Hangzhou Yunuo Chemical Co., Ltd is located in Hangzhou city China. As a global supplier in the chemical industry, Yunuochem is to create added value for customers around the world. Sticking to such business idea of "Good faith wins the busin
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inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryLIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.
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inquiryHigh quality alpha-(2,4-Dichlorophenyl)-1H-imidazole-1-ethanol Cas 24155-42-8 with steady supply Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & i
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inquiry1-(2,4-Dichlorophenyl)-2-(1-imidazolyl)ethanol CAS No.:24155-42-8 Name: alpha-(2,4-Dichlorophenyl)-1H-imidazole-1-ethanol Synonyms: 1-(2,4-Dichlorophenyl)-2-(1-imidazolyl)ethanol Molecular Structure Mol
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualified
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct Name: alpha-(2,4-Dichlorophenyl)-1H-imidazole-1-ethanol Synonyms: 1-(2,4-DICHLOROPHENYL)-2-(1H-IMIDAZOL-1-YL)ETHANOL;1-(2,4-dichlorophenyl)-2-(1-imidazolyl)ethanol;1-(2,4-DICHLOROPHENYL)-2-IMIDAZOL-1-YL ETHANOL;1H-IMIDAZOLE-1-ETHANOL, ALPHA-
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inquiryAdvantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best service is
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryAbout Product Details Items Specifications Test Results Appearance White to white crystalline powde
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inquiryAbout us Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad.
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inquiryalpha-(2,4-Dichlorophenyl)-1H-imidazole-1-ethanol CAS: 24155-42-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializin
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiryAppearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryalpha-(2,4-Dichlorophenyl)-1H-imidazole-1-ethanol CAS 24155-42-8 Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and esta
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiry1-(2,4-dichlorophenyl)-2-(imidazol-1-yl)ethanone
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol at 20℃; for 12h; | 98% |
With potassium borohydride In methanol for 1h; Reflux; | 90.5% |
With sodium tetrahydroborate In methanol for 2h; Reflux; | 88% |
1H-imidazole
α-(chloromethyl)-2,4-dichlorobenzyl alcohol
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
With 1,1,1,3',3',3'-hexafluoro-propanol; alumina-supported potassium hydroxide at 45℃; for 3.5h; | 90% |
With potassium carbonate; sodium iodide In water; butanone | 78.7% |
With sodium In N-methyl-acetamide; methanol; water |
1H-imidazole
2-(2,4-dichlorophenyl)oxirane
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
With pyridine In ethanol for 12h; Ring cleavage; Heating; | 63% |
Stage #1: 1H-imidazole With sodium hydride In N,N-dimethyl-formamide at 20℃; Inert atmosphere; Stage #2: 2-(2,4-dichlorophenyl)oxirane In N,N-dimethyl-formamide at 60℃; Inert atmosphere; | 57% |
Stage #1: 1H-imidazole With sodium hydride In N,N-dimethyl-formamide Inert atmosphere; Stage #2: 2-(2,4-dichlorophenyl)oxirane In N,N-dimethyl-formamide at 20℃; Inert atmosphere; |
tetra-n-butylammonium imidazolate
α-(chloromethyl)-2,4-dichlorobenzyl alcohol
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
In acetonitrile Reflux; | 68% |
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In methanol for 2h; | 95% |
tetra-n-butylammonium imidazolate
2-bromo-1-(2,4-dichlorophenyl)ethanol
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
In acetonitrile Reflux; | 40% |
2,2',4'-trichloroacetophenone
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 28 percent / CH2Cl2 / 2 h / 40 °C 2: sodium borohydride View Scheme | |
Multi-step reaction with 2 steps 1: sodium tetrahydroborate / isopropyl alcohol / 2 h / 3 - 20 °C 2: acetonitrile / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: dichloromethane 2: potassium borohydride / methanol / 1 h / Reflux View Scheme |
