As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
About Product Technical Details (-)-PERILLALDEHYDE Chemical Properties Melting point <25 °C Boiling point 104-105 °C10
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inquiry(-)-PERILLALDEHYDE CAS:2111-75-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme
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inquiryAdvantage 1: The product passed the professional production process and quality inspection, the purity is 99% +. 2: Highly qualified engineers to provide technical documents and service. 3: We could provide sample for your test. 4: High qualit
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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CHENGDU YANXI is a comprehensive manufacturer and an international distribution of products throughout the world. Specialized in Scrap metal, Chemical raw materials, Paper products and color industry. We aim to become leading position in global dis
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp
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inquiryPerillaldehyde cas 2111-75-3Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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Conditions | Yield |
---|---|
With oxygen In 1,3,5-trimethyl-benzene at 60℃; under 760.051 Torr; for 4h; Solvent; Reagent/catalyst; | 100% |
With Iron(III) nitrate nonahydrate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen; sodium chloride In 1,2-dichloro-ethane at 20℃; for 9h; | 90% |
With tert.-butylhydroperoxide; oxygen In decane; toluene at 80℃; under 750.075 Torr; Schlenk technique; | 90% |
Conditions | Yield |
---|---|
With hydrogenchloride; aluminum isopropoxide In ethyl acetate; benzene | 84% |
Conditions | Yield |
---|---|
With Bis(N-methylpiperazinyl) aluminum hydride In tetrahydrofuran for 9h; Heating; | 78% |
Conditions | Yield |
---|---|
With 6C16H36N(1+)*2Zn(2+)*4Na(1+)*[Bi2Zn2(ZnW9O34)2](14-); urea hydrogen peroxide adduct In acetonitrile at 70℃; for 2h; Ene Reaction; | A 40% B 60% |
(+/-)-(1S,5R)-6,6-dimethylbicyclo[3.1.1]hept-2-ene-2-carbaldehyde
perillaldehyde
Conditions | Yield |
---|---|
at 380 - 400℃; beim Leiten durch ein Eisen-Rohr; |
1-Chlor-4-isopropenylcyclohexen
N,N-dimethyl-formamide
perillaldehyde
Conditions | Yield |
---|---|
(i) Li, Et2O, (ii) /BRN= 605365/; Multistep reaction; |
perillaldehyde
Conditions | Yield |
---|---|
With chromic acid levorotatory form; |
perillaldehyde
Conditions | Yield |
---|---|
With chromic acid levorotatory perillaldehyde; |
(methyl)(4-chlorocyclohex-3-en-1-yl)ketone
perillaldehyde
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: (i) Li, Et2O, (ii) /BRN= 605365/ View Scheme |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; sodium sulfite In dichloromethane; 3-chloro-benzenecarboperoxoic acid |
formaldehyd
trans-Crotonaldehyde
isoprene
A
3-methyl-1-vinylcyclohex-3-enecarbaldehyde
B
perillaldehyde
C
4-methyl-1-vinylcyclohex-3-enecarbaldehyde
Conditions | Yield |
---|---|
With pyrrolidine; propionic acid In water at 100℃; for 16h; Autoclave; |
Conditions | Yield |
---|---|
With lithium pyrrolidinoborohydride at 25℃; | 97% |
Stage #1: perillaldehyde With [Ru(2-(ethylthio)-N-[(pyridin-2-yl)methyl]ethan-1-amine)(triphenylphosphine)Cl2]; potassium tert-butylate In isopropyl alcohol under 22502.3 Torr; Autoclave; Inert atmosphere; Stage #2: With hydrogen In isopropyl alcohol at 80℃; under 22502.3 Torr; for 1h; | 96% |
With bis(triphenylphosphine)copper(I) nitrate; hydrogen; 1,4-di(diphenylphosphino)-butane; sodium hydroxide In ethanol at 50℃; under 37503.8 Torr; for 16h; Autoclave; Inert atmosphere; chemoselective reaction; | 92% |
Conditions | Yield |
---|---|
With pyrrolidine | 97% |
perillaldehyde
allylmagnesium bromide
1-(1-hydroxy-3-butenyl)-4-(1-methylethenyl)-cyclohexene
Conditions | Yield |
---|---|
In diethyl ether | 93% |
Conditions | Yield |
---|---|
In acetonitrile for 6h; Ambient temperature; | 92% |
perillaldehyde
ethyl 2-diphenylphosphono-3-(trimethylsilyl)propionate
Conditions | Yield |
---|---|
Stage #1: ethyl 2-diphenylphosphono-3-(trimethylsilyl)propionate With sodium hydride In tetrahydrofuran at 0℃; for 0.5h; Stage #2: perillaldehyde In tetrahydrofuran at -60 - 20℃; for 14.5h; Ando-Horner-Wadsworth-Emmons reaction; -; | 91% |
1-methoxy-2-methyl-1-trimethylsiloxy-1-propene
perillaldehyde
Conditions | Yield |
---|---|
With pyridine N-oxide; lithium chloride In N,N-dimethyl-formamide at 20℃; for 10h; | 91% |
With 1-methyl-1H-imidazole; lithium chloride In N,N-dimethyl-formamide at 20℃; for 10h; | 90% |
