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inquiryN-Dodecanoyl-L-phenlyalanine CAS:14379-64-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality org
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiryN-Dodecanoyl-phenlyalanine Application:824934
Cas:14379-64-7
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inquiry(2s)-2-(dodecanoylamino)-3-phenylpropanoic Acid Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shan
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inquiryn-dodecanoyl chloride
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
Stage #1: Wang resin-bound Fmoc-L-phenylalanine With piperidine In N,N-dimethyl-formamide at 20℃; Stage #2: n-dodecanoyl chloride With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 1h; Stage #3: With trifluoroacetic acid In dichloromethane at 20℃; for 18h; | 99% |
N-n-dodecanoyl methyl (L)-phenylalaninate
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
With sodium hydroxide In tetrahydrofuran; methanol; water at 0℃; for 2h; | 98% |
With sodium hydroxide In tetrahydrofuran; methanol at 20℃; for 2h; | |
Multi-step reaction with 2 steps 1: sodium hydroxide / methanol / 20 °C 2: hydrogenchloride / water View Scheme |
Conditions | Yield |
---|---|
With potassium carbonate In water; acetone at 0 - 20℃; | 89% |
Stage #1: L-phenylalanine With sodium hydroxide In water; acetone for 0.5h; Cooling with ice; Stage #2: n-dodecanoyl chloride In water; acetone | 83% |
With sodium hydroxide at 3℃; |
p-nitrophenyl N-dodecanoyl-D-phenylalaninate
A
4-nitro-phenol
B
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
With coaggregate system composed of 59 mol percent ditetradecyl-dimethylammonium bromide and 41 mol percent hexadecyltrimethylammonium bromide; tris buffer (μ=0.2 with KCl); water; quercitrin; acetonitrile; Z-Phe-His-Leu at 25℃; Rate constant; enantioselective hydrolysis; var. flavonoids; pH 7.6; |
p-nitrophenyl N-dodecanoyl-L-phenylalanine
A
4-nitro-phenol
B
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
With coaggregate system composed of 59 mol percent ditetradecyl-dimethylammonium bromide and 41 mol percent hexadecyltrimethylammonium bromide; tris buffer (μ=0.2 with KCl); water; quercitrin; acetonitrile; Z-Phe-His-Leu at 25℃; Rate constant; enantioselective hydrolysis; var. flavonoids; pH 7.6; | |
With Tris-KCl buffer; water; N,N-dimethyl-N-tetradecyltetradecan-1-aminium bromide; MyrHisLeu In acetonitrile at 25℃; Rate constant; pH 7.6; hydrolysis; other catalysts;; | |
Z-L-Phe-L-His-L-Leu-OH In methanol; water at 25℃; Rate constant; other catalysts (Z-L-His-L-Phe, Z-Phe-L-Phe-L-His, Bz-Gly-L-His-L-Leu, Z-L-Phe-L-His-L-Leu)and by benzylhexadecyldimethylammonium chloride and hexadecyltrimethylammonium chloride; |
p-nitrophenyl N-dodecanoyl-L-phenylalanine
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
With N,N-dimethyl-N-tetradecyltetradecan-1-aminium bromide; N-tetradecanoyl-L-histidyl-L-leucine In water; acetonitrile at 10 - 45℃; Kinetics; Thermodynamic data; ΔG(excit.), other dialkyldimethylammonium bromides; |
p-nitrophenyl n-dodecanoyl-D(L)-phenylalaninate
A
N-dodecanoyl-L-phenylalanine
B
n-dodecanoyl-D-phenylalanine
Conditions | Yield |
---|---|
With N,N-dimethyl-N-tetradecyltetradecan-1-aminium bromide; Z-L-Phe-L-His-L-Leu-OH In water; acetonitrile at 25℃; Rate constant; Product distribution; enantioselective hydrolysis; var. ionic strenght, pH 7.6; | |
With MES buffer; copper(II) ion; (4R,14R)-9-dodecyl-4,14-dihydroxymethyl-6,12-dithia-3,9,15,18-tetraazabicyclo[15.3.1]heneicosa-1(18),17(19),20-triene-2,16-dione In acetonitrile at 25℃; Rate constant; var. macrocyclic ligands and metal ions; | |
Z-Phe-His-Leu In various solvent(s) at 10 - 35℃; pH=7.6; Kinetics; Further Variations:; Temperatures; composition of coaggregates; ionic strength; Hydrolysis; | |
With L-tartaric acid co-embedded with bis-zinc-cyclen complex Zn2Cy into 1,2-dioleoyl-sn-glycero-3-phosphocholine membrane In aq. buffer at 20℃; pH=7.4; Kinetics; Reagent/catalyst; |
n-dodecanoyl chloride
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 83 percent / KHCO3; triethylamine / H2O; CHCl3 / 5 h / 0 °C 2: 98 percent / NaOH / methanol; tetrahydrofuran; H2O / 2 h / 0 °C View Scheme |
L-phenylalanine
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: SOCl2 / 6 h 2: 83 percent / KHCO3; triethylamine / H2O; CHCl3 / 5 h / 0 °C 3: 98 percent / NaOH / methanol; tetrahydrofuran; H2O / 2 h / 0 °C View Scheme | |
