The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry2-SEC-BUTYLCYCLOHEXANONE Basic information Product Name: 2-SEC-BUTYLCYCLOHEXANONE Synonyms: 2-(1-methylpropyl)-cyclohexanon;2-sec-butyl-cyclohexanon;Cyclohexanone, sec.-butyl, # 2;Cycloh
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiryAbout Our Group Since 1996 when our factory was put into production to year of 2020, our group has successively invested in more than 52 factories with shares and subordinates.We focus on manufacture Pharm & c
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Min.Order:10 Gram
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiry2-(1-METHYLPROPYL)CYCLOHEXANONE cas 14765-30-1Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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Raw material ,higher purity, support by origional factory, fully large stock Basic information Product Name: 2-SEC-BUTYLCYCLOHEXANONE Synonyms: 2-sec-Butylcyclohexanone (mixture of isomers);2-sec-Butylcyclohexanone 2-sec-Butylcyclohexanone
Cas:14765-30-1
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
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1. Physical State Liquid 2. Appearance clear, colorless to pale yellow 3. Odor Acetone or peppermint odor FeaturesCyclohexanone is…
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inquiryConditions | Yield |
---|---|
With N-benzylbenzenesulfonamide; mesitylcopper(I) In toluene at 0℃; for 6h; | 90% |
2,6-dibromocyclohexanone
2-sec-butylcyclohexanone
Conditions | Yield |
---|---|
In tetrahydrofuran at -78℃; |
2-(1-methylpropylidene)cyclohexanone
2-sec-butylcyclohexanone
Conditions | Yield |
---|---|
With hydrogen; palladium |
(Z)-2-Butene
lithium 1-cyclohexenolate
A
2-sec-butylcyclohexanone
B
2,6-di(sec-butyl)cyclohexanone
Conditions | Yield |
---|---|
Yield given. Multistep reaction. Yields of byproduct given; |
trans-2-Butene
lithium 1-cyclohexenolate
A
2-sec-butylcyclohexanone
B
2,6-di(sec-butyl)cyclohexanone
Conditions | Yield |
---|---|
Yield given. Multistep reaction. Yields of byproduct given; |
(E)-2-ethylidenecyclohexan-1-one
A
2-sec-butylcyclohexanone
Conditions | Yield |
---|---|
N-benzylbenzenesulfonamide; mesitylcopper(I) In toluene at 0℃; for 6h; Addition; | A 90 % Chromat. B n/a |
1-acetoxy-6-bromo-cyclohexene
2-sec-butylcyclohexanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Zn / tetrahydrofuran 2: H2 / Pd View Scheme |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In propan-1-ol for 2h; Reflux; | 100% |
2-sec-butylcyclohexanone
aniline
(-)-N-(phenyl)-[2-sec-butylcyclohexyl]amine
Conditions | Yield |
---|---|
Stage #1: 2-sec-butylcyclohexanone; aniline With [(R)-BINAP]PdBr2 In chloroform for 0.166667h; Inert atmosphere; Stage #2: With hydrogen In chloroform at 70℃; under 41372.9 Torr; for 24h; enantioselective reaction; | 80% |
Conditions | Yield |
---|---|
With iodine at 80℃; for 24h; Sealed tube; | 56% |
2-sec-butylcyclohexanone
4-methoxy-aniline
Conditions | Yield |
---|---|
With 2,2,6,6-tetramethyl-piperidine; trifluorormethanesulfonic acid; oxygen In m-xylene at 130℃; under 760.051 Torr; for 8h; Sealed tube; | 47% |
2-sec-butylcyclohexanone
dimethyl sulfoxide
Conditions | Yield |
---|---|
With iodine at 80℃; for 24h; Sealed tube; | 42% |
2-sec-butylcyclohexanone
Conditions | Yield |
---|---|
With pyridine; bis(trichloromethyl) carbonate In dichloromethane at 35℃; for 24h; | 34% |
2-sec-butylcyclohexanone
7-sec-butyl-oxepan-2-one
Conditions | Yield |
---|---|
With peracetic acid |
Methyl dimethoxyacetate
2-sec-butylcyclohexanone
2-sec-Butyl-6-(2,2-dimethoxy-acetyl)-cyclohexanone
Conditions | Yield |
---|---|
With n-butyllithium; diisopropylamine 1.) hexane, THF, -78 deg C, 45 min, 2.) hexane, THF, RT, overnight; Yield given. Multistep reaction; |
2-sec-butylcyclohexanone
7-sec-Butyl-2-(4-fluoro-phenyl)-4,5,6,7-tetrahydro-2H-indazole-3-carbaldehyde
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) diisopropylamine, n-BuLi / 1.) hexane, THF, -78 deg C, 45 min, 2.) hexane, THF, RT, overnight 2: 1.) Et3N, 2.) aq. HCl / 1.) EtOH, from RT to reflux, 2.) THF, reflux, 4 h View Scheme |
