DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:1668-10-6
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Cas:1668-10-6
Min.Order:0
Negotiable
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inquiryProduct name Glycinamide hydrochloride Alias Glycinamide monohydrochloride; 2-amino-2-oxoethanaminium; 2-AMINOACETAMIDE HYDROCHLORIDE; GLY-NH2 HYDROCHLORIDE; GLYCINE AMIDE HYDROCHLORIDE; GLYCINE-NH2
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Min.Order:1 Kilogram
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Min.Order:1 Gram
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inquiryPRODUCT DETAILS Glycinamide hydrochloride Basic information Product
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Type:Lab/Research institutions
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Appearance:White to beige Crystalline Powder Storage:Inert atmosphere,Room Temperature Application:Glycinamide hydrochloride is a buffer that is useful in the physiological pH range. And it is also used as a pharmaceutical intermediate, in
Cas:1668-10-6
Min.Order:25 Kilogram
Negotiable
Type:Lab/Research institutions
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Min.Order:1 Kilogram
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Min.Order:0 Metric Ton
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Min.Order:10 Kilogram
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Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With hydrogenchloride; 2-hydroxyethanethiol In tetrahydrofuran at -78℃; | 86% |
Conditions | Yield |
---|---|
With ammonia In ethanol at 100℃; for 0.5h; | 76% |
4-methylene-1-oxa-6,9-diazaspiro<4,5>decane-7,10-dione
A
glycinamide hydrochloride
B
3-hydroxy-4-(2-hydroxyethyl)-2(5H)-furanone
Conditions | Yield |
---|---|
With hydrogenchloride at 100℃; for 1.5h; Product distribution; other conditions, other reagents; | A 33% B 56% |
glycinamide hydrochloride
Conditions | Yield |
---|---|
bei dreiwoechigem Aufbewahren; |
Conditions | Yield |
---|---|
With ammonia In methanol for 72h; Ambient temperature; |
glycinamide hydrochloride
N-Benzyloxycarbonyl-L-proline
Nα-benzyloxycarbonyl-L-prolyl-glycinamide
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; | 100% |
Stage #1: N-Benzyloxycarbonyl-L-proline With 1,1'-carbonyldiimidazole In tetrahydrofuran at 20℃; Stage #2: glycinamide hydrochloride With triethylamine In tetrahydrofuran at 20℃; Further stages.; | 53% |
With 4-methyl-morpholine; isobutyl chloroformate 1) DMF, -15 deg C, 15 min, 2) -10 deg C, 14h; Yield given. Multistep reaction; |
glycinamide hydrochloride
N-(benzyloxycarbonyl)-L-phenylalanine benzyl ester
Z-L-phenylalanylglycinamide
Conditions | Yield |
---|---|
With S166C-SBnCOOH; triethylamine; calcium chloride In water; N,N-dimethyl-formamide for 1h; Ambient temperature; | 100% |
With triethylamine; enzyme mutant SBL-S166C-S-[(4S,5R)-indenooxazolidinonyl] In water; N,N-dimethyl-formamide at 20℃; for 1h; pH=5.8; | 100% |
With triethylamine; S166C-S-S-(CH2)2-O-β-D-Glc(Ac)2 subtilisin protease In water; N,N-dimethyl-formamide at 20℃; for 1h; pH=5.8; Enzymatic reaction; MES buffer; | 95% |
With subtilisin BPN'; triethylamine In water; N,N-dimethyl-formamide Ambient temperature; | 80% |
Conditions | Yield |
---|---|
With S166C-SCH2CH2NH3+; triethylamine; calcium chloride In water; N,N-dimethyl-formamide for 5h; Ambient temperature; | 100% |
With triethylamine; enzyme mutant SBL-S166C-S-CH2C(CH2NH3)3 In water; N,N-dimethyl-formamide at 20℃; for 5h; pH=5.8; | 71% |
With triethylamine; S166C-S-S-(CH2)2-O-β-D-Gal subtilisin protease In water; N,N-dimethyl-formamide at 20℃; for 5h; pH=5.8; Enzymatic reaction; MES buffer; | 67% |
