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inquiry4-CHLOROPHENYL ISOTHIOCYANATE Basic information Product Name: 4-CHLOROPHENYL ISOTHIOCYANATE Synonyms: 4-Chlorophenyl isothiocyanate 99%;P-CHLOROPHENYL ISOTHIOCYANATE;4-Chlorophenyl isothiocyate, 99%;4-CHLOROPHENYL ISOTHIOCYANATE;AKOS BBS-0000
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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4-Chlorophenyl isothiocyanateAppearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agrochemi
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4-Chlorophenyl isothiocyanate cas 2131-55-7Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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At Capot,We can synthesize and purify your complex molecules from 100 gram to 10 tons.Appearance:Clear colorless to light yellow liquid Storage:Dry,Seal and Cool place Package:1G,5G,10G,25G,100G,250G,500G,1KG,5KG,10KG,25KG,50KG,100KG,150KG,200KG. App
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inquiry4-chlorobenzohydroximoyl chloride
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
With triethylamine; thiourea In tetrahydrofuran Ambient temperature; | 100% |
carbon disulfide
N-p-chlorophenyltriphenylphosphinimine
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
In benzene for 2h; Heating; | 96% |
potassium cyanate
5-[2-(4-bromophenyl)-2-oxoethyl]-3-(4-chlorophenyl)-2-thioxo-1,3-thiazolidin-4-one
A
2,4-bis[2-(4-bromophenyl)-2-oxoethylidene]cyclobutane-1,3-dione
B
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
In 1,4-dioxane; methanol at 90℃; for 0.416667h; | A n/a B 95% |
p-chlorophenyldithiocarbamic acid triethylamine salt
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
With iodine; triethylamine In acetonitrile at 5℃; Cooling with ice; | 94% |
With [bis(acetoxy)iodo]benzene; triethylamine In acetonitrile Cooling with ice; | 93% |
With sodium persulfate; potassium carbonate In water at 20℃; for 1h; Green chemistry; chemoselective reaction; | 85% |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In dichloromethane; water at 0 - 20℃; for 1h; | 92% |
With sodium hydrogencarbonate In dichloromethane; water at 0 - 20℃; for 1.5h; | 81% |
With sodium hydrogencarbonate In dichloromethane; water at 0 - 20℃; for 1.5h; | 81% |
4-chlorophenyldithiocarbamate sodium salt
N-phenyl-benzimidoyl chloride
A
4-Chlorophenyl isothiocyanate
B
N-Phenylbenzothioamide
Conditions | Yield |
---|---|
In diethyl ether 0 deg C to r.t.; | A 83% B 92% |
Conditions | Yield |
---|---|
Stage #1: carbon disulfide; 4-chloro-aniline With potassium carbonate In water at 40℃; for 6h; Inert atmosphere; Stage #2: With 1,3,5-trichloro-2,4,6-triazine In dichloromethane; water; N,N-dimethyl-formamide at 0℃; Inert atmosphere; Stage #3: With sodium hydroxide In dichloromethane; water pH=11; Inert atmosphere; | 92% |
Stage #1: carbon disulfide; 4-chloro-aniline With 1,4-diaza-bicyclo[2.2.2]octane In toluene at 20℃; for 8h; Stage #2: With bis(trichloromethyl) carbonate In dichloromethane at -5℃; Reflux; | 84.7% |
With potassium hydroxide at 20℃; for 1.5h; Milling; Green chemistry; | 75% |
(4-chloro-phenyl)-dithiocarbamic acid
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
With 1,1'-(ethane-1,2-diyl)dipyridinium bistribromide; triethylamine In acetonitrile Cooling with ice; | 92% |
With benzene-1,3,5-tricarboxylic acid In dichloromethane | |
With bis(trichloromethyl) carbonate In dichloromethane | |
With bis(trichloromethyl) carbonate In dichloromethane at -5℃; for 8h; Reflux; | |
With cobalt(II) chloride hexahydrate; sodium hydrogencarbonate In ethyl acetate at 20℃; for 1h; |
Conditions | Yield |
---|---|
With sodium hydroxide In toluene for 1h; Heating; | 91% |