2,4-dichlorophenacyl bromide
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium tetrahydroborate / isopropyl alcohol / 2 h / 3 - 20 °C 2: acetonitrile / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / N,N-dimethyl-formamide; water / 20 °C 2: sodium tetrahydroborate / methanol / 2 h / 5 - 50 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / 20 °C 2: sodium tetrahydroborate / methanol / 2 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / tetrahydrofuran / 3 h / 20 °C 2: sodium tetrahydroborate / methanol / 3 h / 0 °C / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / N,N-dimethyl-formamide / 20 °C 2: sodium tetrahydroborate; methanol / 2 h / 0 °C / Reflux View Scheme |
1,3-Dichlorobenzene
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: aluminum (III) chloride / 3 h / 30 °C 2.1: triethylamine / methanol / 20 °C 2.2: 4 h / 65 °C 3.1: sodium tetrahydroborate / ethanol / 12 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: aluminum (III) chloride 2: triethylamine / methanol / 65 °C 3: sodium tetrahydroborate / ethanol / 20 °C View Scheme |
1-(2,4-dichlorophenyl)ethan-1-one
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: bromine / chloroform / 1.5 h / 0 - 20 °C 2: potassium carbonate / 20 °C 3: sodium tetrahydroborate / methanol / 2 h / Reflux View Scheme | |
Multi-step reaction with 3 steps 1: bromine / chloroform / 1 h / 0 - 20 °C 2: potassium carbonate / tetrahydrofuran / 3 h / 20 °C 3: sodium tetrahydroborate / methanol / 3 h / 0 °C / Reflux View Scheme | |
Multi-step reaction with 3 steps 1: bromine / chloroform / 1 h / 0 - 20 °C 2: potassium carbonate / N,N-dimethyl-formamide / 20 °C 3: sodium tetrahydroborate; methanol / 2 h / 0 °C / Reflux View Scheme |
2,2',4'-trichloroacetophenone
A
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: acetonitrile 2: NaBH4 / ethanol View Scheme |
2,4-dichlorobenzaldeyhde
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: potassium hydroxide / acetonitrile; water / 3 h / 60 °C / Inert atmosphere 2.1: sodium hydride / N,N-dimethyl-formamide / 20 °C / Inert atmosphere 2.2: 60 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1.1: potassium hydroxide / acetonitrile / 60 - 65 °C / Inert atmosphere 2.1: sodium hydride / N,N-dimethyl-formamide / Inert atmosphere 2.2: 20 °C / Inert atmosphere View Scheme |
2,4-dichlorophenacyl bromide
A
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: CHCl3 / 0 °C 2: sodium borohydride / ethanol / 4 h / Heating View Scheme |
2,4-dichlorobenzaldeyhde
A
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 82 percent / aq. KOH / acetonitrile / 3 h / 60 °C 2: 63 percent / pyridine / ethanol / 12 h / Heating View Scheme |
Hexanoyl chloride
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 4h; Ambient temperature; | 97% |
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
2-bromoethyl-2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside
Conditions | Yield |
---|---|
In acetonitrile at 110℃; | 96% |
In acetonitrile at 110℃; for 24h; | 90% |
3-Bromomethyl-7-chlorobenzothiophene
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
sertaconazole nitrate
Conditions | Yield |
---|---|
Stage #1: 3-Bromomethyl-7-chlorobenzothiophene; 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With tetrabutyl-ammonium chloride; sodium hydroxide In water; toluene at 80℃; for 4h; Stage #2: With nitric acid | 95.7% |
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
3-chloroprop-1-ene
1-[2-(2,4-dichlorophenyl)-2-(2-propenyloxy)ethyl]-1H-imidazole
Conditions | Yield |
---|---|
Stage #1: 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With potassium hydroxide In water; dimethyl sulfoxide at 20℃; for 1h; Stage #2: 3-chloroprop-1-ene In water; dimethyl sulfoxide at 30℃; for 3h; Solvent; Temperature; | 95.6% |
Stage #1: 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With potassium hydroxide In water; dimethyl sulfoxide at 20 - 35℃; for 1h; Stage #2: 3-chloroprop-1-ene In water; dimethyl sulfoxide at 35 - 40℃; Reagent/catalyst; | 68% |
