Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:158063-66-2
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 4-(Trifluoromethyl)nicotinic acid CAS No.
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inquiry4-(Trifluoromethyl)nicotinic acid Basic information Product Name: 4-(Trifluoromethyl)nicotinic acid Synonyms: BUTTPARK 43\57-42;4-(TRIFLUOROMETHYL)NICOTINIC ACID;4-
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:158063-66-2
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inquiryOur advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can be sent
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct Name: 4-(Trifluoromethyl)nicotinic acid Synonyms: 4-(TrifluoroMethyl)-3-Pyridinecarboxylic Acid;3-Pyridinecarboxylic acid, 4-(trifluoromethyl)-;4-(Trifluoromethyl)pyridine-3-carboxy
Cas:158063-66-2
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inquiry1. Best prices with satisfied quality; 2. It's clients' right to choose the package's Courier (EMS, DHL, FedEx, UPS); 3.It's clients' right to choose the packing way for his produccts from many recent effective packing ways;
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryProduct Name: 4-(Trifluoromethyl)nicotinic acid CAS: 158063-66-2 MF: C7H4F3NO2 MW: 191.11 EINECS: 623-902-1 Mol File: 158063-66-2.mol 4-(Trifluoromethyl)nicotinic acid Structure 4-(Trifluoromethyl)nicotinic acid Chemical Propertie
Cas:158063-66-2
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inquiry4-(Trifluoromethyl)nicotinic acid CAS:158063-66-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quali
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inquiry4-(Trifluoromethyl)nicotinic acid CAS: 158063-66-2 Specification Product Name 4-(Trifluoromethyl)nicotinic acid CAS No. 158063-66-2 Appearance solid
Cas:158063-66-2
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Appearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By
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inquiryOur advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquirylow price high quality high purity good sevice stock Appearance:white Storage:Preserve In Well-Closed, Light-Resistant and Tight Containers. Store In Cool & Dry Place Package:1g,5g,10g...1kg,5kg...more Application:Pharmaceutical intermediat
Cas:158063-66-2
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:158063-66-2
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung, LG, Merck, Thermo Fisher Scientific and so o
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:158063-66-2
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryWe Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:158063-66-2
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inquiry4-trifluoromethyl-3-pyridinecarboxamide
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
With sodium hydroxide In water at 100℃; for 4h; Concentration; | 99.1% |
Stage #1: 4-trifluoromethyl-3-pyridinecarboxamide With hydrogenchloride; water for 5h; Heating / reflux; Stage #2: With sodium carbonate In water pH=3; | 89.7% |
With sodium hydroxide at 100℃; for 5h; |
4-(trifluoromethyl)nicotinonitrile
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
With water; sodium hydroxide at 100℃; Temperature; | 98.3% |
With sodium hydroxide In ethanol at 80℃; for 10h; Temperature; Inert atmosphere; | 90.1% |
Stage #1: 4-(trifluoromethyl)nicotinonitrile With potassium hydroxide; water In water; ethylene glycol at 200℃; for 4h; Stage #2: With hydrogenchloride In water; ethylene glycol at 20℃; | 84% |
With sulfuric acid In water at 110℃; for 12h; |
2-chloro-4-(trifluoromethyl)pyridine-3-carboxylic acid
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
With ammonium formate; 10% palladium on active carbon In methanol at 25℃; for 0.25h; | 89% |
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
Stage #1: N-(2-methoxycarbonylvinyl)-4,4,4-trifluoro-3-oxo-1-butenamine With sodium methylate In methanol at 20 - 65℃; for 7h; Inert atmosphere; Stage #2: With water at 20℃; for 12h; | 86.2% |
Stage #1: N-(2-methoxycarbonylvinyl)-4,4,4-trifluoro-3-oxo-1-butenamine With sodium methylate In methanol for 6.5h; Reflux; Stage #2: With water; sodium hydroxide In methanol at 50℃; Time; | 75% |
With sodium methylate In methanol at 20℃; for 6.5h; Time; Reflux; |
4-trifluoromethylpyridine
carbon dioxide
