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Synthetic route

: 421-59-0
trifluoromethyldiiodophosphine

A: sodium phosphite

B: 75-46-7
trifluoromethan

C: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
With NaOH In water 20°C (24 h); hydrolysis;	A n/a B 99.5% C 100%

...Expand

: 1020-31-1
3,5-Di-tert-butylcatechol

: 13450-91-4
gallium(III) iodide

A: gallium(III) tris(3,5-di-tert-butyl-1,2-semibenzoquinonate)

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
With NaOH In toluene byproducts: H2; N2 atmospher; treatment of catechol and NaOH in toluene (stirring, 30 min), dropwise addn. of GaI in toluene (4 h); sepn. of NaI (filtration off, drying), collectin of Ga-complex by evapn. of filtrate;	A 97% B n/a

...Expand

: 108-89-4
picoline

: 13510-35-5
indium(III) iodide

: 4679-12-3, 61373-02-2
sodium 3,5-di-tert-butyl-o-benzosemiquinolate

: [InI(((CH3)3C)2C6H2O2)(CH3C5H4N)2]2*2(CH3)2NCHO

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
With NaH In tetrahydrofuran byproducts: H2; N2, soln. of semiquinonate sodium salt added dropwise over 1 h to a soln. of In-salt, stirred for 2 h at room temp., NaI removed by filtrn., excess 4-picoline added to the filtrate; collected, dried, recrystd. (DMF); elem. anal.; further intermediates and other products. discussed;	A 50% B 92%

...Expand

: bis(cyclopentadienyl)zirconium diiodide

: 128-04-1
sodium dimethyldithiocarbamate

A: bis(η5-cyclopentadienyl)(N,N-dimethyldithiocarbamato)iodozirconium(IV)

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
In dichloromethane Kinetics; React. of starting complexes (CH2Cl2, 12 h, room temp., anhydrous conditions, dry Ar).; Crystn. from CH2Cl2 under hexane (-15°C), elem. anal., variable-temp. NMR spectroscopy.;	A 88% B n/a

...Expand

: Ma[W(CO)3(η5-cyclopentadienyl)]*2(DME)

: (C6H5)2Sn(C(CH3)3)I

A: 1-tert-butyl-1-((η(5)-cyclopentadienyl)tricarbonyltungsten)diphenyltin

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
In tetrahydrofuran; toluene N2-atmosphere; stirring (room temp., overnight), evapn. (reduced pressure), toluene addn., stirring (1 h), filtering, concg.; n-hexane addn., crystn. (fridge); elem. anal.;	A 83% B n/a

...Expand

: 15602-40-1
sodium hexacarbonyltantalate*THF

: 18820-83-2
pyridine hydroiodide

A: 112713-58-3
tetracarbonyl{1,2-bis(diphenylphosphino)ethane}iodotantalum

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
With C2H4(P(C6H5)2)2 In tetrahydrofuran; toluene byproducts: C5H5N, CO, H2; Treating of suspn. of diphos and (H-py)I in THF with Ta-complex at room temp. under a CO atmosphere.; Immediate react. with evolution of CO and H2 (gas chromy.) obsd. Stirring (2 h, room temp.), removal of THF (vac., room temp.), dissolving of residue (toluene, CO), stirring (2 h), filtn., treating with n-heptane. Sepn. of microcryst., elem. anal.;	A 79% B n/a

Yield

With C2H4(P(C6H5)2)2 In tetrahydrofuran; toluene byproducts: C5H5N, CO, H2; Treating of suspn. of diphos and (H-py)I in THF with Ta-complex at room temp. under a CO atmosphere.; Immediate react. with evolution of CO and H2 (gas chromy.) obsd. Stirring (2 h, room temp.), removal of THF (vac., room temp.), dissolving of residue (toluene, CO), stirring (2 h), filtn., treating with n-heptane. Sepn. of microcryst., elem. anal.;

A 79%
B n/a

...Expand

: 15602-39-8
sodium{(THF)2.3} hexacarbonylniobate

: 18820-83-2
pyridine hydroiodide

A: 112713-57-2
tetracarbonyl{1,2-bis(diphenylphosphino)ethane}iodoniobium

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
With C2H4(P(C6H5)2)2 In tetrahydrofuran; toluene byproducts: C5H5N, CO, H2; Treating of suspn. of diphos and (H-py)I in THF with Nb-complex at room temp. under a CO atmosphere.; Immediate react. with evolution of CO and H2 (gas chromy.) obsd. Stirring (2 h, room temp.), removal of THF (vac., room temp.), dissolving of residue (toluene, CO), stirring (2 h), filtn., treating with n-heptane. Sepn. of microcryst., elem. anal.;	A 76% B n/a

