-O-t-butyldimethylsilyl-1,6-anhydro-β-D-mannopyranose
mannosan
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 70 percent / Bu4NF / tetrahydrofuran / 0.17 h 2: pyridinium p-toluenesulfonate / methanol / 30 h / Heating View Scheme |
2,3-O-Isopropylidene-6-O-(p-tolylsulfonyl)-D-mannono-1,4-lactone
mannosan
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 98 percent / imidazole / dimethylformamide / 10 h / Ambient temperature 2: 90 percent / iBu2AlH / hexane; toluene / 4 h / -78 °C 3: 12 percent / NaH / dimethylformamide / 1.5 h / Ambient temperature 4: pyridinium p-toluenesulfonate / methanol / 30 h / Heating View Scheme | |
Multi-step reaction with 5 steps 1: 98 percent / imidazole / dimethylformamide / 10 h / Ambient temperature 2: 90 percent / iBu2AlH / hexane; toluene / 4 h / -78 °C 3: 35 percent / NaH / dimethylformamide / 1.5 h / Ambient temperature 4: 70 percent / Bu4NF / tetrahydrofuran / 0.17 h 5: pyridinium p-toluenesulfonate / methanol / 30 h / Heating View Scheme |
mannosan
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 12 percent / NaH / dimethylformamide / 1.5 h / Ambient temperature 2: pyridinium p-toluenesulfonate / methanol / 30 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1: 35 percent / NaH / dimethylformamide / 1.5 h / Ambient temperature 2: 70 percent / Bu4NF / tetrahydrofuran / 0.17 h 3: pyridinium p-toluenesulfonate / methanol / 30 h / Heating View Scheme |
2,3-O-Isopropylidene-5-O-tert-butyldimethylsilyl-6-O-(p-tolylsulfonyl)-D-mannono-1,4-lactone
mannosan
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 90 percent / iBu2AlH / hexane; toluene / 4 h / -78 °C 2: 12 percent / NaH / dimethylformamide / 1.5 h / Ambient temperature 3: pyridinium p-toluenesulfonate / methanol / 30 h / Heating View Scheme | |
Multi-step reaction with 4 steps 1: 90 percent / iBu2AlH / hexane; toluene / 4 h / -78 °C 2: 35 percent / NaH / dimethylformamide / 1.5 h / Ambient temperature 3: 70 percent / Bu4NF / tetrahydrofuran / 0.17 h 4: pyridinium p-toluenesulfonate / methanol / 30 h / Heating View Scheme |
2,3:5,6-di-O-isopropylidene-α-D-mannofuranose
mannosan
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: 80 percent / Collins' reagent / CH2Cl2 / 0.5 h / Ambient temperature 2: gl. AcOH, water / 4 h / 60 °C 3: 61 percent / pyridine / 10 h / Ambient temperature 4: 98 percent / imidazole / dimethylformamide / 10 h / Ambient temperature 5: 90 percent / iBu2AlH / hexane; toluene / 4 h / -78 °C 6: 12 percent / NaH / dimethylformamide / 1.5 h / Ambient temperature 7: pyridinium p-toluenesulfonate / methanol / 30 h / Heating View Scheme | |
Multi-step reaction with 8 steps 1: 80 percent / Collins' reagent / CH2Cl2 / 0.5 h / Ambient temperature 2: gl. AcOH, water / 4 h / 60 °C 3: 61 percent / pyridine / 10 h / Ambient temperature 4: 98 percent / imidazole / dimethylformamide / 10 h / Ambient temperature 5: 90 percent / iBu2AlH / hexane; toluene / 4 h / -78 °C 6: 35 percent / NaH / dimethylformamide / 1.5 h / Ambient temperature 7: 70 percent / Bu4NF / tetrahydrofuran / 0.17 h 8: pyridinium p-toluenesulfonate / methanol / 30 h / Heating View Scheme |
2,3,5,6-di-O-isopropylidene-D-mannono-1,4-lactone
mannosan
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: gl. AcOH, water / 4 h / 60 °C 2: 61 percent / pyridine / 10 h / Ambient temperature 3: 98 percent / imidazole / dimethylformamide / 10 h / Ambient temperature 4: 90 percent / iBu2AlH / hexane; toluene / 4 h / -78 °C 5: 12 percent / NaH / dimethylformamide / 1.5 h / Ambient temperature 6: pyridinium p-toluenesulfonate / methanol / 30 h / Heating View Scheme | |
Multi-step reaction with 7 steps 1: gl. AcOH, water / 4 h / 60 °C 2: 61 percent / pyridine / 10 h / Ambient temperature 3: 98 percent / imidazole / dimethylformamide / 10 h / Ambient temperature 4: 90 percent / iBu2AlH / hexane; toluene / 4 h / -78 °C 5: 35 percent / NaH / dimethylformamide / 1.5 h / Ambient temperature 6: 70 percent / Bu4NF / tetrahydrofuran / 0.17 h 7: pyridinium p-toluenesulfonate / methanol / 30 h / Heating View Scheme |
