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Cas:1484-84-0
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inquiryDayangChem exported this product to many countries and regions at best price in China. If you are looking for the product’s supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product specifica
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inquiry2-Piperidineethanol Basic information Product Name: 2-Piperidineethanol Synonyms: 2-(2-Piperidinyl)ethanol;PIPERIDINE-2-ETHANOL;LABOTEST-BB LTBB000546;2-(2-HYDROXYETHYL)PIPERIDINE;2-
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inquiry2-Piperidineethanol CAS No. 1484-84-0 Molecular Formula C7H15NO Appearance w
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Product name:2-Hydroxyethylpiperidine CAS No.:1484-84-0 Molecule Formula:C7H16NO Molecule Weight:130.21 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING IT
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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2-Piperidineethanol Chemical Properties Melting point 38-40 °C (lit.) Boiling point 234 °C (lit.) density 1.01 refractive index 1.4749 (estimate) Fp >230 °F storage temp. Keep in dark place,Sealed in dry,Room Te
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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Min.Order:1 Gram
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiry2-PiperidineethanolAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Conditions | Yield |
---|---|
With 1,4-dioxane; nickel at 160℃; under 191232 Torr; Hydrogenation; | |
With ethanol; nickel at 150℃; under 95616 Torr; Hydrogenation; | |
With acetic acid; platinum Hydrogenation; |
N-benzyl-2-(2-hydroxyethyl)piperidine
2(RS)-(2-hydroxyethyl)piperidine
Conditions | Yield |
---|---|
With palladium on activated charcoal; ammonium formate In methanol for 12h; Heating; Yield given; |
2(RS)-(2-hydroxyethyl)piperidine
Conditions | Yield |
---|---|
With ethanol; sodium |
2(RS)-(2-hydroxyethyl)piperidine
Conditions | Yield |
---|---|
With ethanol; sodium |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 30 percent / H2O2, sodium tungstate dihydrate / methanol / under 5 deg C, then Rt, 24 h 2: CH2Cl2 / 12 h / Heating 3: 94 percent / LiAlH4 / tetrahydrofuran / 0 deg C, then reflux, 3 h 4: ammonium formate, 10percent Pd/C / methanol / 12 h / Heating View Scheme |
2-isobutoxyhexahydroisoxazolo<2,3-a>-pyridine
2(RS)-(2-hydroxyethyl)piperidine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: CH2Cl2 / 12 h / Heating 2: 94 percent / LiAlH4 / tetrahydrofuran / 0 deg C, then reflux, 3 h 3: ammonium formate, 10percent Pd/C / methanol / 12 h / Heating View Scheme |
(2S,3aR)-8-Benzyl-2-isobutoxy-hexahydro-isoxazolo[2,3-a]pyridin-8-ium; bromide
2(RS)-(2-hydroxyethyl)piperidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 94 percent / LiAlH4 / tetrahydrofuran / 0 deg C, then reflux, 3 h 2: ammonium formate, 10percent Pd/C / methanol / 12 h / Heating View Scheme |
Conditions | Yield |
---|---|
pyridine |
2(RS)-(2-hydroxyethyl)piperidine
di-tert-butyl dicarbonate
tert-butyl 2-(2-hydroxyethyl)piperidine-1-carboxylate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 4h; | 100% |
