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inquiry2-Methoxy-5-trifluoromethyl-aniline
trichloromethyl chloroformate
2-methoxy-5-trifluoromethylphenyl isocyanate
Conditions | Yield |
---|---|
With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene In dichloromethane at 0 - 20℃; for 1.5h; | 88% |
With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene In dichloromethane at 0 - 20℃; for 1.5h; | 88% |
With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene In dichloromethane at 0 - 20℃; for 1.5h; | 88% |
phosgene
2-Methoxy-5-trifluoromethyl-aniline
2-methoxy-5-trifluoromethylphenyl isocyanate
Conditions | Yield |
---|---|
With pyridine In diethyl ether; dichloromethane; toluene | |
With pyridine In dichloromethane; toluene at 0 - 20℃; for 3.5h; | |
With sodium hydrogencarbonate In dichloromethane; water at 0℃; for 0.5h; |
4-(4-acetylphenoxy)-5-aminopyridine
2-Methoxy-5-trifluoromethyl-aniline
2-methoxy-5-trifluoromethylphenyl isocyanate
2-Methoxy-5-trifluoromethyl-aniline
N,N,N',N'-tetramethyl-1,8-diaminonaphthalene
trichloromethyl chloroformate
2-methoxy-5-trifluoromethylphenyl isocyanate
Conditions | Yield |
---|---|
In dichloromethane |
bis(trichloromethyl) carbonate
2-Methoxy-5-trifluoromethyl-aniline
2-methoxy-5-trifluoromethylphenyl isocyanate
Conditions | Yield |
---|---|
With pyrographite In ethyl acetate for 2h; Reflux; |
5-(4-aminophenoxy)isoindoline-1,3-dione
2-methoxy-5-trifluoromethylphenyl isocyanate
Conditions | Yield |
---|---|
In dichloromethane at 0 - 20℃; for 12 - 22h; Product distribution / selectivity; | 96% |
2-methoxy-5-trifluoromethylphenyl isocyanate
2-bromo-6-fluoroaniline
3-(2-bromo-6-fluorophenyl)-1-[2-methoxy-5-(trifluoromethyl)phenyl]urea
Conditions | Yield |
---|---|
In acetonitrile at 35 - 88℃; for 38 - 45h; Product distribution / selectivity; | 87.5% |
2-Fluoroaniline
2-methoxy-5-trifluoromethylphenyl isocyanate
N-(2-fluorophenyl)-N'-[2-methoxy-5-(trifluoromethyl)phenyl]urea
Conditions | Yield |
---|---|
In acetonitrile at 82℃; for 4h; | 86.4% |
In acetonitrile for 4h; Reflux; Large scale; | 85.9% |
In acetonitrile at 0℃; for 7.25h; Reflux; Large scale; | 85.9% |
In acetonitrile for 4h; Reflux; Large scale; | 85.9% |
In acetonitrile Reflux; |
N-(4-fluoro-3-methylphenyl)-piperazine
(2E)-3-{3-fluoro-2-[(triphenylphosphoranylidene)amino]phenyl}-propenoic acid methyl ester
2-methoxy-5-trifluoromethylphenyl isocyanate
Conditions | Yield |
---|---|
79% |
(2E)-3-{3-fluoro-2-[(triphenylphosphoranylidene)amino]phenyl}-propenoic acid methyl ester
2-methoxy-5-trifluoromethylphenyl isocyanate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; | 62% |
2-methoxy-5-trifluoromethylphenyl isocyanate
3-chloro-aniline
Conditions | Yield |
---|---|
In dichloromethane at 0℃; for 0.75h; | 55% |
9-methyl-1,2,3,4-tetrahydro-pyrazino[1,2-a]indole
(2E)-3-{3-fluoro-2-[(triphenylphosphoranylidene)amino]phenyl}-propenoic acid methyl ester
2-methoxy-5-trifluoromethylphenyl isocyanate
[8-fluoro-3-(2-methoxy-5-trifluoromethyl-phenyl)-2-(9-methyl-3,4-dihydro-1H-pyrazino[1,2-a]indol-2-yl)-3,4-dihydro-quinazolin-4-yl]acetic acid methyl ester
Conditions | Yield |
---|---|
Stage #1: (2E)-3-{3-fluoro-2-[(triphenylphosphoranylidene)amino]phenyl}-propenoic acid methyl ester; 2-methoxy-5-trifluoromethylphenyl isocyanate In dichloromethane at 20℃; Stage #2: 9-methyl-1,2,3,4-tetrahydro-pyrazino[1,2-a]indole With silica gel In 1,4-dioxane; dichloromethane at 20℃; Heating / reflux; | 42% |
2-methoxy-5-trifluoromethylphenyl isocyanate
(2E)-3-{2-[(triphenylphosphoranylidene)amino]phenyl}-propenoic acid methyl ester
Conditions | Yield |
---|---|
In dichloromethane at 20℃; | 38% |
2-methoxy-5-trifluoromethylphenyl isocyanate
4-fluoroaniline
Conditions | Yield |
---|---|
In ethyl acetate | |
In ethyl acetate at 20℃; for 72h; | |
In ethyl acetate at 20℃; for 72h; | |
In ethyl acetate at 20℃; for 72h; Product distribution / selectivity; |
2-methoxy-5-trifluoromethylphenyl isocyanate
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; |
2-methoxy-5-trifluoromethylphenyl isocyanate
