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Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
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Type:Lab/Research institutions
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Min.Order:1 Gram
Negotiable
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Min.Order:1 Kilogram
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Min.Order:0
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Min.Order:1 Gram
Negotiable
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Type:Trading Company
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1,2,3,4-tetraphenyltriphenylene
hexabenzocoronene
Conditions | Yield |
---|---|
With iron(III) chloride In nitromethane; dichloromethane for 2h; Inert atmosphere; | 99.8% |
Conditions | Yield |
---|---|
With iron(III) chloride In nitromethane; dichloromethane at 20℃; for 4h; Inert atmosphere; | 95% |
With tetrabutylammonium tetrafluoroborate; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane at 20℃; Electrolysis; Inert atmosphere; Schlenk technique; | 95% |
With iron(III) chloride In nitromethane; dichloromethane for 0.5h; Inert atmosphere; | 93% |
1,3,5-tris(2'-biphenyl)ylbenzene
hexabenzocoronene
Conditions | Yield |
---|---|
With iron(III) chloride In nitromethane; dichloromethane for 1h; | 80% |
Conditions | Yield |
---|---|
at 500℃; under 0.1 Torr; | |
With aluminium trichloride; sodium chloride at 120 - 130℃; | |
at 500℃; under 0.1 Torr; |
Conditions | Yield |
---|---|
With sulfur at 320℃; |
benzo[fg]naphthacen-8-one
hexabenzocoronene
Conditions | Yield |
---|---|
With zinc(II) chloride; zinc at 330 - 350℃; |
Conditions | Yield |
---|---|
With copper at 400℃; for 1.5h; |
Conditions | Yield |
---|---|
With aluminium trichloride; copper; sodium chloride 1.) 120 deg C, 3 min; 2.) 400 deg C, 90 min; Yield given. Multistep reaction. Yields of byproduct given; |
aluminium trichloride
hexabenzo[a,cd,f,j,lm,o]perylene
hexabenzocoronene
Conditions | Yield |
---|---|
at 120 - 130℃; |
Conditions | Yield |
---|---|
With molybdenum(V) chloride In dichloromethane at 20℃; for 24h; Scholl reaction; |
hexabenzocoronene
Conditions | Yield |
---|---|
With aluminum (III) chloride; Iodine monochloride In tetrachloromethane at 80℃; for 72h; | 90% |
Conditions | Yield |
---|---|
With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin at 80℃; for 48h; Inert atmosphere; Schlenk technique; | 27% |
hexabenzocoronene
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In tetrahydrofuran at 65℃; under 37503 - 45003.6 Torr; for 168000h; | 10% |
Conditions | Yield |
---|---|
In solid heating the precursor in a sealed quartz ampules under vac. (1E-5 mbar) together with quartz plates at 400°C for 72 h, then at 800 or 650°C for 24 h; detected by mass-spectrometry; |
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