With triethylamine In dichloromethane at 20℃; | 99% |
With sodium carbonate In dichloromethane; water at 20℃; for 24h; Inert atmosphere; | 98% |
2(RS)-(2-hydroxyethyl)piperidine
4-methoxy-2,6-dimethylbenzenesulfonyl chloride
C16H25NO4S
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; | 100% |
With triethylamine In dichloromethane at 0 - 20℃; | |
With triethylamine In dichloromethane at 0℃; for 1h; | |
With triethylamine In dichloromethane at 0 - 20℃; |
2(RS)-(2-hydroxyethyl)piperidine
S-tert-butoxycarbonyl-4,6-dimethyl-2-mercaptopyrimidine
tert-butyl 2-(2-hydroxyethyl)piperidine-1-carboxylate
Conditions | Yield |
---|---|
In chloroform | 99.9% |
In chloroform |
2(RS)-(2-hydroxyethyl)piperidine
benzyl chloroformate
2-(2-hydroxyethyl)-piperidine-1-carboxylic acid benzyl ester
Conditions | Yield |
---|---|
With potassium carbonate In ethanol; water at 0 - 20℃; for 3.25h; | 99% |
With sodium carbonate In dichloromethane for 1h; Ambient temperature; | 87% |
Stage #1: 2(RS)-(2-hydroxyethyl)piperidine With sodium hydrogencarbonate In dichloromethane at 20℃; Stage #2: benzyl chloroformate In dichloromethane at 0℃; for 1h; | 63% |
2(RS)-(2-hydroxyethyl)piperidine
carbonic acid dimethyl ester
hexahydro-3H-pyrido<1,2-c><1,3>oxazin-1-one
Conditions | Yield |
---|---|
With sodium methylate In methanol for 144h; Ambient temperature; | 98% |
2(RS)-(2-hydroxyethyl)piperidine
tert-butyldimethylsilyl chloride
2-<2-(tert-butyldimethylsiloxy)ethyl>piperidine
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; for 4h; | 98% |
With 1H-imidazole In dichloromethane at 20℃; for 4.5h; | 98% |
With 1H-imidazole In dichloromethane at 20℃; for 4h; | 90% |
With 1H-imidazole In dichloromethane Inert atmosphere; | 78% |
2(RS)-(2-hydroxyethyl)piperidine
PVS
2-[1-(2-benzenesulfonyl-ethyl)-piperidin-2-yl]-ethanol
Conditions | Yield |
---|---|
In xylene for 48h; Heating; | 95% |
2(RS)-(2-hydroxyethyl)piperidine
N-benzoyl-2-(2-hydroxyethyl)piperidine
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 12h; regioselective reaction; | 95% |
2(RS)-(2-hydroxyethyl)piperidine
2-chloro-6-methoxy-3-nitropyridine
Conditions | Yield |
---|---|
In ethanol for 2h; Heating / reflux; | 94.1% |
Conditions | Yield |
---|---|
94% |
2(RS)-(2-hydroxyethyl)piperidine
2-(2-Chloroethyl)piperidine Hydrochloride
Conditions | Yield |
---|---|
With thionyl chloride In chloroform for 2h; Heating; | 93% |
With thionyl chloride In dichloromethane for 12h; Reflux; | 89% |
With hydrogenchloride; chloroform Anschliessendes Erwaermen mit Thionylchlorid.; | |
With thionyl chloride In chloroform at 20℃; for 24h; Inert atmosphere; Cooling with ice; |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 18h; Acylation; | 93% |
With sodium hydroxide; triethylamine In tetrahydrofuran; ethanol; dichloromethane |
2(RS)-(2-hydroxyethyl)piperidine
N-(Benzyloxycarbonyloxy)succinimide
2-(2-hydroxyethyl)-piperidine-1-carboxylic acid benzyl ester
Conditions | Yield |
---|---|
In 1,4-dioxane; water at 25℃; for 24h; | 93% |
With triethylamine In dichloromethane at 23℃; for 18h; | 43% |
2(RS)-(2-hydroxyethyl)piperidine
3-bromo-2-isopropyl-5-methylthiophene-1,1-dioxide
2-[1-((2E,4Z)-4-Bromo-6-methyl-hepta-2,4-dienyl)-piperidin-2-yl]-ethanol
Conditions | Yield |
---|---|