glycinamide hydrochloride
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide
Fmoc-Gly-NH2
Conditions | Yield |
---|---|
With sodium carbonate In acetone at 20℃; for 1h; | 100% |
With sodium hydrogencarbonate In acetone at 20℃; for 2h; pH=7; | 80% |
With sodium carbonate In water; acetone at 0 - 20℃; for 1.5h; | 72% |
6-bromopyrazolo[1,5-a]pyrimidine-3-carboxylic acid
glycinamide hydrochloride
N-(2-amino-2-oxoethyl)-6-bromopyrazolo[1,5-a]pyrimidine-3-carboxamide
Conditions | Yield |
---|---|
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine In N,N-dimethyl-formamide at 20℃; for 2h; | 100% |
sodium 1-(2,5-dimethoxyphenyl)-3-ethoxy-3-oxoprop-1-en-1-olate
glycinamide hydrochloride
ethyl (Z)-3-( (2-amino-2-oxoethyl)amino)-3-(2,5-dimethoxyphenyl)acrylate
Conditions | Yield |
---|---|
Stage #1: glycinamide hydrochloride With sodium methylate at 65℃; for 1h; Stage #2: sodium 1-(2,5-dimethoxyphenyl)-3-ethoxy-3-oxoprop-1-en-1-olate With acetic acid at 10℃; for 16.5h; | 100% |
glycinamide hydrochloride
2,2,2-trifluoroethyl ((benzyloxy)carbonyl)-L-phenylalaninate
A
N-Cbz-L-Phe
B
Z-L-phenylalanylglycinamide
Conditions | Yield |
---|---|
With Tris buffer; TEA; Celite; α-chymotrypsin In acetonitrile at 30℃; for 1h; | A 0.6% B 99% |
glycinamide hydrochloride
Nα-benzyloxycarbonyl-L-lysine thiobenzyl ester
Conditions | Yield |
---|---|
With S166C-SBnCOOH; triethylamine; calcium chloride In water; N,N-dimethyl-formamide for 5h; Ambient temperature; | 99% |
glycinamide hydrochloride
Z-L-Ala benzyl ester
CBZ-L-alanylglycinamide
Conditions | Yield |
---|---|
With triethylamine; enzyme mutant SBL-S166C-S-(CH2)2-NMe3(1+) In water; N,N-dimethyl-formamide at 20℃; for 5h; pH=5.8; | 99% |
With S166C-SBn; triethylamine; calcium chloride In water; N,N-dimethyl-formamide for 5h; Ambient temperature; | 95% |
With triethylamine; S166C-S-S-(CH2)2-O-β-D-Gal(Ac)3 subtilisin protease In water; N,N-dimethyl-formamide at 20℃; for 5h; pH=5.8; Enzymatic reaction; MES buffer; | 92% |
Conditions | Yield |
---|---|
With 4-methyl-morpholine; isobutyl chloroformate In tetrahydrofuran for 24h; slowly from 0 deg C to room temp.; | 98% |
glycinamide hydrochloride
(S)-1-((benzyloxy)carbonyl)pyrrolidine-3-carboxylic acid
C15H19N3O4
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In acetonitrile at 0 - 20℃; for 24h; Inert atmosphere; | 98% |
glycinamide hydrochloride
<<6-methoxy-5-(trifluoromethyl)-1-naphthalenyl>sulfonyl>chloride
Conditions | Yield |
---|---|
With sodium carbonate In 1,4-dioxane for 1h; Ambient temperature; | 97.8% |
3-{4-fluoro-2-[3-(trifluoromethyl)benzyl]-1-benzothien-7-yl}benzoic acid
glycinamide hydrochloride
N-(2-amino-2-oxoethyl)-3-{4-fluoro-2-[3-(trifluoromethyl)-benzyl]-1-benzothiophen-7-yl}benzamide
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl acetamide at 0 - 20℃; for 1h; Inert atmosphere; | 97% |
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 5h; | 60% |
Conditions | Yield |
---|---|
With potassium carbonate In water; acetonitrile at 5 - 30℃; for 7h; Reagent/catalyst; Solvent; | 97% |
Stage #1: glycinamide hydrochloride With potassium carbonate In water Stage #2: acryloyl chloride In diethyl ether; water at 5 - 20℃; | 72% |
With potassium carbonate In dichloromethane at 5 - 20℃; pH=7 - 8; | 68% |
Conditions | Yield |
---|---|
Stage #1: glycinamide hydrochloride With triethylamine In dichloromethane for 0.25h; Stage #2: m-bromobenzoic acid With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In dichloromethane; ethyl acetate at 20℃; Cooling with ice; | 97% |
glycinamide hydrochloride
(2R)-2-{[(benzyloxy)carbonyl]amino}-4-tert-butoxy-4-oxobutanoic acid
D-(benzyloxycarbonyl)-β-tert-butylaspartylglycinamide
