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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

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Cas:15709-74-7

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

BROMOTRIS(TRIPHENYLPHOSPHINE)COPPER(I)&

Cas:15709-74-7

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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine chemicals, ph

Bromotris(triphenylphosphine)copper(I)

Cas:15709-74-7

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Qingdao Beluga Import and Export Co., LTD

BROMOTRIS(TRIPHENYLPHOSPHINE)COPPER(I)& CAS:15709-74-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in hi

BROMOTRIS(TRIPHENYLPHOSPHINE)COPPER(I)& CAS:15709-74-7

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Copper,bromotris(triphenylphosphine)-, (T-4)-

Cas:15709-74-7

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:15709-74-7

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Copper,bromotris(triphenylphosphine)-, (T-4)-

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Bromotris(triphenylphosphine)copper

Cas:15709-74-7

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Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

15709-74-7

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Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

Bromotris(triphenylphosphine)copper(I) Cas no.15709-74-7 98%

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Hebei Mojin Biotechnology Co.,Ltd

1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification

Copper,bromotris(triphenylphosphine)-, (T-4)-

Cas:15709-74-7

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Xi`an Eastling Biotech Co., Ltd.

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou

BROMOTRIS(TRIPHENYLPHOSPHINE)COPPER(I)&

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Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

Copper,bromotris(triphenylphosphine)-, (T-4)-

Cas:15709-74-7

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Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

BROMOTRIS(TRIPHENYLPHOSPHINE)COPPER(I)&

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Copper,bromotris(triphenylphosphine)-, (T-4)-

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Guangdong Juda Chemical Industrial Co.,Limited

Appearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China

Bromocopper - triphenylphosphine (1:3) CAS No.15709-74-7

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DB BIOTECH CO., LTD

best seller Application:API

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BOC Sciences

We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white to yellow powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as

BROMOTRIS(TRIPHENYLPHOSPHINE)COPPER(I)

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Hangzhou Fandachem Co.,Ltd

tris(triphenylphosphane)copper(I) bromideAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express

tris(triphenylphosphane)copper(I) bromide

Cas:15709-74-7

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Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

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Asure Biochem CO.,LTD.

*stable and better quality products*efficient and meticulous servicesAppearance:Powder Storage:Store in dry, cool and ventilated place Package:10G/bottle 1kg/tin 5kg/tin 25kg/carton Application:1. Chemical raw materials 2. Used as an analytical reage

Bromotris(triphenylphosphine)copper(I)

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Shanghai Chinqesen Biotechnology Co., Ltd.

Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

15709-74-7

Cas:15709-74-7

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Hebei Muhuang Technology Co., Ltd

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BROMOTRIS(TRIPHENYLPHOSPHINE)COPPER(I)&

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Chemsigma International Co.,Ltd.

bulk?production Application:Pharmaceutical intermediates

BROMOTRIS(TRIPHENYLPHOSPHINE)COPPER(I)&

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ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

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HWRK Chem

in store Package:10g Application:Organic Chemicals

BROMOTRIS(TRIPHENYLPHOSPHINE)COPPER(I)

Cas:15709-74-7

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Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

Copper,bromotris(triphenylphosphine)-, (T-4)-

Cas:15709-74-7

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Hubei Jusheng Technology Co., Ltd.,

1, High quality with competitive price: We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcels can be sent out within 24 hours after payment. Tracking number is available. 2)

Bromotris(triphenylphosphine)copper/high quality/best price

Cas:15709-74-7

Min.Order:10 Gram

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Jilin haofei import and export trade Co.,Ltd

Price, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right

BROMOTRIS(TRIPHENYLPHOSPHINE)COPPER(I) CAS NO.15709-74-7

Cas:15709-74-7

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HuBei Ipure Biotech CO.,ltd

HuBei ipure is a diversified product production and operation enterprise, with API, pharma intermediates, and other fine chemicals as well as R&D and pigments development and sales as one of the large enterprises, with more than 130 acres of pl

Bromotris(triphenylphosphine)copper/high quality/best price

Cas:15709-74-7

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Synthetic route

triphenylphosphine
603-35-0

triphenylphosphine

copper(ll) bromide
7789-45-9

copper(ll) bromide

bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

Conditions
ConditionsYield
In methanol for 0.5h; Heating / reflux;93%
In methanol for 0.5h; Heating / reflux;93%
In acetone to soln. of bromide in hot acetone soln. of triphenylphosphine in hot acetone added dropwise with stirring, refluxed for several h; filterd, washed with petroleum ether, dried for several h in vac.; elem.anal.;34%
triphenylphosphine
603-35-0

triphenylphosphine

copper(I) bromide
7787-70-4

copper(I) bromide

bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

Conditions
ConditionsYield
In methanol for 4 - 5h;90%
In methanol for 0.5h; Reflux;87%
In acetonitrile at 80℃; for 1h; Inert atmosphere;71%
In chloroform pptd. from CHCl3 soln. of stoich. amt. of CuBr and PPh3; according to P.F. Barron et al., J. Chem. Soc., Dalton Trans., 1987, 1099 and G. Costa , E. Reisenhofer and L. Stefani, J. Inorg. Nucl. Chem., 1965, 27, 2581;
In methanol at 60℃; for 0.166667h;1.18 g
BrCu*(x)H2O

