As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryP,P'-DIOCTYLDIPHENYLAMINE Chemical Properties Boiling point 476.5±34.0 °C(Predicted) density 0.935±0.06 g/cm3(Predicted) storage temp. Keep in dark place,Inert atmosphere,Room temperature pka 2.00±0.50(Pred
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inquiryP,P'-DIOCTYLDIPHENYLAMINE CAS:15721-78-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality or
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inquiryStock products, own laboratoryAppearance:White to off-white crystal powder Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquirybest price high quality Storage:Room Temperature Application:For pharmacy chemicals Transportation:by sea,air
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inquirygood quality, competitive price, thoughtful after sale serviceAppearance:White to Off-White Solid Storage:Keep it in dry,shady and cool place Package:as your requirement Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by Sea
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inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white crystals powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as
Benzenamine,4-(1,1,3,3-tetramethylbutyl)-N-[4-(1,1,3,3-tetramethylbutyl)phenyl]-Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquirygood quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:1g Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by express or by sea Port:Any port
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Our mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical
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inquirydi[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
4,4'-di-tert-octyldiphenylnitrosoamine
Conditions | Yield |
---|---|
With hydrogenchloride; sodium nitrite In ethanol; isopropyl alcohol at 0 - 5℃; for 1h; | 90% |
Conditions | Yield |
---|---|
With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine In toluene at 80℃; for 24h; Buchwald Reaction; | 88% |
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
3,7-di-tert-octyl-phenothiazine
Conditions | Yield |
---|---|
With sulfur at 480 - 500℃; Inert atmosphere; | 78% |
With iodine; sulfur |
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
N-(2,6-diisopropylphen-yl)-9-bromo-perylene-3,4-dicarboximide
N-(2,6-diisopropylphenyl)-9-[bis(4-tert-octyl)phenyl]aminoperylene-3,4-dicarboximide
Conditions | Yield |
---|---|
With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine In toluene at 80℃; for 24h; Buchwald Reaction; | 77% |
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In toluene at 100℃; Inert atmosphere; | 75% |
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; copper diacetate; potassium carbonate In acetonitrile at 120℃; for 12h; Schlenk technique; Inert atmosphere; | 74% |
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In toluene at 100℃; Inert atmosphere; | 73% |
iodobenzene
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
N,N-bis(4-(2,4,4-trimethylpentan-2-yl)phenyl)aniline
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene for 12h; Buchwald-Hartwig reaction; Inert atmosphere; Reflux; | 65% |
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In toluene at 100℃; for 16h; Inert atmosphere; | 64% |
2-bromothiophene
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
2-(N,N-bis(4-tert-octylphenyl)amino)thiophene
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene for 16h; Reflux; | 62% |
N-(2,6-diisopropylphenyl)-1,6,9,14-tetra[4-(1,1,3,3-tetramethyl-butyl)phenoxy]-11-bromo-terrylene-3,4-dicarboxylic acid imide
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
N-(2,6-diisopropylphenyl)-1,6,9,14-tetra[(4-tert-octyl)phenoxy]-9-[bis(4-tert-octyl)phenyl]aminoterrylene-3,4-dicarboximide
Conditions | Yield |
---|---|
With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine In toluene at 80℃; for 16h; Buchwald Reaction; | 61% |
1.4-dibromobenzene
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
4-bromo-N,N-bis(4-(2,4,4-trimethylpentan-2-yl)phenyl)aniline
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; sodium t-butanolate In toluene at 120℃; for 7h; Inert atmosphere; | 60% |
With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In toluene at 90℃; for 72h; | 36% |
4-Fluoronitrobenzene
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
4-nitro-N,N-bis(4-(2,4,4-trimethylpentan-2-yl)phenyl)aniline
Conditions | Yield |
---|---|
With sodium hydride In dimethyl sulfoxide at 120℃; for 48h; Inert atmosphere; | 60% |
ethyl 2-bromoisobutyrate