Multi-step reaction with 3 steps 1: thionyl chloride / 10 h / 0 °C / Reflux 2: triethylamine / dichloromethane / 20 °C / Cooling with ice 3: sodium hydroxide / methanol; tetrahydrofuran / 2 h / 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: thionyl chloride / 18 h / 0 °C 2: sodium hydrogencarbonate 3: dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 18 h / 0 °C 4: sodium hydroxide / methanol / 20 °C 5: hydrogenchloride / water View Scheme |
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 83 percent / KHCO3; triethylamine / H2O; CHCl3 / 5 h / 0 °C 2: 98 percent / NaOH / methanol; tetrahydrofuran; H2O / 2 h / 0 °C View Scheme | |
Multi-step reaction with 4 steps 1: sodium hydrogencarbonate 2: dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 18 h / 0 °C 3: sodium hydroxide / methanol / 20 °C 4: hydrogenchloride / water View Scheme |
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane 2-chlorotrityl chloride resin; | 34.3 mg |
methyl (2S)-2-amino-3-phenylpropanoate
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / dichloromethane / 20 °C / Cooling with ice 2: sodium hydroxide / methanol; tetrahydrofuran / 2 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 18 h / 0 °C 2: sodium hydroxide / methanol / 20 °C 3: hydrogenchloride / water View Scheme |
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
With hydrogenchloride In water | 1.37 g |
N-dodecanoyl-L-phenylalanine
L-proline methyl ester monohydrochloride
Conditions | Yield |
---|---|
Stage #1: N-dodecanoyl-L-phenylalanine With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine In tetrahydrofuran; N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #2: L-proline methyl ester monohydrochloride In tetrahydrofuran; N,N-dimethyl-formamide at 20℃; for 17h; | 44% |
Stage #1: N-dodecanoyl-L-phenylalanine With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate In tetrahydrofuran; N,N-dimethyl-formamide for 0.166667h; Stage #2: L-proline methyl ester monohydrochloride In tetrahydrofuran; N,N-dimethyl-formamide at 20℃; for 17h; | 44% |
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; | 32% |
N-dodecanoyl-L-phenylalanine
L-Histidine methyl ester
N-lauroyl-L-phenylalanyl-L-histidine methyl ester
n-Dodecylamine
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
With boron trioxide; propylene glycol monoethyl ether at 125℃; for 10h; |
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In chloroform at 20℃; for 12h; |
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dicyclohexyl-carbodiimide / chloroform / 12 h / 20 °C 2: sodium carbonate / water; acetone / 20 °C View Scheme |
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: dicyclohexyl-carbodiimide / chloroform / 12 h / 20 °C 2: sodium carbonate / water; acetone / 20 °C 3: dicyclohexyl-carbodiimide / chloroform / 12 h / 20 °C View Scheme |
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: dicyclohexyl-carbodiimide / chloroform / 12 h / 20 °C 2: sodium carbonate / water; acetone / 20 °C 3: dicyclohexyl-carbodiimide / chloroform / 12 h / 20 °C 4: sodium carbonate / water; acetone / 20 °C View Scheme |
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: dicyclohexyl-carbodiimide / chloroform / 12 h / 20 °C 2.1: sodium carbonate / water; acetone / 20 °C 3.1: dicyclohexyl-carbodiimide / chloroform / 12 h / 20 °C 4.1: sodium carbonate / water; acetone / 20 °C 5.1: dicyclohexyl-carbodiimide / N,N-dimethyl-formamide 5.2: 20 °C View Scheme |
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: dicyclohexyl-carbodiimide / chloroform / 12 h / 20 °C 2.1: sodium carbonate / water; acetone / 20 °C 3.1: dicyclohexyl-carbodiimide / chloroform / 12 h / 20 °C 4.1: sodium carbonate / water; acetone / 20 °C 5.1: dicyclohexyl-carbodiimide / N,N-dimethyl-formamide 5.2: 20 °C 6.1: water; hydrogenchloride / water / 24 h / 20 °C View Scheme |
N-dodecanoyl-L-phenylalanine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: triethylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 20 °C 1.2: 17 h / 20 °C 2.1: lithium hydroxide / tetrahydrofuran; water; methanol / 20 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h 1.2: 17 h / 20 °C 2.1: lithium hydroxide; water / tetrahydrofuran; methanol / 20 h / 0 - 20 °C View Scheme |
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