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
With 2,2,6,6-tetramethylpiperidinyl-lithium In tetrahydrofuran at -75℃; for 2h; | 84% |
carbon dioxide
3-iodo-4-(trifluoromethyl)pyridine
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane at -75℃; for 0.0333333h; | 81% |
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; diethyl ether; water | 77% |
dimethyl (methoxymethylene)malonate
4-amino-1,1,1-trifluoro-3-butene-2-one
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
Stage #1: 4-amino-1,1,1-trifluoro-3-butene-2-one With sodium hydride In 1-methyl-pyrrolidin-2-one at 0 - 10℃; for 1h; Stage #2: dimethyl (methoxymethylene)malonate In 1-methyl-pyrrolidin-2-one; methanol at 65℃; for 7h; Stage #3: With hydrogenchloride In 1-methyl-pyrrolidin-2-one; methanol; water for 9h; Reagent/catalyst; Solvent; Temperature; Reflux; | 49% |
3-methoxy-2-propenenitrile
4-amino-1,1,1-trifluoro-3-butene-2-one
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
Stage #1: 3-methoxy-2-propenenitrile; 4-amino-1,1,1-trifluoro-3-butene-2-one With sodium hydride In tetrahydrofuran at 0 - 20℃; for 3.33333h; Stage #2: With hydrogenchloride In tetrahydrofuran; water Stage #3: With hydrogenchloride; sodium hydroxide; water; sodium methylate more than 3 stages; | 45.3% |
4-trifluoromethylpyridine
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 79 percent / 2,2,6,6-tetramethylpiperidine; butyllithium; iodine / tetrahydrofuran; hexane / 2 h / -75 °C 2: 81 percent / butyllithium / tetrahydrofuran; hexane / 0.03 h / -75 °C View Scheme |
2-chloro-4-trifluoromethyl pyridine
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 82 percent / diisopropylamine; butyllithium / hexane; tetrahydrofuran / 2 h / -75 °C 2: 89 percent / ammonium formate / palladium (10 percent on charcoal) / methanol / 0.25 h / 25 °C View Scheme |
2,6-dichloro-4-(trifluoromethyl)pyridine-3-carbonitrile
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium hydroxide; water / 8 h / 20 °C 2: hydrogen; triethylamine; 5%-palladium/activated carbon / methanol / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine; hydrogen; palladium on activated carbon / tetrahydrofuran / 4 h 2: sodium hydroxide / ethanol / 10 h / 80 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: sodium bromide; sulfuric acid 2: sodium carbonate; 5%-palladium/activated carbon; hydrogen / methanol / 6 h 3: sodium hydroxide / 5 h / 100 °C View Scheme |
2,6-dichloro-4-trifluoromethylnicotinic acid
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
With 5%-palladium/activated carbon; hydrogen; triethylamine In methanol Reagent/catalyst; Reflux; |
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: trichlorophosphate / 18 h / 130 °C / Inert atmosphere 2: triethylamine; hydrogen; palladium on activated carbon / tetrahydrofuran / 4 h 3: sodium hydroxide / ethanol / 10 h / 80 °C / Inert atmosphere View Scheme |
2,6-dihydroxy-3-cyano-4-(trifluoromethyl)pyridine
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: trichlorophosphate / dichloromethane; N,N-dimethyl-formamide / 6 h / 125 °C 2: sodium bromide; sulfuric acid 3: sodium carbonate; 5%-palladium/activated carbon; hydrogen / methanol / 6 h 4: sodium hydroxide / 5 h / 100 °C View Scheme |
2-aminoacetonitrile hydrochloride
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
Stage #1: 4-(trifluoromethyl)nicotinic acid With thionyl chloride In toluene at 0 - 120℃; for 2.5h; Inert atmosphere; Stage #2: 2-aminoacetonitrile hydrochloride With triethylamine In tetrahydrofuran; toluene at 0 - 25℃; for 10h; Inert atmosphere; | 93.4% |
With phosgene; triethylamine In toluene at -10 - 5℃; for 4h; Reagent/catalyst; Solvent; Temperature; | 91.6% |
N,O-dimethylhydroxylamine*hydrochloride
4-(trifluoromethyl)nicotinic acid
N-methoxy-N-methyl-4-(trifluoromethyl)nicotinamide
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane at 20℃; for 5h; Inert atmosphere; | 93% |
With HATU; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 5h; Inert atmosphere; |
Conditions | Yield |
---|---|
With triethylamine In 1,2-dichloro-ethane at 0 - 35℃; for 4h; Solvent; | 90.4% |
With thionyl chloride; triethylamine; N-methyl-acetamide In tetrahydrofuran; benzene |
4-(trifluoromethyl)nicotinic acid
4-(trifluoromethyl)pyridine-3-carbonyl chloride
Conditions | Yield |
---|---|