BrCu*(x)H2O

bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

Conditions
ConditionsYield
With triphenylphosphine In methanol copper halogenide : triphenylphosphine = 1 : 3.5, intensive stirring; suction and drying in high vac., elem. anal.;
copper(I) bromide
7787-70-4

copper(I) bromide

bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

Conditions
ConditionsYield
With triphenylphosphine In dichloromethane stoich. amts. Ph3P and CuBr mixed in small volume methylene chloride; pentane, hexane or cyclohexane added until ppt. began to form, soln. cooled in ice bath and allowed to stand for a few minutes and filtered;
With triphenyl phosphine In chloroform Stoicheiometric quantities of reagents were refluxed for 2-4 h in CHCl3;; the hot soln. was filtered, slow cooling and evapd.;;
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

3-phenyl-2-thioxoimidazolidin-4-one
2010-15-3

3-phenyl-2-thioxoimidazolidin-4-one

{Cu(P(C6H5)3)2(C6H5NC(O)CH2NHC(S))Br}
144886-62-4

{Cu(P(C6H5)3)2(C6H5NC(O)CH2NHC(S))Br}

Conditions
ConditionsYield
In benzene byproducts: triphenylphosphine; addn. of ligand to Cu complex soln.; refluxing, 2h; cooling; filtration; evapn. to half the volume; addn. of petroleum ether; standing, 2-3h; pptn.; centrifuging; washing (petroleum ether); drying (vac.); elem. anal.;96%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

bis(1,2,4-triazol-1-yl)methane
63400-51-1

bis(1,2,4-triazol-1-yl)methane

[(P(C6H5)3)Cu(C5H6N6)Br]
166662-57-3

[(P(C6H5)3)Cu(C5H6N6)Br]

Conditions
ConditionsYield
In acetone byproducts: Ph3P; stirring; elem. anal.;96%
N-phenyl-1-morpholinethiocarbamide
15093-54-6

N-phenyl-1-morpholinethiocarbamide

bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

{Cu(P(C6H5)3)2(C6H5NHC(S)N(CH2CH2)2O)Br}
144886-68-0

{Cu(P(C6H5)3)2(C6H5NHC(S)N(CH2CH2)2O)Br}

Conditions
ConditionsYield
In benzene byproducts: triphenylphosphine; addn. of ligand to Cu complex soln.; refluxing, 2h; cooling; filtration; evapn. to half the volume; addn. of petroleum ether; standing, 2-3h; pptn.; centrifuging; washing (petroleum ether); drying (vac.); elem. anal.;90%
1,10-Phenanthroline
66-71-7

1,10-Phenanthroline

bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

(1,10-phenanthroline)(triphenylphosphine)CuBr
25753-84-8

(1,10-phenanthroline)(triphenylphosphine)CuBr

Conditions
ConditionsYield
In chloroform90%
In chloroform at 20℃; for 0.166667h;90%
In chloroform at 20℃; for 0.5h;75%
In chloroform at 20℃; for 0.5h;75%
In dichloromethane for 2h; Inert atmosphere;
1,6-naphthyridine
253-72-5

1,6-naphthyridine

bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

[CuBr(PPh3)2(4-Mepy)]

[CuBr(PPh3)2(4-Mepy)]

Conditions
ConditionsYield
In chloroform89%
NH-pyrazole
288-13-1

NH-pyrazole

bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

[(P(C6H5)3)2Cu(C3H4N2)Br]
166662-78-8

[(P(C6H5)3)2Cu(C3H4N2)Br]

Conditions
ConditionsYield
In diethyl ether byproducts: Ph3P; stirring (6 h); elem. anal.;88%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

bis(pyrazol-1-yl)methane
27258-04-4

bis(pyrazol-1-yl)methane

[(P(C6H5)3)Cu(C7H8N4)Br]
166662-56-2

[(P(C6H5)3)Cu(C7H8N4)Br]

Conditions
ConditionsYield
In diethyl ether byproducts: Ph3P; stirring (6 h); elem. anal.;87%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