With dilauryl peroxide In 1,2-dichloro-ethane for 1h; Reagent/catalyst; Reflux; | |
Multi-step reaction with 2 steps 1: dilauryl peroxide / 1,2-dichloro-ethane / 1 h / Reflux 2: dilauryl peroxide / 1,2-dichloro-ethane / 1 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: dilauryl peroxide / 1,2-dichloro-ethane / 1 h / Reflux 2: dilauryl peroxide / 1,2-dichloro-ethane / 1 h / Reflux View Scheme | |
With mercury(II) oxide In diethyl ether at 20℃; for 1h; |
Conditions | Yield |
---|---|
With sulfur; rhodium hydrido (PEt3)3 complex In acetone for 8h; Heating; | 87% |
With selenium; sulfur; triethylamine In tetrahydrofuran for 1h; Heating; | 83% |
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane at 20℃; for 1h; | 86% |
With trichlorosilane; triethylamine In benzene at 20℃; for 1h; Elimination; | 80% |
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
With dilauryl peroxide In 1,2-dichloro-ethane for 1h; Reflux; | 86% |
Conditions | Yield |
---|---|
With bis(trichloromethyl) carbonate; sulfur; triethylamine; selenium In dichloromethane for 7h; Heating; | 85% |
Multi-step reaction with 2 steps 1.1: KOH / dimethylformamide / 25 - 28 °C 1.2: 42 percent / dimethylformamide / 10 - 40 °C 2.1: sulfuryl chloride View Scheme |
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
With iron(III) chloride; sodium acetate In acetone at 20℃; for 2h; | 85% |
With bis(trichloromethyl) carbonate In dichloromethane at 20℃; for 4h; | |
With p-toluenesulfonyl chloride for 48h; Inert atmosphere; |
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
With triethylamine; dimethylsilicon dichloride In dichloromethane at 20℃; for 4h; | 84% |
With bis(trichloromethyl) carbonate In chloroform at 0 - 20℃; for 4.5h; | |
With bis(trichloromethyl) carbonate In chloroform at 20℃; for 10h; | |
With bis(trichloromethyl) carbonate In chloroform for 1h; | |
With bis(trichloromethyl) carbonate In chloroform at -10 - 20℃; for 0.5h; |
p-chlorophenyl isocyanide
A
(diphenylmethyl)cyclopentane
B
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile) In toluene at 110℃; for 1h; | A 80% B n/a |
(trifluoromethyl)trimethylsilane
4-chloro-aniline
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
With sulfur; potassium fluoride In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 80% |
trifluoromethane sulfonyl chloride
4-chloro-aniline
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
With triphenylphosphine; sodium iodide In N,N-dimethyl-formamide at 20℃; for 4h; Inert atmosphere; | 80% |
4-chloro-aniline
phenylcarbonochloridothioate
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
In toluene at 115℃; for 24h; Green chemistry; | 76% |
With sodium hydroxide In dichloromethane at 0 - 20℃; for 73h; | 47% |
Conditions | Yield |
---|---|
With dilauryl peroxide In 1,2-dichloro-ethane for 1h; Reflux; | A 7% B 75% |
(4-Chloro-phenyl)-[1,3]dithietan-2-ylidene-amine
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In chloroform 1) 1 h, 10 deg C, 2) 2 h, room temp.; | 72% |
Conditions | Yield |
---|---|
With copper(l) iodide; aniline; sodium hydroxide In tetrahydrofuran at 100℃; for 12h; Reagent/catalyst; | 66.7% |
carbon disulfide
N-(4-chlorophenyl)-2,2,2-trifluoroacetamide
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
With sodium hydroxide; potassium carbonate In acetonitrile at 25℃; for 1.5h; | 55% |
sodium thiocyanide
A
4-chlorophenyl thiocyanate
B
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
With copper In methanol at 20 - 25℃; | A 35% B 35% |
potassium cyanate
3-(4-chloro-phenyl)-2-thioxo-thiazolidin-4-one
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
In 1,4-dioxane; methanol at 90℃; for 0.416667h; | 35% |
1,2,2-trifluorostyrene