Yield

With C2H4(P(C6H5)2)2 In tetrahydrofuran; toluene byproducts: C5H5N, CO, H2; Treating of suspn. of diphos and (H-py)I in THF with Nb-complex at room temp. under a CO atmosphere.; Immediate react. with evolution of CO and H2 (gas chromy.) obsd. Stirring (2 h, room temp.), removal of THF (vac., room temp.), dissolving of residue (toluene, CO), stirring (2 h), filtn., treating with n-heptane. Sepn. of microcryst., elem. anal.;

A 76%
B n/a

...Expand

: [(CH(NC6H3(CH(CH3)2)2)2)2SmI2(C4H8O)](1-)*Na(1+)*5C4H8O=[(CH(NC6H3(CH(CH3)2)2)2)2SmI2(C4H8O)](Na(C4H8O)5)

A: samarium triiodide(THF)3.5

B: [Sm(N,N′-bis(2,6-diisopropylphenyl)formamidinate)3]

C: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
In hexane dissolved in warm hexane (35°C); filtered, volatiles removed (vac.), extd. (toluene), cooled to -10°C overnight; elem. anal.;	A n/a B 72% C n/a

...Expand

: 16940-66-2
sodium tetrahydroborate

A

B

C diborane: diborane

Conditions

Conditions	Yield
In dimethoxyethane (DME) at 20℃; for 1h;	A n/a B n/a C 70%

...Expand

: 16940-66-2
sodium tetrahydroborate

: 33797-51-2
eschenmoser's salt

A: 1231953-83-5
trimethylamine borane

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
In diethyl ether React. of starting materials in Et2O (vac. distd., -196°C), warming to 25°C, and stirring overnight.; Distn. of volatile materials into a -196°C U-trap and fractionalcondensation at -68 and -196°C yields Me3N*BH3 in the -68°C trap.;	A 45.6% B n/a
In neat (no solvent) Mixing of starting powders with vigorous stirring at 25°C under N2.; Condensing of volatile materials in a -196°C U-trap, results after 2 h in a small amt. of a solid.;

...Expand

: 15602-39-8
sodium hexacarbonylniobate*THF

A: 112713-57-2
tetracarbonyl{1,2-bis(diphenylphosphino)ethane}iodoniobium

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
With C2H4(P(C6H5)2)2; I2 In tetrahydrofuran; toluene byproducts: CO; Treating of suspn. of starting compd. in THF with I2 (-78°C, N2 or Ar). Evolution of gas and formation of red soln. takes place upon mixing. Addn. of diphos at -50°C, stirring (room temp.).; Removal of solvent (vac.), dissolving of residue in toluene, filtn., treatment with n-heptane, cooling (-30°C), elem. anal.;	A 43% B n/a

: 15602-40-1
sodium{(THF)2.8} hexacarbonyltantalate

A: 112713-58-3
tetracarbonyl{1,2-bis(diphenylphosphino)ethane}iodotantalum

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
With C2H4(P(C6H5)2)2; I2 In tetrahydrofuran; toluene byproducts: CO; Treating of suspn. of starting compd. in THF with I2 (-78°C, N2 or Ar). Evolution of gas and formation of red soln. takes place upon mixing. Addn. of diphos at -50°C, stirring (1 h, room temp.).; Removal of solvent (vac.), dissolving of brown residue in toluene, filtn., treatment with n-heptane, cooling (-30°C), elem. anal.;	A 42% B n/a

: 15602-41-2
sodium hexacarbonylvanadate

A: 36643-83-1
tetracarbonyl{1,2-bis(diphenylphosphino)ethane}iodovanadium

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
With C2H4(P(C6H5)2)2; I2 In tetrahydrofuran; toluene byproducts: CO; Treating of suspn. of starting compd. in THF with I2 (-78°C, N2 or Ar). Evolution of gas and formation of red soln. takes place upon mixing. Addn. of diphos at -50°C, slow warming of mixt. up to -10°C.; Removal of solvent (vac., -10°C), dissolving of residue in toluene, filtn. (-10°C). Addn. of cold n-heptane causes sepn. of brown solid. Isolation by filtn., recrystn. from toluene/n-heptane, elem. anal.;	A 24% B n/a