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
n-octanoic acid chloride
1-(2,4-dichloro-phenyl)-2-imidazol-1-yl-1-octanoyloxy-ethane
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 4h; Ambient temperature; | 95% |
n-decanoyl chloride
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 4h; Ambient temperature; | 91% |
acetic anhydride
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethyl acetate
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 20℃; for 1.5h; Inert atmosphere; | 91% |
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
(±)-1-(2-azido-2-(2, 4-dichlorophenyl)ethyl)-1H-imidazole
Conditions | Yield |
---|---|
With diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at 0 - 20℃; for 3.25h; Inert atmosphere; | 87% |
With diazabicycloundecane; diphenyl phosphoryl azide In tetrahydrofuran | |
With diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide |
3-(bromomethyl)benzothiophene
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
1-(2-(benzo[b]thiophen-3-ylmethoxy)-2-(2,4-dichlorophenyl)ethyl)-1H-imidazole
Conditions | Yield |
---|---|
Stage #1: 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With tetrabutylammomium bromide; sodium hydroxide In toluene at 85℃; for 0.5h; Stage #2: 3-(bromomethyl)benzothiophene In toluene for 3h; Heating; | 86% |
Stage #1: 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With tetrabutylammomium bromide; sodium hydroxide In toluene at 85℃; for 0.5h; Stage #2: 3-(bromomethyl)benzothiophene In toluene for 3h; Heating; | 86% |
With sodium hydride 1.) HMPT, RT; 2.) HMPT, 50 deg C, 1 h, 3.) HMPT, 0 deg C, 5 h;; Multistep reaction; |
1-phenylthio-4-chloromethyl-benzene
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
Stage #1: 1-phenylthio-4-chloromethyl-benzene; 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With tetrabutylammomium bromide; sodium hydroxide In water; toluene at 58 - 60℃; for 13.5h; Stage #2: With nitric acid In ethyl acetate; toluene at 25℃; for 3h; | 85.1% |
Stage #1: 1-phenylthio-4-chloromethyl-benzene; 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With sodium hydroxide In tetrahydrofuran; water for 4.5h; Stage #2: With nitric acid In water | 82.1% |
Stage #1: 1-phenylthio-4-chloromethyl-benzene; 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With tetrabutylammomium bromide; sodium hydroxide In water; toluene at 58℃; for 13.5h; Stage #2: With nitric acid In ethyl acetate; toluene at 25℃; for 3h; | 74.7% |
Stage #1: 1-phenylthio-4-chloromethyl-benzene; 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With tetrabutylammomium bromide; sodium hydroxide In water; toluene at 58 - 60℃; for 13.5h; Stage #2: With nitric acid In ethyl acetate at 25℃; for 3h; | 71.4% |
Nonanoyl chloride
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 4h; Ambient temperature; | 84% |
propionyl chloride
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 4h; Ambient temperature; | 83% |
n-dodecanoyl chloride
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
1-(2,4-dichloro-phenyl)-1-dodecanoyloxy-2-imidazol-1-yl-ethane
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 4h; Ambient temperature; | 82% |
undecanoyl chloride
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 4h; Ambient temperature; | 82% |
trans-geranyl bromide
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
Stage #1: 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With sodium hydride In N,N-dimethyl-formamide at 40℃; for 0.5h; deprotonation; Stage #2: trans-geranyl bromide In N,N-dimethyl-formamide at 20℃; for 0.5h; Etherification; | 82% |
In N-methyl-acetamide |
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
sertaconazole
Conditions | Yield |
---|---|
Stage #1: 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With tetra-(n-butyl)ammonium iodide; sodium hydroxide In water; toluene at 50℃; for 0.25h; Inert atmosphere; Stage #2: 7-chloro-3-(chloromethyl)benzo[b]thiophene In water; toluene at 50℃; for 4h; Inert atmosphere; | 82% |
