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Cas:16245-79-7
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inquiryBenzenamine, 4-octyl- 4-N-OCTYLANILINE Basic information Product Name: 4-N-OCTYLANILINE Synonyms: Benzenamine, 4-octyl-;4-OCTYLANILINE;4-N-OCTYLANILINE;P-OCTYLANILINE;TIMTEC-BB SBB0083
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Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In tetrahydrofuran at 25℃; for 2h; Inert atmosphere; | 92% |
4-octylaniline
Conditions | Yield |
---|---|
1% Pd/C In methanol at 20℃; for 2h; Inert atmosphere; | 85% |
With Pd-C In methanol | 85% |
1-nitro-4-(oct-1-yn-1-yl)benzene
4-octylaniline
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In ethyl acetate under 3750.38 Torr; for 3h; | 66% |
Conditions | Yield |
---|---|
With zinc(II) chloride at 255 - 258℃; for 21h; | 48.7% |
(i)CoCl2, (ii) aq. NH3; Multistep reaction; |
9-octyl-9-bora-bicyclo[3.3.1]nonane
para-nitrophenyl triflate
A
4-octylaniline
B
1-(4-nitro-phenyl)-octane
Conditions | Yield |
---|---|
With potassium phosphate; tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane at 85℃; for 5h; | A 30% B 48% |
Conditions | Yield |
---|---|
With cobalt(II) chloride at 212℃; |
4'-aminooctanoylphenone
4-octylaniline
Conditions | Yield |
---|---|
With hydrogenchloride; amalgamated zinc |
Conditions | Yield |
---|---|
With hydrogen; nitric acid; nickel 1) 96 percent H2SO4, 35 deg C to 45 deg C, 1.5 h, 2) 120 deg C, 100 atm, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; |
Octylbenzene
4-octylaniline
Conditions | Yield |
---|---|
Multistep reaction; | |
Stage #1: Octylbenzene With aluminum (III) chloride; acetyl chloride Stage #2: Schmidt reaction; |
Conditions | Yield |
---|---|
at 212℃; |
Conditions | Yield |
---|---|
at 270 - 280℃; ueber mehrere Stufen; |
A
4-octylaniline
Conditions | Yield |
---|---|
With water at 25℃; for 0.00833333h; pH=4.8 - 5.4; Product distribution; sonication; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 93 percent / AlCl3 / 0.17 h / 60 °C 2: 1) 78 percent nitric acid, 2) H2 / 2) Raney nickel / 1) 96 percent H2SO4, 35 deg C to 45 deg C, 1.5 h, 2) 120 deg C, 100 atm, 2 h View Scheme |
benzene
4-octylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 93 percent / AlCl3 / 0.17 h / 60 °C 2: 1) 78 percent nitric acid, 2) H2 / 2) Raney nickel / 1) 96 percent H2SO4, 35 deg C to 45 deg C, 1.5 h, 2) 120 deg C, 100 atm, 2 h View Scheme |
1-Iodooctane
4-octylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: cobalt (II)-chloride / 212 °C View Scheme |
1-(4-chlorophenyl)-5,5-dimethylhexan-1-one
4-octylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: CuCl; aqueous NH3 / 250 - 270 °C 2: amalgamated zinc; aqueous HCl View Scheme |
aniline
4-octylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: cobalt (II)-chloride / 212 °C View Scheme |
chlorobenzene
4-octylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: AlCl3 2: CuCl; aqueous NH3 / 250 - 270 °C 3: amalgamated zinc; aqueous HCl View Scheme |
n-octanoic acid chloride
4-octylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: AlCl3 2: CuCl; aqueous NH3 / 250 - 270 °C 3: amalgamated zinc; aqueous HCl View Scheme | |
Multi-step reaction with 3 steps 1: aluminum (III) chloride 2: hydrazine 3: aluminum (III) chloride; acetyl chloride View Scheme |
N-(4-[2-[trimethylammonio]ethoxy]benzylidene)-4-n-octylaniline bromide
A
4-octylaniline
Conditions | Yield |
---|---|
With BF2(NC4H(CH3)2)2CO(CH2)10C3H4N2(1+)*Cl(1-)=BF2(NC4H(CH3)2)2CO(CH2)10C3H4N2Cl |
n-octyne
4-octylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; N-ethyl-N,N-diisopropylamine / acetonitrile / 0.33 h / Inert atmosphere 1.2: 50 °C / Inert atmosphere 2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 3750.38 Torr View Scheme |
n-octanophenone
4-octylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrazine 2: aluminum (III) chloride; acetyl chloride View Scheme |
benzene
4-octylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: aluminum (III) chloride 2: hydrazine 3: aluminum (III) chloride; acetyl chloride View Scheme |
para-nitrophenyl bromide
4-octylaniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: palladium diacetate / water 2: Pd-C / methanol View Scheme |
Conditions | Yield |
---|---|
at 20℃; for 1h; | 100% |
for 1h; | 100% |
sulfuric acid at 50℃; for 1h; | 95% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 25℃; for 21h; Cooling with ether-dry ice; | 100% |
With triethylamine at 20 - 50℃; Inert atmosphere of N2; | |
With triethylamine In tetrahydrofuran at 25℃; for 21h; Inert atmosphere; |
3,3',4,4'-biphenyltetracarboxylic anhydride
4-octylaniline
Conditions | Yield |
---|---|
In neat (no solvent) for 0.25h; Solvent; Time; Milling; | 99% |
2,4-dichloro-1,5-dinitrobenzene
4-octylaniline