N,N-dimethyl-N'-phenylthiourea
705-62-4

N,N-dimethyl-N'-phenylthiourea

{Cu(P(C6H5)3)2(C6H5NHC(S)N(CH3)2)Br}
144749-75-7

{Cu(P(C6H5)3)2(C6H5NHC(S)N(CH3)2)Br}

Conditions
ConditionsYield
In benzene slow addn. of ligand soln. to soln. of Cu-complex, refluxing (2 h); concg. in vac., addn. of petroleum ether (60-80°C), standing (2-3 h), centrifugation, washing (petroleum ether), drying in vac., elem. anal.;86%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

1,1-dibutyl-3-phenylthiourea
15093-47-7

1,1-dibutyl-3-phenylthiourea

bromo(N,N-dibutyl-N'-phenylthiourea-S)bis(triphenylphosphine-P)copper(I)
144749-78-0

bromo(N,N-dibutyl-N'-phenylthiourea-S)bis(triphenylphosphine-P)copper(I)

Conditions
ConditionsYield
In benzene slow addn. of ligand soln. to soln. of Cu-complex, refluxing (2 h); concg. in vac., addn. of petroleum ether (60-80°C), standing (2-3 h), centrifugation, washing (petroleum ether), drying in vac., elem. anal.;86%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

1-Phenyl-1H-tetrazole-5-thiol
86-93-1

1-Phenyl-1H-tetrazole-5-thiol

CuBr(triphenylphosphane)2(1-phenyl-1H-tetrazole-5(4H)-thione)
144886-65-7

CuBr(triphenylphosphane)2(1-phenyl-1H-tetrazole-5(4H)-thione)

Conditions
ConditionsYield
In benzene byproducts: triphenylphosphine; addn. of ligand to Cu complex soln.; refluxing, 2h; cooling; filtration; evapn. to half the volume; addn. of petroleum ether; standing, 2-3h; pptn.; centrifuging; washing (petroleum ether); drying (vac.); elem. anal.;85%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

diethyl (1,10-phenanthrolin-4-yl)phosphonate
1422766-85-5

diethyl (1,10-phenanthrolin-4-yl)phosphonate

CuI(diethyl (1,10-phenanthrolin-4-yl)phosphonate)(triphenylphosphine)bromide

CuI(diethyl (1,10-phenanthrolin-4-yl)phosphonate)(triphenylphosphine)bromide

Conditions
ConditionsYield
In chloroform at 20℃; for 0.166667h;82%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

N-[(5-chloro-2-nitrophenyl)carbamothioyl]pentanamide

N-[(5-chloro-2-nitrophenyl)carbamothioyl]pentanamide

{N-[(5-chloro-2-nitrophenyl)carbamothioyl]pentanamide}[bis(triphenylphosphine)]copper(I) bromide

{N-[(5-chloro-2-nitrophenyl)carbamothioyl]pentanamide}[bis(triphenylphosphine)]copper(I) bromide

Conditions
ConditionsYield
In methanol; dichloromethane for 5 - 6h;79%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

N-[(4-methyl-2-nitrophenyl)carbamothioyl]butanamide

N-[(4-methyl-2-nitrophenyl)carbamothioyl]butanamide

{N-[(4-methyl-2-nitrophenyl)carbamothioyl]-butanamide}[bis(triphenylphosphine)]copper(I)bromide

{N-[(4-methyl-2-nitrophenyl)carbamothioyl]-butanamide}[bis(triphenylphosphine)]copper(I)bromide

Conditions
ConditionsYield
In methanol; dichloromethane for 5 - 6h;78%
thiazolidine-2-thione
134469-06-0

thiazolidine-2-thione

bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

copper(I)(1,3-thiazolidine-2-thione)-bis(triphenylphosphine) bromide
122201-83-6

copper(I)(1,3-thiazolidine-2-thione)-bis(triphenylphosphine) bromide

Conditions
ConditionsYield
In benzene slow addn. of ligand soln. to soln. of Cu-complex, refluxing (2 h); concg. in vac., addn. of petroleum ether (60-80°C), standing (2-3 h), centrifugation, washing (petroleum ether), drying in vac., elem. anal.;77%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

diethyl (1,10-phenanthrolin-5-yl)phosphonate
1422766-81-1

diethyl (1,10-phenanthrolin-5-yl)phosphonate

C34H32BrCuN2O3P2

C34H32BrCuN2O3P2

Conditions
ConditionsYield
In chloroform at 20℃; for 0.166667h;77%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

diethyl (1,10-phenanthrolin-5-yl)phosphonate
1422766-81-1

diethyl (1,10-phenanthrolin-5-yl)phosphonate

CuI(diethyl (1,10-phenanthrolin-5-yl)phosphonate)(triphenylphosphine)bromide

CuI(diethyl (1,10-phenanthrolin-5-yl)phosphonate)(triphenylphosphine)bromide

Conditions
ConditionsYield
In chloroform at 20℃; for 0.166667h;77%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