Conditions | Yield |
---|---|
With water In sulfolane at 220℃; for 0.05h; Microwave irradiation; | A 14.7 %Chromat. B 63.9 %Chromat. |
methyl α-D-mannofuranoside
A
1,6-Anhydro-β-D-mannohexofuranose
B
mannosan
Conditions | Yield |
---|---|
In sulfolane at 240℃; for 0.05h; Microwave irradiation; | A 57.1 %Chromat. B 5.8 %Chromat. |
With water In sulfolane at 240℃; for 0.05h; Microwave irradiation; | A 12.5 %Chromat. B 48.1 %Chromat. |
(2R,3S,4S,5S,6S)-2-(hydroxymethyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triol
mannosan
Conditions | Yield |
---|---|
With water In sulfolane at 280℃; for 0.05h; Microwave irradiation; | 79.8 %Chromat. |
mannosan
Conditions | Yield |
---|---|
With sodium hydroxide at 0 - 20℃; Inert atmosphere; |
β-D-mannose
mannosan
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: pyridine / 1 h / 0 - 20 °C / Inert atmosphere 2: sodium hydroxide / 0 - 20 °C / Inert atmosphere View Scheme |
acetic anhydride
mannosan
D-Mannose pentaacetate
Conditions | Yield |
---|---|
scandium tris(trifluoromethanesulfonate) at 20℃; for 5h; | 95% |
benzyl bromide
mannosan
1,6-anhydro-2,3,4-tri-O-benzyl-β-D-mannopyranose
Conditions | Yield |
---|---|
Stage #1: mannosan With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 1h; Stage #2: benzyl bromide In N,N-dimethyl-formamide at 15 - 20℃; for 15h; | 92% |
With barium dihydroxide; barium(II) oxide In N,N-dimethyl-formamide for 1h; Ambient temperature; Yield given; | |
With tetra-(n-butyl)ammonium iodide; sodium hydride 1.) DMF, DMF; Multistep reaction; |
triisopropylsilyl trifluoromethanesulfonate
mannosan
1,6-anhydro-2,3,4-tris-O-(triisopropylsilyl)-β-D-mannopyranose
Conditions | Yield |
---|---|
With pyridine In 1,1,2,2-tetrachloroethane at 110℃; for 15h; | 92% |
tert-butyldimethylsilane
mannosan
Conditions | Yield |
---|---|
With [Ir(COD)(PPh3)2]SbF6 In N,N-dimethyl acetamide at 70℃; | A 86% B 5% |
chloro-trimethyl-silane
mannosan
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere; | 86% |
triisopropylsilyl trifluoromethanesulfonate
mannosan
1,6-anhydro-2,4-bis-O-(triisopropylsilyl)-β-D-mannopyranose
Conditions | Yield |
---|---|
In pyridine; dichloromethane | 80% |
Conditions | Yield |
---|---|
With iron(III)-acetylacetonate; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 4h; Green chemistry; regioselective reaction; | 78% |
9,9-dichloro-9H-fluorene
mannosan
1,6-anhydro-2,3-O-fluoren-9-ylidene-β-D-mannopyranose
Conditions | Yield |
---|---|
With pyridine at 110℃; for 96h; | 73% |
Conditions | Yield |
---|---|
With diphenylborate ethanolamine ester; silver(l) oxide In acetonitrile at 40℃; for 48h; Inert atmosphere; regioselective reaction; | 73% |
1-bromomethyl-4-bromobenzene
mannosan
A
1,6-anhydro-2-O-(4-bromobenzyl)-β-D-mannopyranoside
Conditions | Yield |
---|---|
With diphenylborate ethanolamine ester; silver(l) oxide In acetonitrile at 40℃; for 48h; Inert atmosphere; regioselective reaction; | A 73% B n/a |
2-bromomethylnaphthyl bromide
mannosan
1,6-anhydro-2-O-(2-naphthyl)methyl-β-D-mannopyranoside
Conditions | Yield |
---|---|
With diphenylborate ethanolamine ester; silver(l) oxide In acetonitrile at 40℃; for 48h; Inert atmosphere; regioselective reaction; | 71% |
acrylic acid methyl ester
mannosan
Conditions | Yield |
---|---|
With Quinuclidine; [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate; oxybis(diphenylborane) In acetonitrile at 25℃; for 16h; Reagent/catalyst; Irradiation; Inert atmosphere; Schlenk technique; Sealed tube; | 68% |
benzaldehyde dimethyl acetal
mannosan
1,6-anhydro-2,3-O-endo-benzylidene-β-D-mannopyranose
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 50℃; for 1h; | 65.2% |
benzyl bromide
mannosan
