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Cas:2444-49-7
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Min.Order:1 Kilogram
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Type:Trading Company
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Conditions | Yield |
---|---|
With sulfur; potassium hydroxide; water In tetrahydrofuran for 2h; Ambient temperature; | A 30% B 10% |
Conditions | Yield |
---|---|
With diethyl ether; sodium ethanolate beim Behandeln anschliessend mit Dischwefeldichlorid in Petrolaether; |
diallyl disulphide
A
3-vinyl-4H-<1,2>-dithiin
B
diallyl sulphide
C
diallyl trisulfide
D
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 50℃; for 168h; Further byproducts given; | A 0.7 % Chromat. B 3 % Chromat. C 9.7 % Chromat. D 0.47 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
D
5-methyl-4,7-dithiadeca-1,9-diene
Conditions | Yield |
---|---|
at 80℃; for 240h; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D 0.45 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
D
2‐ethenyl‐4H‐1,3‐dithiine
Conditions | Yield |
---|---|
at 50℃; for 168h; Further byproducts given; | A 3 % Chromat. B 9.7 % Chromat. C 0.47 % Chromat. D 0.3 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D 0.68 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D 0.42 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D 0.86 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Yield given. Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D n/a |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Yield given. Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D n/a |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D 2.3 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D 0.2 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D 0.7 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D 0.25 % Chromat. |
allyl bromide
A
diallyl disulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
With polysulfide; tetraethylammonium perchlorate In N,N-dimethyl-formamide in situ electrochemical generation of polysulfide from carbon-sulfur cathode; Title compound not separated from byproducts; |
3-chloroprop-1-ene
A
diallyl disulphide
B
diallyl sulphide
C
diallyl trisulfide
D
diallyl tetrasulfide
Conditions | Yield |
---|---|
Stage #1: With sodium sulfide; sodium hydroxide; sulfur; polyethylene glycol In water at 45 - 60℃; under 1173.78 Torr; Stage #2: 3-chloroprop-1-ene In water at 45 - 50℃; under 915.2 - 4897.34 Torr; Product distribution / selectivity; continuous process; | |
Stage #1: With sodium sulfide; sodium hydroxide; sulfur In water at 45 - 60℃; under 1173.78 Torr; Stage #2: 3-chloroprop-1-ene In water at 45 - 50℃; under 915.2 - 4897.34 Torr; Product distribution / selectivity; continuous process; |
allicin
A
diallyl disulphide
B
diallyl sulphide
C
diallyl trisulfide
D
diallyl tetrasulfide
E
bis-2-propenyl pentasulfide
Conditions | Yield |
---|---|
With sulfur; dibutylamine at 60 - 70℃; for 1h; Product distribution / selectivity; |
allicin
A
diallyl disulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 60 - 70℃; for 1h; Product distribution / selectivity; |
allicin
A
diallyl disulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
D
bis-2-propenyl pentasulfide
Conditions | Yield |
---|---|
at 70℃; for 1h; Product distribution / selectivity; | |
With sulfur at 60 - 70℃; for 1h; Product distribution / selectivity; |
allicin
A
diallyl disulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
D
bis-2-propenyl pentasulfide
E
diallyl hexasulfide
Conditions | Yield |
---|---|
With sulfur at 60 - 70℃; for 1h; Product distribution / selectivity; |
allicin
A
diallyl disulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
D
bis-2-propenyl pentasulfide
E
diallyl hexasulfide
F
diallyl heptasulfide
Conditions | Yield |
---|---|
With sulfur at 70℃; for 1h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
at 70℃; for 1h; Product distribution / selectivity; |
allicin
A
diallyl trisulfide
B
diallyl tetrasulfide
C
bis-2-propenyl pentasulfide
D
diallyl hexasulfide
E
diallyl heptasulfide
Conditions | Yield |
---|---|
With sulfur at 70℃; for 1h; Product distribution / selectivity; |
allicin
A
diallyl trisulfide
B
diallyl tetrasulfide
C
bis-2-propenyl pentasulfide
D
diallyl heptasulfide
Conditions | Yield |
---|---|
With sulfur at 70℃; for 1h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
In ethanol Electrochem. Process; diallyltetrasulfide added to a soln. of CuBr2*2H2O in EtOH, placed into glass reservoir, copper electrodes mounted via air tight seal, system maintained for 20 h under an applied tension of alternating current (50 Hz, 0.2 V, 0.1 mA); crystn. on electrodes; |
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