Conditions | Yield |
---|---|
With Dimethylphenylsilane In acetonitrile at 20℃; for 2h; Inert atmosphere; Green chemistry; | 91% |
Stage #1: perillaldehyde; aniline In methanol at 20℃; for 12h; Stage #2: With sodium tetrahydroborate In methanol at 20℃; for 2h; Cooling with ice; | 89% |
Stage #1: perillaldehyde; aniline In methanol for 24h; Stage #2: With sodium tetrahydroborate In methanol at 0 - 20℃; |
perillaldehyde
ethyl sodiodiethylphosphonoacetate
(E)-3-(4-Isopropenyl-cyclohex-1-enyl)-acrylic acid ethyl ester
Conditions | Yield |
---|---|
In tetrahydrofuran Ambient temperature; | 89.5% |
Conditions | Yield |
---|---|
Stage #1: perillaldehyde; N-butylamine In methanol at 20℃; for 12h; Stage #2: With methanol; sodium tetrahydroborate at 20℃; for 2h; Temperature; Reagent/catalyst; Cooling with ice; | 88% |
Stage #1: perillaldehyde; N-butylamine In methanol for 24h; Stage #2: With sodium tetrahydroborate In methanol at 0 - 20℃; |
perillaldehyde
[4-(1-methylethenyl)-1-cyclohexen-1-yl]methylamine
Conditions | Yield |
---|---|
With N,N'-bis(salicylidene)-1,2-phenylene-diaminocobalt(II); ammonia; hydrogen In water at 120℃; for 24h; Autoclave; | 87% |
perillaldehyde
4-isopropenylcyclohexene-1-carbonitrile
Conditions | Yield |
---|---|
With ammonia; oxygen In tert-Amyl alcohol at 40℃; under 750.075 Torr; for 24h; Green chemistry; | 85% |
4-phenylbut-1-en-3-yne
perillaldehyde
Conditions | Yield |
---|---|
Stage #1: 4-phenylbut-1-en-3-yne; perillaldehyde With [(1S,4R)-3-[4-(diphenylphosphino)-2,5-dimethyl-3-thienyl]-4,7,7-trimethylbicyclo[2.2.1]hept-2-en-2-yl]diphenylphosphine; copper(l) chloride; sodium t-butanolate In tetrahydrofuran at 22℃; for 8h; Inert atmosphere; Glovebox; Stage #2: With sodium perborate tetrahydrate In tetrahydrofuran at 22℃; for 3h; Inert atmosphere; Glovebox; | 79% |
[2-(acetoxymethyl)prop-2-enyl]trimethylsilane
perillaldehyde
2-(4-Isopropenyl-cyclohex-1-enyl)-4-methylene-tetrahydro-furan
Conditions | Yield |
---|---|
With triphenylphosphine; palladium diacetate In 1,4-dioxane Heating; | 71% |
Conditions | Yield |
---|---|
With acetic acid; zinc In water at 20℃; for 0.333333h; Green chemistry; | A 6% B 71% |
Conditions | Yield |
---|---|
Stage #1: perillaldehyde With iron(III) chloride In dichloromethane; water at 20℃; Stage #2: With sodium hypochlorite In dichloromethane; water at 20℃; for 0.583333h; | A 68% B 30% |
perillaldehyde
Conditions | Yield |
---|---|
With selenium(IV) oxide In ethanol for 18h; Heating; | A 66% B n/a |
Conditions | Yield |
---|---|
With Co(3,5-DitBu-Ibu-Phyrin) In chlorobenzene at 80℃; for 24h; Molecular sieve; | 50% |
Conditions | Yield |
---|---|
With [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate In 1,2-dichloro-ethane at 20℃; for 16h; Irradiation; regioselective reaction; | 48% |
perillaldehyde
4-hydroxy-2-deoxy-2-thiocoumarin
Conditions | Yield |
---|---|
ytterbium(III) trifluoromethanesulphonate In methanol Knoevenagel reaction; | A 44% B 36% |
Allyl acetate
perillaldehyde
1-(1-hydroxy-3-butenyl)-4-(1-methylethenyl)-cyclohexene
Conditions | Yield |
---|---|
With tetraethylammonium tosylate; zinc(II) chloride; bis-triphenylphosphine-palladium(II) chloride In N,N-dimethyl-formamide electrochemical reduction; | 42% |
Conditions | Yield |
---|---|
With hydrazine hydrate In water at 20℃; for 1h; | 40% |
perillaldehyde
O,O-dimethyl bismethylphosphonate
A
(Z)-4-isopropenyl-1-(2-(dimethylphosphono)-2-(trimethylsilylvinyl))cyclohexene
B
(E)-4-isopropenyl-1-(2-(dimethylphosphono)-2-(trimethylsilylvinyl))cyclohexene
Conditions | Yield |
---|---|
Stage #1: O,O-dimethyl bismethylphosphonate With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -70℃; for 0.25h; Inert atmosphere; Stage #2: perillaldehyde In tetrahydrofuran; hexane at -70℃; for 0.25h; Peterson Olefination; Inert atmosphere; Stage #3: With benzoic acid methyl ester In tetrahydrofuran; hexane at 20℃; for 12h; Reagent/catalyst; Inert atmosphere; | A 24% B 18% |
With benzoic acid methyl ester; lithium diisopropyl amide In tetrahydrofuran at -78 - 20℃; for 12.5h; Peterson Olefination; Inert atmosphere; Overall yield = 53 %; | A n/a B n/a |
Conditions | Yield |
---|---|
With triethylamine hydrochloride In 5,5-dimethyl-1,3-cyclohexadiene at 140℃; for 16h; Inert atmosphere; Enzymatic reaction; | 23% |
Conditions | Yield |
---|---|
Multistep reaction; |
perillaldehyde
p-menth-3-en-7-ol
Conditions | Yield |
---|---|
(i) Li, liq. NH3, iPrOH, Et2O, (ii) aq. H2SO4; Multistep reaction; |
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