In xylene at 116℃; for 7.5h; Product distribution; other amines; amine-induced ring-opening reaction of 2-alkyl-3-bromo-5-methylthiophene-1,1-dioxides; optimization and mechanistic considerations; kinetic study; deuterium incorporation experiments; kinetic isotope effect; | 91% |
In xylene at 116℃; for 7.5h; | 91% |
Conditions | Yield |
---|---|
In toluene at 20℃; for 1h; Addition; | 91% |
2(RS)-(2-hydroxyethyl)piperidine
aniline
N-(2-piperidin-2-yl-ethyl)-aniline
Conditions | Yield |
---|---|
With cesiumhydroxide monohydrate; oxygen In 1,3,5-trimethyl-benzene at 180℃; for 24h; | 88% |
2(RS)-(2-hydroxyethyl)piperidine
pivaloyl chloride
2-(2-Hydroxyethyl)-1-(2,2-dimethylpropanoyl)piperidine
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 18h; Acylation; | 87% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 18h; Carboxylation; | 85% |
2(RS)-(2-hydroxyethyl)piperidine
9-fluorenylmethyl N-succinimidyl carbonate
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 0.5h; | 85% |
2(RS)-(2-hydroxyethyl)piperidine
Bis-(dimethylamino)-phenylboran
2-phenyl-1,3,2-oxazaborabicyclo[4.4.0]decane
Conditions | Yield |
---|---|
In benzene byproducts: MeNH2; absence of air; refluxing (5 h); solvent removal, distn.; elem. anal.; | 85% |
Conditions | Yield |
---|---|
With sodium hydroxide In toluene at 20℃; for 2h; Carboxylation; | 84% |
Conditions | Yield |
---|---|
In tetrahydrofuran for 15h; Heating / reflux; | 84% |
2(RS)-(2-hydroxyethyl)piperidine
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 60 - 80℃; | 84% |
2(RS)-(2-hydroxyethyl)piperidine
2-(piperidin-2-yl)acetic acid
Conditions | Yield |
---|---|
Stage #1: 2(RS)-(2-hydroxyethyl)piperidine With chromium(VI) oxide; sulfuric acid In water at 0 - 20℃; for 4.5h; Stage #2: With barium dihydroxide In water Stage #3: With carbon dioxide In water | 83% |
Stage #1: 2(RS)-(2-hydroxyethyl)piperidine With hydrogenchloride; sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide In water; ethyl acetate at 5 - 20℃; for 0.833333h; pH=8.0 - 9.0; Stage #2: With hydrogenchloride; sodium chlorite In water; ethyl acetate at 20 - 33℃; for 16.5h; pH=5.0; | 78% |
With chromium(VI) oxide; sulfuric acid at 0 - 20℃; for 15.25h; Jones oxidation; | 68% |
2(RS)-(2-hydroxyethyl)piperidine
2,6-dichlorobenzaldehyde
α-(2,6-dichlorophenyl)-2-(2-hydroxyethyl)-1-piperidineacetonitrile
Conditions | Yield |
---|---|
With potassium cyanide In hydrogenchloride | 83% |
2(RS)-(2-hydroxyethyl)piperidine
benzoyl chloride
A
N-benzoyl-2-(2-hydroxyethyl)piperidine
Conditions | Yield |
---|---|
With di(n-butyl)tin oxide; triethylamine In toluene for 0.15h; Irradiation; | A 82% B 11% |
With di(n-butyl)tin oxide; triethylamine In toluene for 0.15h; Irradiation; | A 76% B 19% |
With triethylamine In tetrahydrofuran for 48h; |
2(RS)-(2-hydroxyethyl)piperidine
tert-butyl 2-(2-hydroxyethyl)piperidine-1-carboxylate
Conditions | Yield |
---|---|
82% |
Conditions | Yield |
---|---|
With hydrogen bromide In water for 24h; Reflux; | 82% |
With hydrogen bromide In water Reflux; |
2(RS)-(2-hydroxyethyl)piperidine
Conditions | Yield |
---|---|
With potassium fluoride In 1-methyl-pyrrolidin-2-one Heating; | 81% |
Conditions | Yield |
---|---|
80% |
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