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; copper diacetate; potassium carbonate In acetonitrile at 120℃; for 12h; Schlenk technique; Inert atmosphere; | 59% |
para-nitrophenyl bromide
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
4-nitro-N,N-bis(4-(2,4,4-trimethylpentan-2-yl)phenyl)aniline
Conditions | Yield |
---|---|
With sodium t-butanolate; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0) at 20 - 90℃; for 16h; | 45% |
9,10-dibromo-1,6,7,12-tetrachloro-3,4-perylenedicarboxylic acid anhydride
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
Conditions | Yield |
---|---|
Stage #1: 9,10-dibromo-1,6,7,12-tetrachloro-3,4-perylenedicarboxylic acid anhydride; di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine With palladium diacetate; sodium t-butanolate; tricyclohexylphosphine In toluene at 100℃; for 24h; Inert atmosphere; Stage #2: With acetic acid In dichloromethane at 70℃; | 38% |
4-[bis-(4-iodophenyl)amino]benzaldehyde
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
Conditions | Yield |
---|---|
With 18-crown-6 ether; copper; potassium carbonate In 1,2-dichloro-benzene for 48h; Reflux; Inert atmosphere; | 34% |
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
methyl iodide
Conditions | Yield |
---|---|
Stage #1: di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine With sodium hydride In tetrahydrofuran for 1.5h; Stage #2: methyl iodide In tetrahydrofuran for 16h; | 32% |
6,7-dibromo-1H,3H-naphtho<1,8-cd>pyran-1,3-dione
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
Conditions | Yield |
---|---|
Stage #1: 6,7-dibromo-1H,3H-naphtho<1,8-cd>pyran-1,3-dione; di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 90℃; Inert atmosphere; Stage #2: With acetic anhydride; acetic acid In dichloromethane at 20℃; | 25% |
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
5,8,12-tribromo-2-(2,6-diisopropylphenyl)-1H-benzo[5,10]anthra[2,1,9-def]isoquinoline-1,3(2H)-dione
C118H150N4O2
Conditions | Yield |
---|---|
With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine In toluene at 80℃; for 48h; Buchwald Reaction; | 10% |
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
Conditions | Yield |
---|---|
With potassium hydroxide; 18-crown-6 ether; oxygen In dimethyl sulfoxide at 25℃; Product distribution; base-catalysed oxidation of secondary amines, possible mechanism, paramagnetic and diamagnetic oxidation products, ESR and GC-MS study; |
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 90 percent / sodium nitrite, aq. HCl / propan-2-ol; ethanol / 1 h / 0 - 5 °C 2: Zn, AcOH / propan-2-ol / 3.5 h / 20 - 25 °C View Scheme |
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
2,2-di-(4-tert-octylphenyl)picrylhydrazine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 90 percent / sodium nitrite, aq. HCl / propan-2-ol; ethanol / 1 h / 0 - 5 °C 2: Zn, AcOH / propan-2-ol / 3.5 h / 20 - 25 °C 3: sodium bicarbonate / propan-2-ol / 0.5 h / Heating View Scheme |
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
2,2-di(4-tert-octylphenyl)-1-picrylhydrazyl, free radical
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 90 percent / sodium nitrite, aq. HCl / propan-2-ol; ethanol / 1 h / 0 - 5 °C 2: Zn, AcOH / propan-2-ol / 3.5 h / 20 - 25 °C 3: sodium bicarbonate / propan-2-ol / 0.5 h / Heating 4: 74 percent / PbO2, Na2SO4 / CHCl3 / 1 h / 25 °C View Scheme |
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: iodine; sulfur 2: aqueous H2O2; acetic acid View Scheme |
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
N,N-bis(4-bromophenyl)-N',N'-bis(4-(2,4,4-trimethylpentan-2-yl)phenyl)-1,4-phenylenediamine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium hydride / dimethyl sulfoxide / 48 h / 120 °C / Inert atmosphere 2: palladium 10% on activated carbon; hydrazine hydrate / ethanol / Inert atmosphere; Reflux 3: 1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate / toluene / 6 h / Inert atmosphere; Reflux View Scheme |
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: tri-tert-butyl phosphine; sodium t-butanolate; palladium diacetate / toluene / 16 h / Reflux 2.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 - 20 °C 2.2: 16.5 h / -78 - 20 °C View Scheme |
N-(1'-ethylpropyl)-8-bromo-10-(bis(4-(2,4,4-trimethylpentane-2-yl)phenyl)amino)perylene-3,4-dicarboximide
di[p-(2,4,4-trimethyl-2-pentyl)phenyl]amine
N-(1'-ethylpropyl)-9,11-bis(bis(4-(2,4,4-trimethylpentane-2-yl)phenyl)amino)perylene-3,4-dicarboximide
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 80℃; Inert atmosphere; | 40 mg |
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 80℃; Inert atmosphere; | 40 mg |
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