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; |
2-methoxy-5-trifluoromethylphenyl isocyanate
Conditions | Yield |
---|---|
In dichloromethane; N,N-dimethyl-formamide |
4-(4-acetylphenoxy)-5-aminopyridine
2-methoxy-5-trifluoromethylphenyl isocyanate
4-Fluoronitrobenzene
4-Hydroxyacetophenone
1-(4-(4-nitrophenoxy)phenyl)ethanone
4-chloro-pyridine-2-carbonyl chloride
2-methoxy-5-trifluoromethylphenyl isocyanate
2-Methoxy-5-trifluoromethyl-aniline
isopropylamine
A
4-(2-(N-isopropylcarbamoyl)-pyridin-4-yloxy)aniline
B
4-amino-phenol
2-methoxy-5-trifluoromethylphenyl isocyanate
2-Methoxy-5-trifluoromethyl-aniline
4-(4-amino-3-chloro-phenoxy)-pyridine-2-carboxylic acid methylamide
2-methoxy-5-trifluoromethylphenyl isocyanate
amino-4 hydroxy-2 toluene
2-Methoxy-5-trifluoromethyl-aniline
A
3-(2-(N-methylcarbamoyl)-pyridin-4-yloxy)-4-methylaniline
B
4-chloro-N-methylpicolinamide
4-(4-aminophenoxy)-N,N-dimethylpicolinamide
2-methoxy-5-trifluoromethylphenyl isocyanate
2-Methoxy-5-trifluoromethyl-aniline
4-(1-oxoisoindolin-5-yloxy)aniline
4-(2-(N-isopropylcarbamoyl)-pyridin-4-yloxy)aniline
2-methoxy-5-trifluoromethylphenyl isocyanate
2-Methoxy-5-trifluoromethyl-aniline
methyl 5-(4-aminophenoxy)pyridine-3-carboxylate
N-methylphthalimide
2-methoxy-5-trifluoromethylphenyl isocyanate
2-Methoxy-5-trifluoromethyl-aniline
4-chloro-N-methylpicolinamide
5-methyl-1-(pyridin-4-yl)methyl-1H-benzimidazol-4-ylamine
2-methoxy-5-trifluoromethylphenyl isocyanate
Conditions | Yield |
---|---|
In dichloromethane for 4h; |
1-(Pyridin-4-yl)methyl-1H-benzimidazol-4-ylamine
2-methoxy-5-trifluoromethylphenyl isocyanate
Conditions | Yield |
---|---|
In dichloromethane; N,N-dimethyl-formamide at 20℃; for 16h; |
6-(3-aminophenyl)-N-(pyridin-4-ylmethyl)imidazo[1,2-a]pyrazin-8-amine
2-methoxy-5-trifluoromethylphenyl isocyanate
1-(2-metoxy-5-trifluoromethyl-phenyl)-3-(3-{8-[(-pyridin-4-yl-methyl)-amino]-imidazo[1,2-a]pyrazin-6-yl}-phenyl)-urea
Conditions | Yield |
---|---|
In toluene at 20℃; for 0.5h; |
2-methoxy-5-trifluoromethylphenyl isocyanate
4-(2-aminoethyl)-2-nitro-phenylamine
C17H17F3N4O4
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 2h; |
2-methoxy-5-trifluoromethylphenyl isocyanate
(S)-2-(8-fluoro-3-(2-methoxy-5-(trifluoromethyl)-phenyl)-2-(4-(3-methoxyphenyl)piperazin-1-yl)-3,4-dihydroquinazolin-4-yl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: acetonitrile / Reflux 2: acetic acid; palladium diacetate 3: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetone / Reflux 4: 1,8-diazabicyclo[5.4.0]undec-7-ene; trichlorophosphate / chlorobenzene / Reflux 5: 1,8-diazabicyclo[5.4.0]undec-7-ene / 1,4-dioxane / Reflux 6: ethyl acetate / 20 °C 7: sodium hydrogencarbonate; sodium hydroxide; water / tert-butyl methyl ether / Reflux; Large scale View Scheme | |
Multi-step reaction with 6 steps 1.1: acetonitrile / 4 h / Reflux; Large scale 2.1: acetic acid; sulfuric acid; sulfur trioxide; palladium diacetate; oxygen / 20 h / 20 °C / Inert atmosphere; Large scale 3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetone / 4 h / Reflux; Large scale 4.1: trichlorophosphate / chlorobenzene / 3 h / Reflux; Large scale 4.2: 9 h / Reflux; Large scale 5.1: ethyl acetate / 1 h / 20 °C / Large scale 5.2: 72 h / 20 °C / Large scale 6.1: sodium hydrogencarbonate / water; tert-butyl methyl ether / Large scale 6.2: Reflux; Large scale View Scheme | |
Multi-step reaction with 7 steps 1.1: acetonitrile / 7.25 h / 0 °C / Reflux; Large scale 2.1: acetic acid / Inert atmosphere; Large scale 2.2: 20 h / 20 °C / Inert atmosphere; Large scale 3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetone / 4 h / 55 °C / Reflux; Large scale 4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; trichlorophosphate / chlorobenzene / 12 h / Reflux; Large scale 5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 1,4-dioxane / 4 h / Reflux; Large scale 6.1: ethyl acetate / 76 h / 0 - 20 °C / Large scale 7.1: sodium hydrogencarbonate; water; sodium hydroxide / tert-butyl methyl ether / 22 °C / Reflux; Large scale View Scheme |
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