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inquiry1-Chloroheptane
sodium heptanesulfonate
Conditions | Yield |
---|---|
With water; sodium sulfite at 200℃; |
1-Bromoheptane
sodium heptanesulfonate
Conditions | Yield |
---|---|
With sodium sulfite In water for 24h; Heating; |
n-heptane
sodium heptanesulfonate
Conditions | Yield |
---|---|
Stage #1: n-heptane With P25; sulfur dioxide; oxygen for 5h; Irradiation; Stage #2: With sodium hydroxide In methanol Mechanism; Reagent/catalyst; Solvent; chemoselective reaction; | 600 mg |
Conditions | Yield |
---|---|
In chloroform at 20℃; for 5h; | 95% |
sodium heptanesulfonate
heptanesulfonyl chloride
Conditions | Yield |
---|---|
With thionyl chloride In benzene for 4h; Heating; | |
With phosphorus pentachloride at 140℃; for 0.75h; Neat (no solvent); | |
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 1h; | |
With thionyl chloride Reflux; Inert atmosphere; | |
With thionyl chloride for 6h; Reflux; Inert atmosphere; |
sodium heptanesulfonate
heptane-1-sulfonic acid (2-oxo-tetrahydro-furan-3-yl)-amide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: thionyl chloride / benzene / 4 h / Heating 2: 1,8-diazabicyclo[5.4.0]-undec-7-ene; 4-dimethylaminopyridine / CH2Cl2 / 24 h / 20 °C View Scheme |
bromine
sodium heptanesulfonate
Conditions | Yield |
---|---|
In water Br2 gas diffused to aq. soln. contg. C7H15SO3Na and Pd complex; |
sodium heptanesulfonate
N-(3-(5-(3'-O-Acetyl-2'-deoxyuridine))prop-2-ynyl)heptane-1-sulfonamide
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: thionyl chloride / Reflux; Inert atmosphere 2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere 3: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere View Scheme |
sodium heptanesulfonate
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: thionyl chloride / Reflux; Inert atmosphere 2.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere 3.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere 4.1: pyridine; pyridinium β-cyanoethyl phosphate; dicyclohexyl-carbodiimide / 48 h / 20 °C / Inert atmosphere 5.1: water; sodium hydroxide / 0.08 h / 100 °C 5.2: Dowex 50-WX8 (Na+ form) View Scheme |
sodium heptanesulfonate
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: thionyl chloride / Reflux; Inert atmosphere 2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere 3: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere 4: pyridine; pyridinium β-cyanoethyl phosphate; dicyclohexyl-carbodiimide / 48 h / 20 °C / Inert atmosphere View Scheme |
sodium heptanesulfonate
benzoyl isocyanate
Conditions | Yield |
---|---|
In toluene Schlenk technique; Inert atmosphere; Reflux; | 293 mg |
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