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Cas:2171-74-6
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Cas:2171-74-6
Min.Order:1 Gram
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Cas:2171-74-6
Min.Order:1 Gram
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Cas:2171-74-6
Min.Order:1 Kilogram
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Cas:2171-74-6
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
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1,3-BENZODIOXOL-2-ONECASAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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Cas:2171-74-6
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
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Cas:2171-74-6
Min.Order:0
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Type:Trading Company
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1,3-Benzodioxol-2-oneAppearance:Off white to slight yellow solid Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier
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Manufacturer,strong R&D,professional team Storage:Store in a cool, dry place. Store in a tightly closed container. Package:according to your requirement Application:ZhiShang Chemical is owned by ZhiShang Group, is a professional new-type chemicals en
Benzo[1,3]dioxol-2-ylidene-dimethyl-ammonium; chloride
1,3-benzodioxol-2-one
Conditions | Yield |
---|---|
With water for 0.0833333h; | 100% |
Conditions | Yield |
---|---|
With pyridine; oxygen at 20℃; for 2h; Irradiation; | 99% |
Conditions | Yield |
---|---|
With sodium methylate at 90℃; for 24h; Molecular sieve; | 90% |
1,3-benzodioxol-2-one
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 14h; Inert atmosphere; Reflux; | 77% |
Conditions | Yield |
---|---|
With tris(bis(trimethylsilyl)amido)lanthanum(III) In toluene at 80℃; for 24h; Inert atmosphere; Schlenk technique; chemoselective reaction; | 74% |
2,2-dichloro-1,3-benzodioxole
triethyl phosphite
A
1,3-benzodioxol-2-one
B
2,2-bis(diethylphosphono)-1,3-benzodioxole
Conditions | Yield |
---|---|
at 150 - 160℃; for 5h; | A n/a B 65% |
Conditions | Yield |
---|---|
With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine In 2-methyltetrahydrofuran at 30℃; for 3h; | 64% |
at 250℃; |
2-ethoxy-benzo[1,3]dioxole
1,3-benzodioxol-2-one
Conditions | Yield |
---|---|
With di-tert-butyl peroxide In benzene at 140℃; for 5h; | 55% |
1,3-benzodioxol-2-one
Conditions | Yield |
---|---|
With di-tert-butyl peroxide In benzene at 140℃; for 5h; | 54% |
With tert.-butylhydroperoxide In benzene at 140℃; for 5h; Rate constant; | 54% |
A
1,3-benzodioxol-2-one
B
s-butyl chloride
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide In tetrachloromethane at 130℃; for 2h; Rate constant; | A 50% B 38% |
2-butoxy-1,3-benzodioxole
1,3-benzodioxol-2-one
Conditions | Yield |
---|---|
With di-tert-butyl peroxide In benzene at 140℃; for 5h; | 46% |
Conditions | Yield |
---|---|
31% | |
With potassium hydroxide |
Conditions | Yield |
---|---|
With oxygen; palladium diacetate; tetra-(n-butyl)ammonium iodide In acetonitrile at 120℃; under 15001.5 Torr; Flow reactor; | 26% |
With palladium diacetate; triethylamine; triphenylphosphine In tetrahydrofuran at 100 - 110℃; under 20686.5 Torr; for 15h; Autoclave; | 89 %Chromat. |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide at 20℃; under 9000.9 Torr; for 18h; | 10% |
ethyl (2-hydroxyphenyl) carbonate
1,3-benzodioxol-2-one
1,3-benzodioxol-2-one
Conditions | Yield |
---|---|
at 270 - 290℃; |
Conditions | Yield |
---|---|
With sodium hydroxide; toluene | |
With sodium hydroxide; toluene |
Dichloro-acetic acid 2-(2,2-dichloro-acetoxy)-phenyl ester
1,3-benzodioxol-2-one
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran |
2-methoxy-4,5-benz-1,3-dioxolane
di-tert-butyl peroxide
A
1,3-benzodioxol-2-one
B
tert-butyl alcohol
Conditions | Yield |
---|---|
In chlorobenzene at 140℃; for 1h; Product distribution; Rate constant; other reaction time; |
Conditions | Yield |