A
1,6-anhydro-3-O-benzyl-β-D-mannopyranose
B
1,6-anhydro-2-O-benzyl-β-D-mannopyranoside
Conditions | Yield |
---|---|
With 3 A molecular sieve; bis(tri-n-butyltin)oxide; 1-methyl-1H-imidazole; tetra-(n-butyl)ammonium iodide In toluene 1.) reflux, 15 h; 2.) 2 h; | A 25% B 65% |
With 3 A molecular sieve; bis(tri-n-butyltin)oxide; 1-methyl-1H-imidazole; tetrabutylammomium bromide In toluene 1.) reflux, 15 h; 2.) 8 h; | A 38% B 52% |
1,2-propylene cyclic carbonate
mannosan
Conditions | Yield |
---|---|
With 3-methyl-2-butynyltetramethylenesulfonium hexafluoroantimonate at 90℃; for 0.333333h; | 64% |
mannosan
polymer, product of cationic polymerization, branching degree 0.44, Mw 1.050E4, PDI 1.43 by SEC, Mw 6.37E5 by SLS; monomer(s): 1,6-anhydro-β-D-mannopyranose
Conditions | Yield |
---|---|
With 1-(2-butenyl)tetrahydrothiophenium hexafluoroantimonate In various solvent(s) at 150℃; for 0.666667h; | 63% |
Benzyloxymethyl chloride
mannosan
A
1,6-anhydro-2-O-benzyloxymethyl-β-D-mannopyranoside
Conditions | Yield |
---|---|
With diphenylborate ethanolamine ester; silver(l) oxide In acetonitrile at 40℃; for 48h; Inert atmosphere; regioselective reaction; | A 63% B n/a |
mannosan
polymer, product of cationic polymerization, branching degree 0.43, Mw 3.20E3, PDI 1.35 by SEC, Mw 8.05E4 by SLS; monomer(s): 1,6-anhydro-β-D-mannopyranose
Conditions | Yield |
---|---|
With 1-(2-butenyl)tetrahydrothiophenium hexafluoroantimonate In various solvent(s) at 130℃; for 0.333333h; | 61.6% |
mannosan
polymer, product of cationic polymerization, branching degree 0.43, Mw 4.30E3, PDI 1.49 by SEC, Mw 9.63E4 by SLS; monomer(s): 1,6-anhydro-β-D-mannopyranose
Conditions | Yield |
---|---|
With 1-(2-butenyl)tetrahydrothiophenium hexafluoroantimonate In various solvent(s) at 150℃; for 0.333333h; | 61.1% |
mannosan
polymer, product of cationic polymerization, branching degree 0.41, Mw 2.48E3, PDI 1.31 by SEC, Mw 6.94E4 by SLS; monomer(s): 1,6-anhydro-β-D-mannopyranose
Conditions | Yield |
---|---|
With 1-(2-butenyl)tetrahydrothiophenium hexafluoroantimonate In various solvent(s) at 130℃; for 0.666667h; | 57% |
mannosan
polymer, product of cationic polymerization, branching degree 0.42, Mw 2.17E3, PDI 1.30 by SEC, Mw 3.42E4 by SLS; monomer(s): 1,6-anhydro-β-D-mannopyranose
Conditions | Yield |
---|---|
With 1-(2-butenyl)tetrahydrothiophenium hexafluoroantimonate In various solvent(s) at 130℃; for 0.333333h; | 56.6% |
2-(dimethoxymethyl)naphthalene
mannosan
A
endo-1,6-anhydro-2,3-O-(2-naphthyl)methylene-β-D-mannopyranose
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 20℃; for 24h; | A 55% B 9.2% |
N-benzoyloxybenzotriazole
mannosan
B
1,6-anhydro-2,4-di-O-benzoyl-β-D-mannopyranose
C
1,6-anhydro-2,3,4-tri-O-benzoyl-β-D-mannopyranose
Conditions | Yield |
---|---|
With pyridine at 20℃; for 76h; | A 15% B 54% C 26% |
N-benzoyloxybenzotriazole
mannosan
1,6-anhydro-2,4-di-O-benzoyl-β-D-mannopyranose
Conditions | Yield |
---|---|
With pyridine | 54% |
benzaldehyde dimethyl acetal
mannosan
1,6-anhydro-2,3-O-endo-benzylidene-β-mannopyranose
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 50℃; under 30 Torr; for 3h; | 38% |
With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 65 - 75℃; for 3h; | 24% |
p-Anisaldehyde dimethyl acetal
mannosan
B
1,6-Anhydro-endo-2,3-O-(4-methoxybenzylidene)-β-D-mannopyranose
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 50℃; under 225.023 Torr; for 4h; optical yield given as %de; | A n/a B 31% |
With toluene-4-sulfonic acid In N,N-dimethyl-formamide |
mannosan
polymer, product of cationic polymerization, branching degree 0.44, Mw 5.84E3, PDI 1.84 by SEC, Mw 8.09E4 by SLS; monomer(s): 1,6-anhydro-β-D-mannopyranose
Conditions | Yield |
---|---|
With 1-(2-butenyl)tetrahydrothiophenium hexafluoroantimonate at 210℃; for 0.0166667h; | 23.8% |
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