Yield

With C2H4(P(C6H5)2)2; I2 In tetrahydrofuran; toluene byproducts: CO; Treating of suspn. of starting compd. in THF with I2 (-78°C, N2 or Ar). Evolution of gas and formation of red soln. takes place upon mixing. Addn. of diphos at -50°C, slow warming of mixt. up to -10°C.; Removal of solvent (vac., -10°C), dissolving of residue in toluene, filtn. (-10°C). Addn. of cold n-heptane causes sepn. of brown solid. Isolation by filtn., recrystn. from toluene/n-heptane, elem. anal.;

A 24%
B n/a

: ammonium bromide

: ammonium iodide

: 7757-82-6
sodium sulfate

A: 7681-82-5
sodium iodide

B: 7647-15-6
sodium bromide

Conditions

Conditions	Yield
In not given complete reaction on twofold or threefold evaporating Na2SO4 with a mixture of NH4I and NH4Br;;
In not given complete reaction on twofold or threefold evaporating Na2SO4 with a mixture of NH4I and NH4Br;;

...Expand

: sodium phosphite

: silver(I) iodide

A: 7440-22-4
silver

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
byproducts: PH3, Na5P3O10; at 380.degrre.C in sealed glass tube, in 40-60 min;

...Expand

: sodium azide

: 7553-56-2
iodine

A: 7727-37-9
nitrogen

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
hydrogen sulfide In water Kinetics; catalysts: solid anorganic sulfids and in acids insol. sulfids or H2S in mineralwater;
mercaptoacetic acid In water
pentathionate(2-) In water Kinetics;

...Expand

: sodium azide

: iodine

: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
With sodium sulfide In not given byproducts: N2; adding Na2S*9H2O to neutral or acetic acidic soln. of J2 and NaN3;;
With sodium thiosulfate In not given byproducts: N2; adding sodium thiosulfate to neutral or acetic acidic soln. of J2 and NaN3;;
With Na2S9H2O In not given byproducts: N2; adding Na2S9H2O to neutral or acetic acidic soln. of J2 and NaN3;;
With sodium thiosulfate In not given byproducts: N2; adding sodium thiosulfate to neutral or acetic acidic soln. of J2 and NaN3;;

: 7553-56-2
iodine

: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
With charcoal; double silicate In neat (no solvent) reduction with charcoal in I2 atmosphere at elevated temperature;;
With pyrographite In neat (no solvent) reduction with charcoal in I2 atmosphere at elevated temperature;;

: 7553-56-2
iodine

: sodium thiosulfate

: 1310-73-2
sodium hydroxide

A: 7757-82-6
sodium sulfate

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
In water sulfate precipitates or can be removed with BaI2; no formation of iodate;;
In water sulfate precipitates or can be removed with BaI2; no formation of iodate;;

...Expand

: 7553-56-2
iodine

: sodium fluoride

: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
In water byproducts: F2; presence of Na2CO3;;

: 7553-56-2
iodine

: 7647-14-5
sodium chloride

: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
In not given on presence of water;;

: 7553-56-2
iodine

: 1310-73-2
sodium hydroxide

: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
With Na-amlgam
preparation of very pure crystals; purification by iron iodide method;
In water; Petroleum ether treatment of I2 in petroleum ether (by extractn. of I2-containing solns. generated by electrolysis) with aq. Na2CO3;;
With Na2S2O3 In not given byproducts: Na2SO4, H2O; treating soln. of Na2S2O3 alternating with excess of both I2 and NaOH while heating;; fractionate crystallisation;;
With sodium thiosulfate In not given byproducts: Na2SO4, H2O; treating soln. of Na2S2O3 alternating with excess of both I2 and NaOH while heating;; fractionate crystallisation;;

: 7553-56-2
iodine

: 1310-73-2
sodium hydroxide

A: 497-19-8
sodium carbonate

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
In not given treating soln. of NaOH with I2 and heating residue with charcoal;;
In not given treating soln. of NaOH with I2 and heating residue with charcoal;;

