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inquiryTIANFU CHEM--(1S–4R)-4-(2-amino-6-chloro-9H-purin-9-yl)-2-cyclopentene-1-methanol hydrochloride 1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High qualit
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inquiry(1S–4R)-4-(2-amino-6-chloro-9H-purin-9-yl)-2-cyclopentene-1-methanol hydrochloride CAS:172015-79-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trad
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inquiry(1S,4R)-4-(2-Amino-6-chloro-9H-purin-9... CAS: 172015-79-1 Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard Shelf life 2 years Storage sh
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inquiryProduct name: (1S,4R)-4-(2-Amino-6-Chloro-9H-Purin-9-yl)-2-Cyclopentene-1-Methanol Hydrochloride CAS No.:172015-79-1 Molecule Formula:C11H13Cl2N5O Molecule Weight:302.16 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Sta
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inquiryProduct Name: (1S–4R)-4-(2-amino-6-chloro-9H-purin-9-yl)-2-cyclopentene-1-methanol hydrochloride Synonyms: SIM 2142 (1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)-2-cyclopentene-1-methanolhydrochloride 172015-79-1 100gm;(1S–4R)-4-(2-amino
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiry(1R,4S)-1-[(2-amino-6-chloro-5-formamido-4-pyrimidinyl)amino]-4-(hydroxymethyl)-2-cyclopentene
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; orthoformic acid triethyl ester In water for 4h; Cyclization; | 92% |
With hydrogenchloride; orthoformic acid triethyl ester In water at 0 - 10℃; for 1h; Concentration; Temperature; | 76% |
With hydrogenchloride; orthoformic acid triethyl ester In ethanol at 0 - 10℃; for 10h; | 72.2% |
orthoformic acid triethyl ester
(1R,4S)-1-[(2-amino-6-chloro-5-formamido-4-pyrimidinyl)amino]-4-(hydroxymethyl)-2-cyclopentene
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran; industrial methylated spirit; water at 0 - 25℃; Product distribution / selectivity; | 82% |
With hydrogenchloride In industrial methylated spirit; water at 0 - 25℃; Product distribution / selectivity; | 81% |
(-)-2-azabicyclo[2.2.1]hept-5-en-3-one
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 1.264 g / tetrahydrofuran; H2O / 18 h / 20 - 60 °C 2: 90.5 percent / LiAlH4 / tetrahydrofuran / 19.5 h / 0 °C / Heating 3: 83 percent / Et3N / ethanol / 7 h / Heating 4: 92 percent / triethylorthoformate; HCl / H2O / 4 h View Scheme |
(1R,4S)-1-amino-4-hydroxymethyl-2-cyclopentene
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 83 percent / Et3N / ethanol / 7 h / Heating 2: 92 percent / triethylorthoformate; HCl / H2O / 4 h View Scheme |
N-(2-amino-4,6-dichloropyrimidin-5-yl)formamide
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 83 percent / Et3N / ethanol / 7 h / Heating 2: 92 percent / triethylorthoformate; HCl / H2O / 4 h View Scheme | |
Multi-step reaction with 2 steps 1.1: sodium hydrogencarbonate / ethanol / 0.5 h / 20 °C / Inert atmosphere 1.2: 3 h / 75 - 80 °C / Inert atmosphere 2.1: orthoformic acid triethyl ester; hydrogenchloride / ethanol / 10 h / 0 - 10 °C View Scheme |
2-amino-5-{[(dimethylamino)methylene]amino}-4,6-dichloropyrimidine
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 72 percent / aq. phosphate buffer / 4 h / pH 3.2 / Heating 2: 83 percent / Et3N / ethanol / 7 h / Heating 3: 92 percent / triethylorthoformate; HCl / H2O / 4 h View Scheme |
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 90.5 percent / LiAlH4 / tetrahydrofuran / 19.5 h / 0 °C / Heating 2: 83 percent / Et3N / ethanol / 7 h / Heating 3: 92 percent / triethylorthoformate; HCl / H2O / 4 h View Scheme |
4,6-dichloro-2,5-diformamido-pyrimidine
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
Stage #1: (1S,4R)-4-amino-2-cyclopentene-1-methanol tartrate salt With sodium carbonate In ethanol for 0.5h; Stage #2: 4,6-dichloro-2,5-diformamido-pyrimidine In ethanol for 3h; Heating / reflux; Stage #3: With hydrogenchloride; orthoformic acid triethyl ester more than 3 stages; |
Cyclopropylamine
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
abacavir
Conditions | Yield |
---|---|
In methanol at 70℃; for 12h; Substitution; | 90% |
Stage #1: (1S,cis)-4-(2-amino-6-chloro-9-H-purin-9-yl)-2-cyclopentene-1-methanol hydrochloride With triethylamine In water Stage #2: Cyclopropylamine In water at 70 - 75℃; Concentration; Solvent; Temperature; | 90% |
