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inquiryProduct Name: 1,1 bis(di-isopropylphosphine)ferrocene palladium dichloride Synonyms: PdCl2(dippf);1,1 bis(di-isopropylphosphine)ferrocene palladium dichloride;Dichloro[1,1'-bis(di-i-propylphosphino)ferrocene]palladium (II), 99%;1,1′-B
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inquiry1,1 bis(di-isopropylphosphine)ferrocene palladium dichloride CAS:215788-65-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediate
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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1,1-BIS(DI-ISOPROPYLPHOSPHINE)FERROCENE PALLADIUM(II) CHLORIDECASAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiry1,1'-bis(diisopropylphosphino)ferrocene
dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)
Conditions | Yield |
---|---|
With HCl In diethyl ether; ethanol PdCl2 suspn. in EtOH treated with conc. HCl, stirred at 50°C for30 min, filtered, Fe complex (1 equiv.) soln. in Et2O added at 20°C, stirred for 10 min; crystd. at -35°C, filtered, washed (H2O), dried (vac.); elem. anal.; | 38% |
dichloromethane
dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)
4-mercaptopyridine-3-carboxylic acid
Conditions | Yield |
---|---|
With triethylamine In dichloromethane byproducts: (C2H5)3NHCl; (N2), mixed, stirred at room temp. for 3 h; filtered, pptd.(hexane), recrystd.(CH2Cl2/hexane), elem. anal., IR, NMR,MAS, XRD; | 79% |
dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)
Thiosalicylic acid
[1,1'-bis(diisopropylphosphino)ferrocene]palladium(II) thiosalicylate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane byproducts: (C2H5)3NHCl; (N2), mixed, stirred at room temp. for 3 h; filtered, pptd.(hexane), recrystd.(CH2Cl2/hexane), elem. anal., IR, NMR,MAS, XRD; | 68% |
ortho-mercaptophenol
dichloromethane
dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)
Conditions | Yield |
---|---|
With triethylamine In dichloromethane byproducts: (C2H5)3NHCl; (N2), mixed, stirred at room temp. for 3 h; filtered, pptd.(hexane), recrystd.(CH2Cl2/hexane), elem. anal., IR, NMR,MAS, XRD; | 70% |
3,4-dimercaptotoluene
dichloromethane
dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)
[1,1'-bis(diisopropylphosphino)ferrocene]palladium(II) 3,4-toluenedithiolate * CH2Cl2
Conditions | Yield |
---|---|
With triethylamine In dichloromethane byproducts: (C2H5)3NHCl; (N2), mixed, stirred at room temp. for 3 h; filtered, pptd.(hexane), recrystd.(CH2Cl2/hexane), elem. anal., IR, NMR,MAS, XRD; | 56% |
3,6-dichlorobenzene-1,2-dithiol
dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)
[1,1'-bis(diisopropylphosphino)ferrocene]palladium(II) 3,6-dichloro-1,2-benzenedithiolate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane byproducts: (C2H5)3NHCl; (N2), mixed, stirred at room temp. for 3 h; filtered, pptd.(hexane), recrystd.(CH2Cl2/hexane), elem. anal., IR, NMR,MAS, XRD; | 49% |
dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)
1,2-benzenedithiole
[1,1'-bis(diisopropylphosphino)ferrocene]palladium(II) 1,2-benzenedithiolate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane byproducts: (C2H5)3NHCl; (N2), mixed, stirred at room temp. for 3 h; filtered, pptd.(hexane), recrystd.(CH2Cl2/hexane), elem. anal., IR, NMR,MAS, XRD; | 52% |
dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 0.5h; Inert atmosphere; Schlenk technique; | 69% |
dichloromethane
dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)
thiophenol
Conditions | Yield |
---|---|
With Et3N In toluene byproducts: Et3NHCl; under N2, Pd-complex was added to toluene soln. of thiophenol; Et3NHCl was filtered off, filtrate was evapd. to dryness, residue was recrystd. from CH2Cl2/hexane (1:2), hexane was layered onto CH2Cl2 soln., slow diffusion of hexane at 258 K; elem. anal.; | 68% |
bis(acetonitrile)dichloroplatinum(II)
dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)
[Pt(dippf)Cl2]
Conditions | Yield |
---|---|
In dichloromethane under Ar atm. mixt. (PtCl2(MeCN)2) and dippf in CH2Cl2 was stirred at room temp. for 1 h; soln. was concd., hexane was added, ppt. was filtered, washed with etherand dried in vacuo; elem. anal.; | 32% |
dichloromethane
dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)
silver trifluoromethanesulfonate
acetonitrile
Conditions | Yield |
---|---|
In dichloromethane; acetonitrile byproducts: AgCl; N2; add. of acetonitrile soln. of silver salt to dichloromethane soln. of Pd complex, stirring for 5 min at room temp.; filtration, evapn. at room temp., recrystn. from CH2Cl2; elem. anal.; | 60% |
dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)
sodium iodide
Conditions | Yield |
---|---|
In acetone for 22h; Inert atmosphere; Schlenk technique; | 48% |
dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II)
water
silver(I) 4-methylbenzenesulfonate
[Pd(H2O)(1,1'-bis(diisopropylphosphino)ferrocene)(tosylato)](tosylate)
Conditions | Yield |
---|---|
In dichloromethane (N2); using Schlenk techniques; addn. of AgO3SC6H4CH3 to soln. of PdCl2(Fe(C5H4P(i-Pr)2)2) in CH2Cl2 at room temp.; stirring at room temp. for 2h; filtration, concn., addn. of Et2O, pptn., filtration, washing with Et2O,drying under N2; elem. anal.; |
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