2-sec-butylcyclohexanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) diisopropylamine, n-BuLi / 1.) hexane, THF, -78 deg C, 45 min, 2.) hexane, THF, RT, overnight 2: 1.) Et3N, 2.) aq. HCl / 1.) EtOH, from RT to reflux, 2.) THF, reflux, 4 h View Scheme |
2-sec-butylcyclohexanone
(E)-3-[7-sec-Butyl-2-(4-fluoro-phenyl)-4,5,6,7-tetrahydro-2H-indazol-3-yl]-propenal
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 1.) diisopropylamine, n-BuLi / 1.) hexane, THF, -78 deg C, 45 min, 2.) hexane, THF, RT, overnight 2: 1.) Et3N, 2.) aq. HCl / 1.) EtOH, from RT to reflux, 2.) THF, reflux, 4 h 3: NaH / tetrahydrofuran / Ambient temperature 4: (i-Bu)2AlH / tetrahydrofuran; toluene / 0.5 h 5: MnO2 / benzene / 2 h / Heating View Scheme |
2-sec-butylcyclohexanone
(E)-3-[7-sec-Butyl-2-(4-fluoro-phenyl)-4,5,6,7-tetrahydro-2H-indazol-3-yl]-prop-2-en-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 1.) diisopropylamine, n-BuLi / 1.) hexane, THF, -78 deg C, 45 min, 2.) hexane, THF, RT, overnight 2: 1.) Et3N, 2.) aq. HCl / 1.) EtOH, from RT to reflux, 2.) THF, reflux, 4 h 3: NaH / tetrahydrofuran / Ambient temperature 4: (i-Bu)2AlH / tetrahydrofuran; toluene / 0.5 h View Scheme |
2-sec-butylcyclohexanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) diisopropylamine, n-BuLi / 1.) hexane, THF, -78 deg C, 45 min, 2.) hexane, THF, RT, overnight 2: Et3N / ethanol / 20 - 78 °C View Scheme |
2-sec-butylcyclohexanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) diisopropylamine, n-BuLi / 1.) hexane, THF, -78 deg C, 45 min, 2.) hexane, THF, RT, overnight 2: Et3N / ethanol / 20 - 78 °C View Scheme |
2-sec-butylcyclohexanone
(E)-3-[7-sec-Butyl-2-(4-fluoro-phenyl)-4,5,6,7-tetrahydro-2H-indazol-3-yl]-acrylic acid ethyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.) diisopropylamine, n-BuLi / 1.) hexane, THF, -78 deg C, 45 min, 2.) hexane, THF, RT, overnight 2: 1.) Et3N, 2.) aq. HCl / 1.) EtOH, from RT to reflux, 2.) THF, reflux, 4 h 3: NaH / tetrahydrofuran / Ambient temperature View Scheme |
2-sec-butylcyclohexanone
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: 1.) diisopropylamine, n-BuLi / 1.) hexane, THF, -78 deg C, 45 min, 2.) hexane, THF, RT, overnight 2: 1.) Et3N, 2.) aq. HCl / 1.) EtOH, from RT to reflux, 2.) THF, reflux, 4 h 3: NaH / tetrahydrofuran / Ambient temperature 4: (i-Bu)2AlH / tetrahydrofuran; toluene / 0.5 h 5: MnO2 / benzene / 2 h / Heating 6: tetrahydrofuran 7: 1.) Et3B, air, 2.) NaBH4 / 1.) MeOH, THF, 2 h, 2.) MeOH, THF, from -78 deg C to RT, overnight View Scheme |
2-sec-butylcyclohexanone
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 1.) diisopropylamine, n-BuLi / 1.) hexane, THF, -78 deg C, 45 min, 2.) hexane, THF, RT, overnight 2: 1.) Et3N, 2.) aq. HCl / 1.) EtOH, from RT to reflux, 2.) THF, reflux, 4 h 3: NaH / tetrahydrofuran / Ambient temperature 4: (i-Bu)2AlH / tetrahydrofuran; toluene / 0.5 h 5: MnO2 / benzene / 2 h / Heating 6: tetrahydrofuran View Scheme |
2-sec-butylcyclohexanone
Conditions | Yield |
---|---|
Multi-step reaction with 8 steps 1: 1.) diisopropylamine, n-BuLi / 1.) hexane, THF, -78 deg C, 45 min, 2.) hexane, THF, RT, overnight 2: 1.) Et3N, 2.) aq. HCl / 1.) EtOH, from RT to reflux, 2.) THF, reflux, 4 h 3: NaH / tetrahydrofuran / Ambient temperature 4: (i-Bu)2AlH / tetrahydrofuran; toluene / 0.5 h 5: MnO2 / benzene / 2 h / Heating 6: tetrahydrofuran 7: 1.) Et3B, air, 2.) NaBH4 / 1.) MeOH, THF, 2 h, 2.) MeOH, THF, from -78 deg C to RT, overnight 8: aq. NaOH / methanol / 1 h / 0 - 20 °C View Scheme |
2-sec-butylcyclohexanone
sulfuric acid
hexahydro-3-(1-methylpropyl)-1H-azepin-2-one
2-sec-butylcyclohexanone
ethyl 2-sec.butyl-cyclohexylideneacetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: toluene-4-sulfonic acid / propan-1-ol / 2 h / Reflux 2: propan-1-ol; toluene / 2 h / Reflux View Scheme |
2-sec-butylcyclohexanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium ethanolate / ethanol / 12 h / Reflux 2: hydrogenchloride / water / 2 h / 60 °C View Scheme |
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