4,6-dinitro-N,N'-bis(4-octylphenyl)-benzene-1,3-diamine
Conditions | Yield |
---|---|
In ethanol at 80℃; | 98% |
4-octylaniline
Conditions | Yield |
---|---|
With N-Bromosuccinimide; ammonium acetate In acetonitrile at 0 - 20℃; Inert atmosphere; Schlenk technique; | 97% |
With N-Bromosuccinimide In acetonitrile at 0 - 20℃; Inert atmosphere; | 92.5% |
4-octylaniline
Boc-O-benzyl-D-threonine
[(1R,2S)-2-Benzyloxy-1-(4-octyl-phenylcarbamoyl)-propyl]-carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 4h; | 96% |
4-octylaniline
2-iodo-4-n-octylaniline
Conditions | Yield |
---|---|
With N,N,N-trimethylbenzenemethanaminium dichloroiodate; calcium carbonate In methanol; dichloromethane at 20℃; for 2h; | 96% |
With dihydrogen peroxide; iodine In methanol at 20℃; | 86% |
With dihydrogen peroxide; iodine In methanol at 20℃; | 86% |
With N,N,N-trimethylbenzenemethanaminium dichloroiodate In methanol; dichloromethane at 20℃; for 4h; | 82% |
With N,N,N-trimethylbenzenemethanaminium dichloroiodate; calcium carbonate In methanol; dichloromethane at 20℃; for 2.5h; | 73% |
2,4-dichloro-1,5-dinitrobenzene
4-octylaniline
Conditions | Yield |
---|---|
In ethanol at 20℃; | 96% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate In toluene for 16h; Inert atmosphere; Reflux; | 95% |
Conditions | Yield |
---|---|
Stage #1: 4-octylaniline With hydrogenchloride; sodium nitrite In ethanol; water at 0 - 5℃; for 1h; Stage #2: 1-amino-naphthalene In ethanol at 0 - 5℃; for 4h; | 95% |
3,3'dibromo-2,2'-bithiophene
4-octylaniline
N-[4-octylphenyl]dithieno[3,2-b:2',3'-d]pyrrole
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate In toluene for 12h; Inert atmosphere; Reflux; | 92% |
With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate In toluene for 12h; Inert atmosphere; Reflux; | 92% |
4-octylaniline
1,2-dichloro-ethane
Conditions | Yield |
---|---|
In 2,4,6-trimethylpyrylium sulfoacetate | 89% |
Conditions | Yield |
---|---|
Stage #1: 4-octylaniline With hydrogenchloride; sodium nitrite In ethanol; water for 0.5h; Cooling with ice; Stage #2: phenol With sodium hydroxide In ethanol; water at 0℃; | 88% |
With hydrogenchloride; sodium carbonate; sodium nitrite In water | |
Stage #1: 4-octylaniline With hydrogenchloride; sodium nitrite In water at 0℃; for 0.5h; Stage #2: phenol With sodium carbonate In water at 0℃; for 1h; |
4-octylaniline
N-(4-[2-[trimethylammonio]ethoxy]benzylidene)-4-n-octylaniline bromide
Conditions | Yield |
---|---|
With triethylamine In methanol at 85℃; for 50h; | 88% |
1-Bromo-2-iodobenzene
4-octylaniline
2-bromo-N-(4-octylphenyl)aniline
Conditions | Yield |
---|---|
With sodium t-butanolate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether In toluene at 100℃; for 24h; Inert atmosphere; | 88% |
4-octylaniline
10-(p-formylphenyloxy)decyltrimethylammonium bromide
Conditions | Yield |
---|---|
With acetic acid In ethanol for 12h; Heating; | 87% |
ethyl 3-isocyanatopropanoate
4-octylaniline
ethyl 3-(3-(4-octylphenyl)ureido)propanoate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 0.5h; Reflux; | 87% |
4-octylaniline
2,6-diiodo-4-octylaniline
Conditions | Yield |
---|---|
With pyridine iodine monochloride In methanol Reflux; | 87% |
p-n-octylbenzoyl chloride
4-octylaniline
4-octyl-N-(4-octylphenyl)benzamide
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 20℃; for 18h; | 87% |
1-Bromo-3-iodobenzene
4-octylaniline
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate In toluene at 120℃; for 4h; Inert atmosphere; | 87% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 24h; | 87% |
Conditions | Yield |
---|---|
With sodium t-butanolate; XPhos In toluene at 70℃; for 0.25h; Buchwald-Hartwig amination; Inert atmosphere; | 86% |
With η5‐cyclopentadienyl‐η3‐1‐phenylallylpalladium; sodium t-butanolate; XPhos In toluene at 90℃; Inert atmosphere; | 86% |
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene for 1h; Inert atmosphere; Reflux; | 78% |
4-octylaniline
Conditions | Yield |
---|---|
Stage #1: 4-octylaniline With hydrogenchloride; sodium nitrite In water at 0℃; for 0.25h; Stage #2: With tetrafluoroboric acid In water | 85% |
Conditions | Yield |
---|---|
In toluene at 110℃; for 4h; | 83% |
2,5-dibromo-1,4-benzoquinone
4-octylaniline
2,5-dibromo-N,N'-bis-(4-octyl-phenyl)-benzene-1,4-diamine
Conditions | Yield |
---|---|
With titanium tetrachloride In chlorobenzene at 135℃; for 48h; | 82% |
4-octylaniline
1,1′-bis(2,4-dinitrophenyl)-[4,4′-bipyridine]-1,1′-diium chloride
Conditions | Yield |
---|---|
In ethanol; water for 18h; Heating; | 82% |
With air In ethanol; water at 60℃; for 18h; | 63% |
2-chloroethyl isothiocyanate
4-octylaniline
Conditions | Yield |
---|---|
at 20℃; | 81% |
for 6h; Ambient temperature; |
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