p-chlorobenzenediazonium tetrafluoroborate
potassium thioacyanate
A
4-chlorophenyl thiocyanate
B
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
at -30 - -15℃; | A n/a B n/a C 30% |
p-chlorobenzenediazonium tetrafluoroborate
potassium thioacyanate
A
4-chlorophenyl thiocyanate
B
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
With 1,2,2-trifluorostyrene at -30 - -15℃; | A n/a B n/a C 30% |
O-(4-methoxyphenyl) N-4-chlorophenylthioncarbamate
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
With potassium chloride; water at 25℃; Rate constant; pH=8.5-11.5; |
1-(4-chloranilino-thiocarbonyl)-benzimidazolidine-2-thione
A
2,3-dihydrobenzimidazol-2-thione
B
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane for 16h; Heating; | A 0.9 g B 1.0 g |
Conditions | Yield |
---|---|
With ammonium hydroxide In water; acetonitrile at 20℃; for 3h; | 100% |
With ammonium hydroxide In 1,4-dioxane at 20℃; for 2h; Addition; | 78% |
With ammonia In 1,4-dioxane; water at 0 - 20℃; for 2h; | 78% |
2-(1H-benzo[d]imidazol-2-yl)acetohydrazide
4-Chlorophenyl isothiocyanate
C16H14ClN5OS
Conditions | Yield |
---|---|
In ethanol for 0.5h; Heating; | 100% |
In ethanol for 0.5h; Heating; |
4-Chlorophenyl isothiocyanate
anthranilic acid
3-(4-chlorophenyl)-2-thioxo-2,3-dihydro-1H-quinazolin-4-one
Conditions | Yield |
---|---|
In acetic acid for 16h; Reflux; | 100% |
at 90℃; Green chemistry; | 75% |
In ethanol Heating; | |
With acetic acid |
4-Chlorophenyl isothiocyanate
4-benzylamino-2-phenyl-2-oxazoline
1-benzyl-3-(4-chloro-phenyl)-1-(2-phenyl-4,5-dihydro-oxazol-4-yl)-thiourea
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 1h; | 100% |
2,3,4,5-tetrahydro-1H-3-benzazepine
4-Chlorophenyl isothiocyanate
N-(4-Chlorophenyl)-1 ,2,4,5-tetrahydro-3H-3-benzazepine-3-carbothioamide
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1h; | 100% |
tetrahydrobetacarboline
4-Chlorophenyl isothiocyanate
N-(4-chlorophenyl)-1,3,4,9-tetrahydro-2H-β-carboline-2-carbothioamide
Conditions | Yield |
---|---|
In ethanol | 100% |
2-(2,6-dichlorophenyl)acetohydrazide
4-Chlorophenyl isothiocyanate
N-(4-chlorophenyl)-2-(2-(2,6-dichlorophenyl)acetyl)hydrazinecarbothioamide
Conditions | Yield |
---|---|
In ethanol for 5h; Reflux; | 100% |
In ethanol for 5h; Reflux; | 100% |
4-Chlorophenyl isothiocyanate
N-methylaniline
N-methyl-N-phenyl-N'-p-chlorophenylthiourea
Conditions | Yield |
---|---|
In ethanol at 25 - 30℃; for 1h; | 100% |
4-(1-benzyl-1H-benzimidazol-2-yl)methyl phenoxy carboxylic acid hydrazide
4-Chlorophenyl isothiocyanate
1-benzyl-2-<4-(p-chlorophenyl thiocarbamoylhydrazinocarbonyl)phenoxymethyl>-1H-benzimidazole
Conditions | Yield |
---|---|
In ethanol for 1h; Heating; | 99% |
4-Chlorophenyl isothiocyanate
1,2-diamino-benzene
N1-(2-aminophenyl)-N2-(4-chlorophenyl)thiourea
Conditions | Yield |
---|---|
In methanol for 0.5h; | 99% |
In tetrachloromethane for 1.5h; Heating; | |
In acetonitrile | |
In acetonitrile at 20℃; for 0.5h; | |
In dichloromethane at 25℃; |
2-(benzo[d]oxazol-2-yl)acetonitrile
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
Stage #1: 2-(benzo[d]oxazol-2-yl)acetonitrile; 4-Chlorophenyl isothiocyanate With potassium hydroxide In N,N-dimethyl-formamide at 20℃; for 3h; Stage #2: With hydrogenchloride In water; N,N-dimethyl-formamide at 0℃; pH=3 - 4; | 99% |
2-iodophenylamine
4-Chlorophenyl isothiocyanate
N-(4-chlorophenyl)benzo[d]thiazol-2-amine
Conditions | Yield |
---|---|
With copper(II) nitrate trihydrate; N,N,N,N,-tetramethylethylenediamine; sodium hydrogencarbonate In water at 20℃; for 2h; | 99% |
With tetrabutylammomium bromide; copper(I) bromide In dimethyl sulfoxide at 40℃; for 20h; | 98% |