Conditions | Yield |
---|---|
With 1-hydroxy-pyrrolidine-2,5-dione; triethylamine; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide a) 4 deg C, 3 h, b) RT, 4 h; | 96.6% |
glycinamide hydrochloride
(1H-indol-3-ylcarbonyl)-Asp-Phe-NMeBzl
Conditions | Yield |
---|---|
With benzotriazol-1-ol In N,N-dimethyl-formamide 1.) 0 deg C, 1 h, 2.) RT, 3 h; | 96% |
3,5,5-trimethyl hexanal
glycinamide hydrochloride
(+/-)-2-(2,4,4-trimethylpentyl)imidazolidin-4-one
Conditions | Yield |
---|---|
With triethylamine In methanol for 18h; Inert atmosphere; Reflux; | 96% |
glycinamide hydrochloride
Conditions | Yield |
---|---|
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; | 96% |
4-Aminopent-3-en-2-one
glycinamide hydrochloride
N-(1-methyl-3-oxo-1-butenyl)glycinamide
Conditions | Yield |
---|---|
In methanol for 3h; Heating; | 95% |
Conditions | Yield |
---|---|
With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane | 95% |
Conditions | Yield |
---|---|
Stage #1: glycinamide hydrochloride With sodium hydroxide In water Stage #2: In water at 130℃; for 1h; Reagent/catalyst; | 94.5% |
6-boronopyrazolo[1,5-a]pyrimidine-3-carboxylic acid
glycinamide hydrochloride
(3-{[(2-amino-2-oxoethyl)amino]carbonyl}pyrazolo[1,5-a]pyrimidin-6-yl)boronic acid
Conditions | Yield |
---|---|
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine In N,N-dimethyl-formamide at 20℃; for 1.5h; | 94% |
ethyl 3-{2-[3-(trifluoromethyl)benzyl]-1-benzothiophen-7-yl}benzoate
glycinamide hydrochloride
N-(2-amino-2-oxoethyl)-3-{2-[3-(trifluoromethyl)benzyl]-1-benzothiophen-7-yl}benzamide
Conditions | Yield |
---|---|
Stage #1: ethyl 3-{2-[3-(trifluoromethyl)benzyl]-1-benzothiophen-7-yl}benzoate With water; sodium hydroxide In tetrahydrofuran; ethanol at 60℃; for 0.5h; Stage #2: With hydrogenchloride In tetrahydrofuran; ethanol; water Stage #3: glycinamide hydrochloride With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide for 2h; | 94% |
2-(3,5-dichloro-6-methyl-2-oxopyrazin-1(2H)-yl)-2-phenylacetic acid methyl ester
glycinamide hydrochloride
2-(3-(2-amino-2-oxoethylamino)-5-chloro-6-methyl-2-oxopyrazin-1(2H)-yl)-2-phenylacetic acid methyl ester
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 100℃; for 3h; Microwave irradiation; Sealed vial; | 94% |
2-methylundecanal
glycinamide hydrochloride
(+/-)-2-(undecan-2-yl)imidazolidin-4-one
Conditions | Yield |
---|---|
With triethylamine In methanol for 18h; Inert atmosphere; Reflux; | 94% |
Conditions | Yield |
---|---|
Stage #1: Fmoc-Asp(tBu)-Glu(tBu)-Val-Asp(tBu)-OH With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 20℃; for 0.75h; Stage #2: glycinamide hydrochloride In N,N-dimethyl-formamide at 20℃; for 3h; | 94% |
glycinamide hydrochloride
5-amino-4-hexen-3-one
N-(1-methyl-3-oxo-1-pentenyl)glycinamide
Conditions | Yield |
---|---|
In methanol for 3h; Heating; | 93% |
ethyl 3-(5-chloro-2-methoxyphenyl)-3-oxopropanoate
glycinamide hydrochloride
(Z)-ethyl 3-((2-amino-2-oxoethyl)amino)-3-(5-chloro-2-methoxyphenyl)acrylate
Conditions | Yield |
---|---|
Stage #1: glycinamide hydrochloride With sodium methylate In methanol at 65℃; for 1h; Stage #2: ethyl 3-(5-chloro-2-methoxyphenyl)-3-oxopropanoate With acetic acid at 50℃; for 16h; | 93% |
Stage #1: glycinamide hydrochloride With sodium methylate In methanol at 65℃; for 1h; Stage #2: ethyl 3-(5-chloro-2-methoxyphenyl)-3-oxopropanoate With acetic acid In methanol at 50℃; for 16h; Reflux; | 339.4 g |
glycinamide hydrochloride
(Z)-3-amino-1-(p-tolyl)but-2-en-1-one
N-(1-methyl-3-oxo-3-p-tolyl-1-propenyl)glycinamide
Conditions | Yield |
---|---|
In methanol for 6h; Heating; | 92% |
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