...Expand

: 7553-56-2
iodine

: 7632-00-0
sodium nitrite

A: 10102-43-9
nitrogen(II) oxide

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
With sulfur dioxide In methanol byproducts: CH3OSO3H;	A >99 B >99
With SO2 In methanol byproducts: CH3OSO3H;	A >99 B >99

...Expand

: 7553-56-2
iodine

: 497-19-8
sodium carbonate

: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
With sodium hydrogensulfite; sodium sulfite In water boiling I2-containing absorption-coal with Na2CO3-soln., formation of a iodide/iodate-mixture, reduction of iodate with Na2SO3 and NaHSO3;;
With formic acid In neat (no solvent) heating Na2CO3 and I2 in presence of HCO2H;; product free from iodate;;
With sodium sulfite; starch In water absorption of I2 with starch from I2-containing H2O, treatment with Na2CO3 and Na2SO3;;

: sodium peroxide

: 7553-56-2
iodine

A: sodium iodate

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
In neat (no solvent) byproducts: O2; heating Na2O2 in I2 vapor;;
In neat (no solvent) heating;;
In water concd. aq. soln.;;
In neat (no solvent) byproducts: O2; heating Na2O2 in I2 vapor;;

...Expand

: sodium sulfide

: 7553-56-2
iodine

A: 7704-34-9
sulfur

B: 7681-82-5
sodium iodide

Conditions

Conditions	Yield
In water reaction of aq. Na2S with solid I2;;
In water reaction of aq. Na2S with I2 solution;;
In water reaction of aq. Na2S with I2 solution;;
In water reaction of aq. Na2S with solid I2;;

...Expand

: 7790-99-0
Iodine monochloride

: sodium thiosulfate

A: sodium tetrathionate

B: 7681-82-5
sodium iodide

C: 7647-14-5
sodium chloride

Conditions

Conditions	Yield
In not given in concd. HCl soln., sulfate formed, too;

...Expand

: 7790-99-0
Iodine monochloride

: sodium thiosulfate

A: 7757-82-6
sodium sulfate

B: 7681-82-5
sodium iodide

C: 7647-14-5
sodium chloride

Conditions

Conditions	Yield
In not given in concd. HCl soln.;

...Expand

: 7681-82-5
sodium iodide

: 7553-56-2
iodine

Conditions

Conditions	Yield
With phosgene In acetone at 20℃; for 0.25h; Reagent/catalyst;	100%
With Fe3+-montmorillonite; propionic acid at 25℃; for 6h;
With propionic acid; K 10-montmorillonite; FeCl3; mixture of, dried at 120 degrees C, grounded at 25℃; for 6h;

: 7681-82-5
sodium iodide

: 14900-04-0
triiodide ion

Conditions

Conditions	Yield
With sodium acetate; acetic acid In ethanol; N,N-dimethyl-formamide Kinetics; byproducts: C6H9(OH)(CON(CH3)C6H10N), H2O; aerobic, 30°C; detected spectrophotometrically;	100%
With methyl α-hydroperoxy-α,α-diphenylacetate; sodium acetate; acetic acid In ethanol; N,N-dimethyl-formamide Kinetics; byproducts: (C6H5)2C(COOCH3)OH, H2O; aerobic, 30°C; detected spectrophotometrically;	100%
With sodium persulfate In decane; water Kinetics; investigation of oxidn. of NaI with Na2S2O8 in H2O/decane/sodium bis(2-ethylhexyl)sulfosuccinate microemulsion followed spectrophotometrically at 355 nm (298 °K, various concns. and ionic strength);

: 97128-27-3
Os(η(6)-p-cymene)Cl2(PMe3)

: 7681-82-5
sodium iodide

: 97128-36-4
(η(6)-p-cymene)OsI2(trimethylphosphine)

Conditions

Conditions	Yield
In methanol; dichloromethane 25°C, 6 h, CH2Cl2:CH3OH=20:1; elem. anal.;	100%

: {(C5Me5)rhodium(III)(methyl isocyanide)dichloride}

: 7681-82-5
sodium iodide

: {(C5Me5)rhodium(III)(methyl isocyanide)diiodide}

Conditions

Conditions	Yield
In acetone The rhodium dichloride complex and NaI (10-fold excess) are dissolved in acetone and refluxed for 0.5 h.; solvent removal under vac., addn. of CH2Cl2, filtn., residual NaI is washed (CH2Cl2), the combined washings are concentrated and layered (hexane), elem. anal.;	100%