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
2-(bromomethyl)naphthalene
Conditions | Yield |
---|---|
With N,N,N,N,N,N-hexamethylphosphoric triamide; tetra-(n-butyl)ammonium iodide; sodium hydride at 0℃; | 80% |
Stage #1: 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With tetrabutylammomium bromide; sodium hydroxide In toluene at 85℃; for 0.5h; Stage #2: 2-(bromomethyl)naphthalene In toluene for 3h; Heating; | 72% |
Stage #1: 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With tetrabutylammomium bromide; sodium hydroxide In toluene at 85℃; for 0.5h; Stage #2: 2-(bromomethyl)naphthalene In toluene for 3h; Heating; | 72% |
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
2-bromomethylnaphthyl bromide
Conditions | Yield |
---|---|
Stage #1: 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With tetrabutylammomium bromide; sodium hydroxide In toluene at 85℃; for 0.5h; Stage #2: 2-bromomethylnaphthyl bromide In toluene for 3h; Heating; | 76% |
Stage #1: 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With tetrabutylammomium bromide; sodium hydroxide In toluene at 85℃; for 0.5h; Stage #2: 2-bromomethylnaphthyl bromide In toluene for 3h; Heating; | 76% |
With sodium hydride 1.) HMPA, 20 degC - 25 degC, 1 h; 50 degC - 60 degC, 2 h; 2.) 50 degC, 20 h; Yield given. Multistep reaction; |
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
1-chloro-1-(2,4-dichlorophenyl)-2-(1H-imidazole-1-yl)ethane
Conditions | Yield |
---|---|
With thionyl chloride at 20℃; for 12h; | 74.3% |
With thionyl chloride In dichloromethane | |
With thionyl chloride at 20℃; |
butyryl chloride
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 4h; Ambient temperature; | 74% |
2,4-Dichlorobenzyl chloride
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
miconazole
Conditions | Yield |
---|---|
Stage #1: 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride In tetrahydrofuran at 20℃; for 0.5h; Substitution; Stage #2: 2,4-Dichlorobenzyl chloride In tetrahydrofuran at 45℃; for 16h; Substitution; | 73% |
Stage #1: 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With sodium hydride In N,N-dimethyl-formamide Inert atmosphere; Stage #2: 2,4-Dichlorobenzyl chloride In N,N-dimethyl-formamide at 20℃; |
p-phenylbenzyl bromide
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
1-[2-biphenyl-4-ylmethoxy-2-(2,4-dichloro-phenyl)-ethyl]-1H-imidazole
Conditions | Yield |
---|---|
With N,N,N,N,N,N-hexamethylphosphoric triamide; tetra-(n-butyl)ammonium iodide; sodium hydride at 0℃; | 73% |
n-valeryl chloride
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 4h; Ambient temperature; | 71% |
3-Bromomethylthiophene
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
1-(2-(2,4-dichlorophenyl)-2-(thiophen-3-ylmethoxy)ethyl)-1H-imidazole
Conditions | Yield |
---|---|
Stage #1: 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With tetrabutylammomium bromide; sodium hydroxide In toluene at 85℃; for 0.5h; Stage #2: 3-Bromomethylthiophene In toluene for 3h; Heating; | 71% |
Stage #1: 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With tetrabutylammomium bromide; sodium hydroxide In toluene at 85℃; for 0.5h; Stage #2: 3-Bromomethylthiophene In toluene for 3h; Heating; | 71% |
1,3-Dichloro-2-chloromethyl-benzene
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
Stage #1: 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With sodium hydride In 1,4-dioxane; mineral oil at 20℃; for 1h; Inert atmosphere; Reflux; Stage #2: 1,3-Dichloro-2-chloromethyl-benzene In 1,4-dioxane; mineral oil Inert atmosphere; Reflux; | 70% |
1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol
Conditions | Yield |
---|---|
Stage #1: 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethan-1-ol With sodium hydride In N,N-dimethyl-formamide at -5 - 20℃; for 1.5h; Inert atmosphere; Stage #2: 4-bromobenzyl halide In N,N-dimethyl-formamide at 0 - 20℃; for 1h; Inert atmosphere; | 68.4% |
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