---|---|
With di-tert-butyl peroxide In chlorobenzene at 140℃; Yield given; |
Conditions | Yield |
---|---|
With hydrogen fluoride In various solvent(s) under 19501.6 Torr; for 6h; Heating; |
Conditions | Yield |
---|---|
at 120℃; |
1,3-benzodioxol-2-one
1,3-benzodioxol-2-one
Conditions | Yield |
---|---|
With water |
ethanedinitrile
water
benzene-1,2-diol
A
1,3-benzodioxol-2-one
benzene-1,2-diol
carbonic acid dimethyl ester
A
1,3-benzodioxol-2-one
B
1,2-dimethoxybenzene
C
2-methoxy-phenol
D
3-methylbenzene-1,2-diol
Conditions | Yield |
---|---|
With potassium; magnesium oxide at 309.85℃; Product distribution; Further Variations:; Temperatures; Reagents; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: benzene; diethyl ether 2: NaH / tetrahydrofuran View Scheme |
dimethyl 2,2’-(carbonylbis(oxy))dibenzoate
benzene-1,2-diol
A
1,3-benzodioxol-2-one
B
methyl salicylate
Conditions | Yield |
---|---|
sodium hydroxide In chloroform at 61℃; for 1.5h; Inert atmosphere; |
1,3-benzodioxol-2-one
isopropyl alcohol
A
bis-2-propyl carbonate
B
benzene-1,2-diol
Conditions | Yield |
---|---|
With sodium methylate In neat (no solvent) at 100℃; under 1500.15 Torr; for 5h; Inert atmosphere; Autoclave; | A 67% B 100% |
With sodium methylate at 100℃; for 5h; Temperature; Autoclave; Inert atmosphere; | A 90 %Chromat. B n/a |
1,3-benzodioxol-2-one
butan-1-ol
A
Dibutyl carbonate
B
benzene-1,2-diol
Conditions | Yield |
---|---|
With sodium methylate In neat (no solvent) at 60℃; for 1h; Catalytic behavior; Temperature; Reagent/catalyst; Inert atmosphere; | A 58% B 90% |
With sodium methylate at 60℃; for 1h; Reagent/catalyst; Temperature; Inert atmosphere; | A 71 %Chromat. B n/a |
Conditions | Yield |
---|---|
With magnesium oxide In tetrahydrofuran at 60℃; under 760.051 Torr; for 1h; Catalytic behavior; Time; Temperature; Reagent/catalyst; Solvent; Inert atmosphere; | 77% |
With sodium methylate at 60℃; for 1h; Reagent/catalyst; Temperature; Time; Inert atmosphere; | 95.5 %Chromat. |
1,3-benzodioxol-2-one
2,6-di-tert-butyl-4-methyl-phenol
A
4-(1,3-benzodioxol-5-yl)-2,6-di-tert-butyl-4-methylcyclohexa-2,5-dien-1-one
B
4-(1,3-benzodioxol-5-ylmethyl)-2,6-di-tert-butylphenol
Conditions | Yield |
---|---|
With bis-[(trifluoroacetoxy)iodo]benzene In 1,1,1,3',3',3'-hexafluoro-propanol at 0℃; for 0.0388889h; oxidative Friedel Crafts reaction; | A 64% B n/a |
Conditions | Yield |
---|---|
With diisobutylaluminium hydride In toluene Heating; | 49% |
With water; sodium methylate In toluene at 100℃; for 6h; Temperature; Solvent; | 99 %Chromat. |
1,3-benzodioxol-2-one
D-glucosamine hydrochloride
acetic anhydride
A
1,3,4,6-tetra-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranose
B
1,3,4,6-tetra-O-acetyl-2-phthalimido-2-deoxy-α-D-glucopyranose
Conditions | Yield |
---|---|
Stage #1: D-glucosamine hydrochloride With sodium methylate In methanol at 0 - 20℃; Stage #2: 1,3-benzodioxol-2-one With triethylamine In methanol at 20℃; for 24h; Stage #3: acetic anhydride With pyridine at 20℃; for 48h; optical yield given as %de; | A n/a B 44% |
1,3-benzodioxol-2-one
8-Methyl-decahydro-naphthalen-1-ol
8β-methyl-trans-1α-decalyl hydrogenphthalate
8α-methyl-cis-1β-decalyl hydrogenphthalate
Conditions | Yield |
---|---|
With pyridine for 4h; Heating; | A 40.9% B 6.9% |
With pyridine | A 40.9% B 6.9% |
Conditions | Yield |
---|---|
at 840℃; | 34% |
1,3-benzodioxol-2-one
Eudesmic acid
5-(3,4,5-trimethoxybenzoyl)-1,3-benzodioxol-2-one
Conditions | Yield |
---|---|
With methanesulfonic acid; phosphorus pentoxide at 50℃; for 26h; Friedel Crafts acylation; Inert atmosphere; | 3% |
Conditions | Yield |
---|---|
With ethanol at 0℃; |
1,3-benzodioxol-2-one
ethylamine
ethyl-carbamic acid-(2-hydroxy-phenyl ester)
Conditions | Yield |
---|---|
With ethanol |
Conditions | Yield |
---|---|
With acetone |
1,3-benzodioxol-2-one
1-amino-2-propene
allyl-carbamic acid-(2-hydroxy-phenyl ester)
Conditions | Yield |
---|---|
With benzene at 70℃; |
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