With thionyl chloride; N,N-dimethyl-formamide In benzene for 3h; Heating / reflux; | 90.1% |
With oxalyl dichloride In dichloromethane; N,N-dimethyl-formamide at 20℃; for 3h; | |
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 1h; Product distribution / selectivity; |
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid at 0 - 20℃; | 89.8% |
1-t-Butoxycarbonylpiperazine
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide at 0 - 20℃; for 20h; | 83.9% |
Conditions | Yield |
---|---|
Stage #1: 4-(trifluoromethyl)nicotinic acid With oxalyl dichloride; N,N-dimethyl-formamide at 20℃; for 0.0833333h; Stage #2: C23H21N3O2S With pyridine In N,N-dimethyl-formamide at 20℃; for 0.0833333h; | 82% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 23℃; | 82% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In dichloromethane; N,N-dimethyl-formamide at 20℃; for 18h; | 75% |
2-aminoacetonitrile hydrochloride
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
Stage #1: 2-aminoacetonitrile hydrochloride With triethylamine In 5,5-dimethyl-1,3-cyclohexadiene at 43℃; for 0.333333h; Stage #2: 4-(trifluoromethyl)nicotinic acid With oxalyl dichloride In 5,5-dimethyl-1,3-cyclohexadiene at -20 - 105℃; for 0.7h; Temperature; | 73.7% |
3-hydroxypiperazine
4-(trifluoromethyl)nicotinic acid
C12H13F3N2O2
Conditions | Yield |
---|---|
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine In N,N-dimethyl-formamide at 0 - 20℃; for 20h; | 70% |
N,N-diethylhydrazine
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
Stage #1: 4-(trifluoromethyl)nicotinic acid With triethylamine In dichloromethane at 20℃; for 0.0833333h; Stage #2: N,N-diethylhydrazine With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In tetrahydrofuran; dichloromethane at 20℃; for 0.5h; | 64% |
cycl-isopropylidene malonate
4-(trifluoromethyl)nicotinic acid
C8H6F3NO
Conditions | Yield |
---|---|
With PyBOP; triethylamine In tetrahydrofuran at 20℃; for 18h; | 62% |
Stage #1: 4-(trifluoromethyl)nicotinic acid With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine In tetrahydrofuran at 20℃; for 0.166667h; Stage #2: cycl-isopropylidene malonate In tetrahydrofuran at 20℃; Stage #3: With hydrogenchloride In tetrahydrofuran; water for 18h; Heating / reflux; | 62% |
cycl-isopropylidene malonate
4-(trifluoromethyl)nicotinic acid
methyl 4-trifluoromethylpyridine-3-carboxylate
Conditions | Yield |
---|---|
Stage #1: cycl-isopropylidene malonate; 4-(trifluoromethyl)nicotinic acid With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine In tetrahydrofuran at 20℃; Stage #2: With hydrogenchloride; water In tetrahydrofuran for 18h; Stage #3: In tetrahydrofuran; water | 62% |
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
With pyridine Heating; | 60% |
4-(trifluoromethyl)nicotinic acid
methyl iodide
methyl 4-trifluoromethylpyridine-3-carboxylate
Conditions | Yield |
---|---|
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 20℃; for 12h; | 56.1% |
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 20℃; for 12h; | 56.1% |
4-(trifluoromethyl)nicotinic acid
1,7,11-tri-deacetyl-1,7,11-tri-O-(4-trifluoromethyl-3-pyridylcarbonyl)pyripyropene A
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 68h; | 56% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 17.5h; | 36 mg |
serinol
4-(trifluoromethyl)nicotinic acid
N-(4-trifluoromethylnicotinoyl)serinol
Conditions | Yield |
---|---|
Stage #1: 4-(trifluoromethyl)nicotinic acid With 1,1'-carbonyldiimidazole In tetrahydrofuran at 40 - 50℃; for 6h; Stage #2: serinol In tetrahydrofuran at 50 - 60℃; for 4h; | 55.3% |
2-amino-1-(4-chlorophenyl)-3-methylbutan-1-one hydrochloride
4-(trifluoromethyl)nicotinic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In dichloromethane at 30℃; for 16h; | 51% |
4-(4,5-dimethyl-6-(4-(methylamino)piperidin-1-yl)pyridazin-3-yl)benzonitrile
4-(trifluoromethyl)nicotinic acid
N-(1-(6-(4-cyanophenyl)-4,5-dimethylpyridazin-3-yl)piperidin-4-yl)-N-methyl-4-(trifluoromethyl)nicotinamide hydrochloride
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane for 72h; | 49% |
1,7,11-tri-deacetyl-1,11-di-O-propionylpyripyropene A
4-(trifluoromethyl)nicotinic acid
1,7,11-tri-deacetyl-1,11-di-O-propionyl-7-O-(4-trifluoromethyl-3-pyridylcarbonyl)pyripyropene A
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 4.5h; | 49% |
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