With iron(III) trifluoride; 1,10-Phenanthroline; triethylamine In dimethyl sulfoxide at 80℃; for 2h; | 96% |
2-iodo-4-methylphenol
4-Chlorophenyl isothiocyanate
4-chloro-N-(5-methylbenzo[d][1,3]oxathiol-2-ylidene)benzenamine
Conditions | Yield |
---|---|
With copper(II) nitrate trihydrate; N,N,N,N,-tetramethylethylenediamine; sodium hydrogencarbonate In water at 20℃; for 4h; | 99% |
With 1,4-diaza-bicyclo[2.2.2]octane; 1,10-Phenanthroline; copper dichloride In water at 80℃; for 24h; Inert atmosphere; | 95% |
Stage #1: 2-iodo-4-methylphenol With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate at 40℃; for 1h; Ionic liquid; Inert atmosphere; Green chemistry; Stage #2: 4-Chlorophenyl isothiocyanate at 85℃; for 15h; Ionic liquid; Inert atmosphere; Green chemistry; | 91% |
N1-(2-aminophenyl)-N2-phenylurea
4-Chlorophenyl isothiocyanate
N1-[N-(4-chlorophenyl)thiocarbamoyl]-N2-[N-phenylcarbamoyl]-1,2-diaminobenzene
Conditions | Yield |
---|---|
In methanol for 3h; | 99% |
N1-(4-aminophenyl)-N2-(4-methoxyphenyl)thiourea
4-Chlorophenyl isothiocyanate
N1-[N-(4-chlorophenyl)thiocarbamoyl]-N2-[N-(4-methoxyphenyl)thiocarbamoyl]-1,4-diaminobenzene
Conditions | Yield |
---|---|
In methanol for 0.5h; | 99% |
4-Chlorophenyl isothiocyanate
N1-[N-(4-chlorophenyl)thiocarbamoyl]-N2-[N-(4-methoxyphenyl)thiocarbamoyl]-1,2-diaminobenzene
Conditions | Yield |
---|---|
In methanol for 3h; | 99% |
4-Chlorophenyl isothiocyanate
1,2-diamino-benzene
N1,N2-bis[N-(4-chlorophenyl)thiocarbamoyl]-1,2-diaminobenzene
Conditions | Yield |
---|---|
In methanol for 3h; | 99% |
4-amino-3,4-dihydro-2,2-dimethyl-6-ethylsulfonylamino-2H-1-benzopyran
4-Chlorophenyl isothiocyanate
N-4-chlorophenyl-N'-(6-ethylsulfonylamino-3,4-dihydro-2,2-dimethyl-2H-1-benzopyran-4-yl)thiourea
Conditions | Yield |
---|---|
In dichloromethane for 0.5h; Reflux; | 99% |
N-(2-aminoethyl)-3-(2-(2,4-dichlorophenoxy)phenyl)thiophene-2-sulfonamide
4-Chlorophenyl isothiocyanate
N-(2-(3-(4-chlorophenyl)carbamothioylamino)ethyl)-3-(2-(2,4-dichlorophenoxy)phenyl)thiophene-2-sulfonamide
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; | 99% |
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
With silica gel In dichloromethane at 20℃; for 2h; Inert atmosphere; | 99% |
N-deacetyl-10-methylamino-10-demethoxycolchicine
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; | 99% |
5-(4-chlorophenyl)-2H-tetrazol-2-ylacethydrazide
4-Chlorophenyl isothiocyanate
1-<5-(4-chlorophenyl)-2H-tetrazol-2-ylacetyl>-4-(4-chlorophenyl)thiosemicarbazide
Conditions | Yield |
---|---|
In ethanol for 1h; Heating; | 98% |
4-Chlorophenyl isothiocyanate
2-Hydroxybenzoylhydrazine
4-(4-chlorophenyl)-1-(2-hydroxybenzoyl)-3-thiosemicarbazide
Conditions | Yield |
---|---|
In ethanol for 1h; Heating; | 98% |
In ethanol for 0.25h; Reflux; | 85% |
In methanol at 20℃; under 760.051 Torr; for 24h; | 20% |
4-Chlorophenyl isothiocyanate
α-(2-chlorophenyloxy)propionyl hydrazine
C16H15Cl2N3O2S
Conditions | Yield |
---|---|
In ethanol for 3h; Heating; | 98% |
4-methoxy-aniline
4-Chlorophenyl isothiocyanate
N-(4-chlorophenyl)-N’-(4-methoxyphenyl)thiourea
Conditions | Yield |
---|---|
at 20℃; | 98% |
3-aminopropyl-dimethyl-phosphine oxide
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
In dichloromethane for 3.16667h; | 98% |
N-benzylaminomethyl-dimethylphosphine oxide
4-Chlorophenyl isothiocyanate
Conditions | Yield |
---|---|
In dichloromethane | 98% |
(R/S)-4-amino-6-tert-butyloxycarbonylamino-3,4-dihydro-2,2-dimethyl-2H-1-benzopyran
4-Chlorophenyl isothiocyanate
(RS)-N-4-chlorophenyl-N'-(6-tert-butyloxycarbonylamino-3,4-dihydro-2,2-dimethyl-2H-1-benzopyran-4-yl)thiourea
Conditions | Yield |
---|---|
In dichloromethane for 0.5h; | 98% |
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