: (1-hexadecyl-1,4,8,11,-tetra-azacyclotetradecane)nickel(II) perchlorate

: 7681-82-5
sodium iodide

: (1-hexadecyl-1,4,8,11,-tetra-azacyclotetradecane)nickel(II) iodide

Conditions

Conditions	Yield
In dichloromethane; water A CH2Cl2 layer of Ni(HNC2H4NHC3H6NHC2H4N(C16H33)C3H6)(ClO4)2 is equilibrated with an aq. layer of NaI.; The ClO4(1-) ions are quantitatively replaced by the I(1-) ions forming the complex Ni(HNC2H4NHC3H6NHC2H4N(C16H33)C3H6)I2.;	100%

: 81353-33-5
m-carboran-9-yl(phenyl)iodonium tetrafluoroborate

: 7681-82-5
sodium iodide

: 81353-34-6
phenyl-9-m-carboranyliodonium iodide

Conditions

Conditions	Yield
In water; acetone The precipitated iodide was washed with water and ether and dried in the dark. Elem. anal.;	100%

: 81353-28-8
phenyl-9-o-carboranyliodonium tetrafluoroborate

: 7681-82-5
sodium iodide

: 81353-29-9
phenyl-9-0-carboranyliodonium iodide

Conditions

Conditions	Yield
In water; acetone The precipitated iodide was washed with water and ether and dried in the dark. Elem. anal.;	100%

: [C5H5Rh(P(CH3)3)2(C2H4)](2+)*2BF4(1-)*CH3NO2=[C5H5Rh(P(CH3)3)2(C2H4)](BF4)2*CH3NO2

: 7681-82-5
sodium iodide

: 103093-04-5
[C5H5Rh(P(CH3)3)2I](1+)*BF4(1-)=[C5H5Rh(P(CH3)3)2I]BF4

Conditions

Conditions	Yield
In methanol N2; stirring (55°C, 5 h), cooling (room temp.); solvent removal, dissolving (MeNO2), filtration, pptn. on ether addn., filtration, washing (ether), drying (vac.);	100%

: 55839-76-4, 173829-27-1, 173829-26-0
diag-(η(5)-C5H4Me)Re(CO)2Br2

: 7681-82-5
sodium iodide

: 185566-67-0, 185630-64-2
diag-(η(5)-C5H4Me)Re(CO)2I2

Conditions

Conditions	Yield
In acetone N2-atmosphere; excess NaI; solvent removal, drying (vac., 25°C, then 100-105°C, 18 h);	100%

: (η(6)-p-cymene)Ru(C11H14NO2)Cl

: 7681-82-5
sodium iodide

: (η(6)-p-cymene)Ru(C11H14NO2)I

Conditions

Conditions	Yield
In methanol N2 atmosphere, addn. of NaI to soln. of Ru complex, stirring (room temp., 1 h); evapn. of solvent, dissolution (CH2Cl2), evapn. of solvent, filtration, R(Ru),R(C)/S(Ru),R(C) diastereomers in a ratio of 88:12; elem. anal.;	100%

: PdCl2((C4H9)2C3H3N2(CH2C6H5)2)2

: PdClBr((C4H9)2C3H3N2(CH2C6H5)2)2

: 7681-82-5
sodium iodide

: trans-diiodo bis[(4R,5R)-1,3-dibenzyl-4,5-di-tert-butylimidazolin-2-ylidene]palladium(II)

Conditions

Conditions	Yield
In N,N-dimethyl-formamide mixt. of Pd-complexes and NaI in DMF was stirred for 12 h at 120°C, cooled to ambient temp. under Ar; Et2O was added, washed with H2O, dried over MgSO4, filtered, concd., silica gel with cyclohexane/AcOEt, crystd. by slow evapn. in CH2Cl2 and cyclohexane;	100%

...Expand

: (η(6).-p-cymene)Ru(C9H13N2O)Cl

: 7681-82-5
sodium iodide

: (η(6).-p-cymene)Ru(C9H13N2O)I

Conditions

Conditions	Yield
In methanol N2 atmosphere, addn. of NaI to soln. of Ru complex, stirring (room temp., 1 h); evapn. of solvent, dissolution (CH2Cl2), evapn. of solvent, filtration, R(Ru),R(C)/S(Ru),R(C) diastereomers in a ratio of 65:35; elem. anal.;	100%