In isopropyl alcohol at 90 - 95℃; for 12h; sealed reactor; | |
In ethanol at 25 - 78℃; for 6h; | |
With sodium carbonate In ethanol at 70 - 80℃; | 25 g |
pyrographite
Cyclopropylamine
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
abacavir
Conditions | Yield |
---|---|
With sodium hydroxide In acetone | 90% |
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
With sodium carbonate In ethanol at 75 - 80℃; for 6h; Solvent; Reagent/catalyst; Inert atmosphere; | 87.1% |
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 90 percent / methanol / 12 h / 70 °C 2: 98 percent / H2 / Pd-C / ethanol / 1.5 h / 2585.74 Torr View Scheme |
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
(1S,4R)-4-[2-amino-6-chloro-9H-purin-9-yl]-2-cyclopentene-1-methanol
Conditions | Yield |
---|---|
With ammonia In water at 10 - 15℃; for 1h; pH=7 - 7.5; |
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
(1S,4R)-4-[2-amino-6-(cyclopropylamino)-9H-purin-9-yl]-2-cyclopentene-1-methanol hydrobromide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ethanol / 6 h / 25 - 78 °C 2: hydrogen bromide / ethanol; water / 0.75 h / 25 - 30 °C View Scheme |
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
(1S,4R)-4-[2-amino-6-(cyclopropylamino)-9H-purin-9-yl]-2-cyclopentene-1-methanol malonate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ethanol / 6 h / 25 - 78 °C 2: ethanol / 0.75 h / 25 - 70 °C View Scheme |
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
(1S,4R)-4-[2-amino-6-(cyclopropylamino)-9H-purin-9-yl]-2-cyclopentene-1-methanol maleate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ethanol / 6 h / 25 - 78 °C 2: ethanol / 0.25 h / 25 - 30 °C View Scheme |
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
(1S,4R)-4-[2-amino-6-(cyclopropylamino)-9H-purin-9-yl]-2-cyclopentene-1-methanol monooxalate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ethanol / 6 h / 25 - 78 °C 2: ethanol; water / 2.25 h / 0 - 75 °C View Scheme |
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ethanol / 6 h / 25 - 78 °C 2: hydrogen bromide / ethanol; water / 0.75 h / 25 - 30 °C View Scheme |
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
di-tert-butyl diisopropylphosphoramide
3-chloro-benzenecarboperoxoic acid
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
Stage #1: di-tert-butyl diisopropylphosphoramide; ((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride With 1H-tetrazole In dichloromethane at 20℃; for 1h; Stage #2: 3-chloro-benzenecarboperoxoic acid In dichloromethane at -40 - -10℃; for 2.33333h; | 161 mg |
2-methoxyethylamine
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
In tetrahydrofuran; ethanol at 120℃; for 0.75h; Microwave irradiation; | 81 mg |
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
carbovir
Conditions | Yield |
---|---|
With sodium hydroxide In water at 130℃; for 1h; Microwave irradiation; | 55 mg |
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: methanol / 6 h / 20 °C 2: 1-methyl-1H-imidazole / acetonitrile / 0.5 h / 20 °C / Inert atmosphere View Scheme |
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 1H-tetrazole / dichloromethane / 1 h / 20 °C 1.2: 2.33 h / -40 - -10 °C 2.1: hydrogenchloride / ethyl acetate / 3 h / 20 °C View Scheme |
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: 1H-tetrazole / dichloromethane / 1 h / 20 °C 1.2: 2.33 h / -40 - -10 °C 2.1: hydrogenchloride / ethyl acetate / 3 h / 20 °C 3.1: methanol / 2.5 h / 50 - 60 °C / Microwave irradiation View Scheme |
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
With sodium hydrogensulfide In ethanol; water at 20℃; for 18h; | 11 mg |
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
With tert-butylmagnesium chloride In tetrahydrofuran at 20℃; Inert atmosphere; | 7.16 mg |
sodium methylate
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
((1S,4R)-4-(2-amino-6-methoxy-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol
Conditions | Yield |
---|---|
With methanol at 20℃; for 6h; | 0.47 g |
dimethyl amine
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
In ethanol; water at 20℃; for 1h; | 20 mg |
methylamine
((1S,4R)-4-(2-amino-6-chloro-9H-purin-9-yl)cyclopent-2-en-1-yl)methanol hydrochloride
Conditions | Yield |
---|---|
In tetrahydrofuran; ethanol at 120℃; for 1h; Microwave irradiation; | 13 mg |
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