N-[(2-chloro-4-nitrophenyl)carbamothioyl]pentanamide

N-[(2-chloro-4-nitrophenyl)carbamothioyl]pentanamide

{N-[(2-chloro-4-nitrophenyl)carbamothioyl]pentanamide}[bis(triphenylphosphine)]copper(I) bromide

{N-[(2-chloro-4-nitrophenyl)carbamothioyl]pentanamide}[bis(triphenylphosphine)]copper(I) bromide

Conditions
ConditionsYield
In methanol; dichloromethane for 5 - 6h;77%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

N-[(2-bromophenyl)carbamothioyl]pentanamide

N-[(2-bromophenyl)carbamothioyl]pentanamide

{N-[(2-bromophenyl)carbamothioyl]pentanamide}-[bis(triphenylphosphine)]copper(I) bromide

{N-[(2-bromophenyl)carbamothioyl]pentanamide}-[bis(triphenylphosphine)]copper(I) bromide

Conditions
ConditionsYield
In methanol; dichloromethane for 5 - 6h;75%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

acetylthiourea
591-08-2

acetylthiourea

bromidoacetylthioureabis(triphenylphosphine)copper(I)

bromidoacetylthioureabis(triphenylphosphine)copper(I)

Conditions
ConditionsYield
In methanol; chloroform at 60℃; for 1h;74%
imidazole-2-thione
872-35-5

imidazole-2-thione

bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

(triphenylphosphine)2(imidazoline-2(1,3H)-thione)(bromo)copper(I)
242486-22-2

(triphenylphosphine)2(imidazoline-2(1,3H)-thione)(bromo)copper(I)

Conditions
ConditionsYield
In diethyl ether N2-atmosphere; 2 equivs. of ligand, stirring for 3 h; collection (filtration), washing (Et2O); elem. anal.;71%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

dichloromethane
75-09-2

dichloromethane

(Bu4N)2[Sn3S4(thioglycolate)3]

(Bu4N)2[Sn3S4(thioglycolate)3]

water
7732-18-5

water

[(Ph3P)2Cu]2SnS(dithioglycolate)2*2dichloromethane*water

[(Ph3P)2Cu]2SnS(dithioglycolate)2*2dichloromethane*water

Conditions
ConditionsYield
In dichloromethane addn. of CH2Cl2 to 1:1 mixt. of copper compd. and tin compd., heating for 5 min; filtration, keeping in air for 3 ds, isolation of crystals, washing withdiethyl ether, drying in air, elem. anal.;69.4%
[2,2]bipyridinyl
366-18-7

[2,2]bipyridinyl

bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

(triphenylphosphine)(2,2'-bipyridine)copper(I) bromide
25753-81-5

(triphenylphosphine)(2,2'-bipyridine)copper(I) bromide

Conditions
ConditionsYield
In chloroform at 20℃; for 0.5h;68%
In chloroform at 20℃; for 0.5h;68%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

ethyl N-(4-bromobenzenecarbothioyl)carbamate
57774-75-1

ethyl N-(4-bromobenzenecarbothioyl)carbamate

[CuBr(N-carboethoxy-4-bromobenzene thioamide)(PPh3)2]
505058-73-1

[CuBr(N-carboethoxy-4-bromobenzene thioamide)(PPh3)2]

Conditions
ConditionsYield
In benzene byproducts: PPh3; soln. N-carboethoxy-4-bromobenzene thioamide (benzene), soln. CuBr(PPh3)3 (benzene); mixed at 25°C; heated under reflux for 0.5 to 1 h; concd. to half volume under reduced pressure; addition of petroleum ether (60-80°C); stand for 2-3 h; filtered;washed several times (petroleum ether); dried in vac.; elem. anal.;67%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

diethyl (1,10-phenanthrolin-3-yl)phosphonate
1422766-84-4

diethyl (1,10-phenanthrolin-3-yl)phosphonate

CuI(diethyl (1,10-phenanthrolin-3-yl)phosphonate)(triphenylphosphine) bromide

CuI(diethyl (1,10-phenanthrolin-3-yl)phosphonate)(triphenylphosphine) bromide

Conditions
ConditionsYield
In chloroform at 20℃; for 0.166667h;67%
bromotris(triphenylphosphine)copper(I)
15709-74-7

bromotris(triphenylphosphine)copper(I)

diethyl (1,10-phenanthrolin-4-yl)phosphonate
1422766-85-5

diethyl (1,10-phenanthrolin-4-yl)phosphonate

C34H32BrCuN2O3P2

C34H32BrCuN2O3P2

Conditions
ConditionsYield
In chloroform at 20℃; for 0.166667h;67%

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