: 1040922-31-3
Pd(CH3COO)(C5H5N)(C5H4NC6H4NSO2C6H4NO2)

: 7681-82-5
sodium iodide

: 1176325-74-8
C22H17IN4O4PdS

Conditions

Conditions	Yield
In ethanol at 23℃; for 0.5h;	100%

: 1352399-60-0
[RuI2(η6-C6H5(CH2)4SO3(i-Bu))]2

: 7681-82-5
sodium iodide

: [RuI2(η6-C6H5(CH2)4SO3Na)]2

Conditions

Conditions	Yield
In acetone (N2); using Schlenk techniques; suspending of (RuI2(η6-C6H5(CH2)4SO3(i-Bu)))2 in acetone with NaI, stirring at reflux; pptn., filtration, washing with EtOH, drying in vac.;	100%

: (SRu,RC)-chloro(η5-methylcyclopentadienyl)[propane-1,2-diylbis(diphenylphosphane-κP)]ruthenium

: 7681-82-5
sodium iodide

: (RRu,RC)-iodo(η5-methylcyclopentadienyl)[propane-1,2-diylbis(diphenylphosphane-κP)]ruthenium

Conditions

Conditions	Yield
In methanol; chloroform at 20℃; for 24h; Inert atmosphere;	100%

: sodium sulfide

: 15857-57-5
tetraphosphorus decasulfide

: neodymium(III) sulphide

: 7681-82-5
sodium iodide

: rubidium iodide

: Rb2NaNd(PS4)2

Conditions

Conditions	Yield
In melt at 650℃; for 20h; Sealed tube;	100%

...Expand

: [dichlorido(1,3-dimethylbenzimidazol-2-ylidene)(η5-pentamethylcyclopentadienyl)iridium(III)]

: 7681-82-5
sodium iodide

: (N,N′-dimethyl-2-benzimidazolylidene)IrCp*I2

Conditions

Conditions	Yield
In acetone at 20℃; for 22h; Inert atmosphere; Schlenk technique; Glovebox;	100%

: {{P(R,S),3R,4R,P`(R,S)}-1-(t-butoxycarbonyl)-3,4-bis((S)2-hydroxypropylphenylphosphino)pyrrolidine-P,P`}dichloropalladium

: 7681-82-5
sodium iodide

: {{P(R,S),3R,4R,P`(R,S)}-1-(t-butoxycarbonyl)-3,4-bis((S)2-hydroxypropylphenylphosphino)pyrrolidine-P,P`}diiodopalladium

Conditions

Conditions	Yield
In dichloromethane byproducts: NaCl; Ar-atmosphere; stirring for 24 h;; chromd. (silica gel); evapd. dried for 14 h in vacuo; elem. anal.;;	99%

: [(2,6-xylyl isocyanide)(pentamethylcyclopentadienyl)dichlororhodium(III)]

: 7681-82-5
sodium iodide

: (η5-pentamethylcyclopentadienyl)Rh(2,6-xylyl isocyanide)I2

Conditions

Conditions	Yield
In tetrahydrofuran for 3h; Reflux;	99%
In acetone The rhodium dichloride complex and NaI (10-fold excess) are dissolved in acetone and refluxed.;

: 130214-50-5
trans-{PdCl2(1C-diphenylphosphinomethyl-2C-methyl-o-carborane)2

: 7681-82-5
sodium iodide

: 2Pd(2+)*2Cl(1-)*2B10H8C2(CH3)CH2P(C6H5)2(2-)*2H(1+) = {PdCl(B10H9C2(CH3)CH2P(C6H5)2)}2

Conditions

Conditions	Yield
In propan-1-ol refluxing Pd-complex and 10-fold excess of NaJ in propanol until soln. fading, pptn. on cooling; filtration, washing (water, MeOH, hexane), drying; elem. anal.; isomer product mixt. not sepd.;	99%

: {W(CC6H5)(Cl)(CO)2(C5H5N)2}

: 7681-82-5
sodium iodide

: W(CC6H5)I(CO)2(C5H5N)2

Conditions

Conditions	Yield
In tetrahydrofuran under inert atm.; soln. of complex and NaI stirred for 12 h; evapd. (vac.), dissolved in CH2Cl2, filtered, concd., addn. of hexane, crystn.;	99%

: [Cp(2(S),3(S)-bis(diphenylphosphino)butane)Ru(BzS(O)Me)]PF6

: 7681-82-5
sodium iodide

A: [Cp(2(S),3(S)-bis(diphenylphosphino)butane)RuI]

: 824-86-2
R-PhCH2S(O)Me

: 824-86-2
S-PhCH2S(O)Me

Conditions

Conditions	Yield
In acetone inert atmosphere; refluxed; 15 h;; evapd.; dissolved in CH2Cl2; chromd. (SiO2, CH2Cl2, then acetone); HPLC (Chiracel, hexane/i-propanol);;	A n/a B 1% C 99%

...Expand

: (C5H5)Rh(P(CH(CH3)2)3)(OCOCF3)(C6H5CHC(C6H5))

: 7681-82-5
sodium iodide

: 112317-58-5, 85931-02-8
cyclopentadienyl-1,2-diphenylvinyl-iodid-triisopropylphosphine-rhodium(III)

Conditions

Conditions	Yield
In acetone under Ar, NaI mixed in acetone with Rh complex;	99%

: 158414-97-2, 16985-53-8
carbonylchlorodiiodobis(triethylphosphine)rhodium(III)

: 7681-82-5
sodium iodide

: 158367-94-3
carbonyltriiodobis(triethylphosphine)rhodium(III)

Conditions

Conditions	Yield
In acetone inert atmosphere; stirring Rh-complex with 5 equiv. of NaI (room temp., 15 min); concn., addn. of light petroleum, filtration, concn., addn. of Et2O, crystn. (-30°C, 48 h), filtration at -40°C; elem. anal.;	99%

: 23895-60-5
tri-n-butylstannyldibromomethane

: 7681-82-5
sodium iodide

: 213203-63-5
tri-n-butyl(diiodomethyl)stannane

Conditions

Conditions	Yield
In acetone Ar; NaI addn. to stirred Sn-compd. soln. at room temp., mixt. evapn. after 18 h (reduced pressure); residue diln. (hexane), filtration, concn. (reduced pressure), diln. (CH2Cl2), filtration, concn. (reduced pressure);	99%

: 194346-40-2
cis-[bis(1,3,5-triaza-7-phosphaadamantane)dichloroplatinum(II)]

: 7681-82-5
sodium iodide

: 330805-47-5, 852447-80-4
trans-diiodobis(1,3,5-triaza-7-phosphaadamantane)platinum(II)

Conditions

Conditions	Yield
In water addn. of aq. soln. of NaI to aq. soln. of platinum complex; crystn. by slow evapn. of solvent;	99%

: 198629-52-6
[PtClMe(2,9-dimethyl-1,10-phenanthroline)(CH2=CHOH)]

: 7681-82-5
sodium iodide

: 198629-60-6
[PtIMe(2,9-dimethyl-1,10-phenanthroline)(CH2=CHOH)]

Conditions

Conditions	Yield
In chloroform slight excess of NaI, stirring at room temp. for 1 h; sepn. of org. layer, washing (water), filtration over Na2SO4, solvent removal (vac.);	99%

: RuCl2(sIMes)(CHPh)(pyridine)2

: 7681-82-5
sodium iodide

: (1,3-dimesityl-4,5-dihydroimidazol-2-ylidene)I2(pyridine)Ru(benzylidene)

Conditions

Conditions	Yield
In not given byproducts: NaCl, pyridine; under Ar or N2; within 2 h at 25°C;	99%

: (CH3)4N(1+)*((HCON(CH3)2)3VFe3S4Cl3)(1-)*2HCON(CH3)2=(CH3)4N[(HCON(CH3)2)3VFe3S4Cl3]*2HCON(CH3)2

: 7681-82-5
sodium iodide

: (CH3)4N(1+)*((HCON(CH3)2)3VFe3S4I3)(1-)*2HCON(CH3)2=(CH3)4N[(HCON(CH3)2)3VFe3S4I3]*2HCON(CH3)2

Conditions

Conditions	Yield
In N,N-dimethyl-formamide (N2); stirring (1 h), filtration, layering with ether, standing (-20°C, overnight), filtration; extn. (CH3CN), taking to dryness, recrystn. (DMF, diethyl ether); elem. anal.;	99%