Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryOur advantage: 1: High quality and Competitive price 2: Quality control, GC&HPLC&NMR or as your requested 3: Packing as your requested, and double check before shipment 4: Prompt shipment with professional documents 5: Excellent after-
Cas:592-88-1
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
We are leading fine chemicals supplier in China and Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediat
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inquiryAppearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:As customer request Port:Qingda
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Donglian as a factory and supplier of aroma chemicals in China, We can provide different quantities of custom synthesis chemicals in food flavor scale more than fourteen years.in addition, our company has researched and developed four series
Diallyl sulfide Melting point -83 °C Boiling point 138 °C (lit.) Density 0.887 g/mL at 25 °C (lit.) Vapor density 3.9 (vs air) Vapor pressure 7 mm Hg ( 20 °C) Refractive in
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inquiryLonwin Industry group limited as a professional manufactor & exporter of chemical materials ,we totally haver more than 270 stuffs, we have been on this line for more than 9 years. Our chemical materials are exported to lot of countries and regio
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inquiryJinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
Superior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Sealed in a cool ,dry and microtherm place , avoid light . Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:synthetic perfume Tra
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:592-88-1
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
Supply top quality products with a reasonable price Application:api
FEMA 2042, Allyl sulfide Package:as requirements Application:FEMA 2042, Allyl sulfide Port:Shanghai, China
1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highl
Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an
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inquiryAllyl sulfideAppearance:Colorless liquid Storage:200MT Package:as your requirement Application:Pharmaceutical Intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by sea LCL/F
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
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inquiryDiallyl sulfide Basic information Product Name: Diallyl sulfide Synonyms: (CH2=CHCH2)2S;1-propene,3,3’-thiobis-;3-(Allylsulfanyl)-1-propene;3,3’-thiobis
Cas:592-88-1
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inquiryZhejiang Newfine Industry Co.,Ltd. is a professional supplier of Aromatic Chemicals,Fragrance & Flavor use Chemicals,Pine Chemicals,Fine Chemicals,Food Additives and some Essential Oils. We have 12 years experi
Strong R&D strength and team We have a R&D team with around 30 R&D personnel.All of our employees have chemical backgrounds and have worked in the chemical industry for many years.Our laboratory can synthesize target products with wei
Cas:592-88-1
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inquiryZhengzhou Kingorgchem Chemical Technology Co., Ltd. was founded on the basis of Organophosphorus Chemistry Lab of Institute of Chemistry Henan Academy of Sciences in 2015. The laboratory covers 600 m2 and the pilot plant covers 2000 m2. Kingorgchem i
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inquirydiallyl sulfoxide
diallyl sulphide
Conditions | Yield |
---|---|
With trifluoromethylsulfonic anhydride; potassium iodide In acetonitrile at 20℃; for 0.0833333h; | 95% |
With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; potassium iodide for 0.0333333h; Neat (no solvent); chemoselective reaction; | 93% |
With iodine; sodium hydrogensulfite In chloroform at 50℃; for 3h; Temperature; | 90% |
With Silphos; iodine In acetonitrile for 0.25h; Heating; | 89% |
With sodium iodide at 20℃; for 1h; Green chemistry; | 87% |
Conditions | Yield |
---|---|
With hexamethyldisilathiane at 150 - 160℃; for 7h; | 84% |
With potassium sulfide |
2-methylpropan-2-thiol
allyl bromide
A
allyl tert-butyl sulfide
B
diallyl sulphide
Conditions | Yield |
---|---|
With sodium methylate In methanol 0 deg C, 1 h; 25 deg C, overnight; Yields of byproduct given. Title compound not separated from byproducts; | A 66% B n/a |
Conditions | Yield |
---|---|
With hydrogen sulfide In dimethyl sulfoxide at 40℃; for 3h; | A 11% B 50.8% |
bis[2-chloro-3-(trimethylsilyl)-propyl]sulfide
diallyl sulphide
Conditions | Yield |
---|---|
With potassium tert-butylate In methanol at 20℃; for 7h; | 47% |
Dithiocarbonic acid S-allyl ester O-benzyl ester
A
diallyl sulphide
B
dibenzyl sulfide
C
allyl(benzyl)sulfide
Conditions | Yield |
---|---|
With 1,2-bis-(diphenylphosphino)ethane; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 65℃; for 7h; | A n/a B n/a C 32% |
2-allylmercapto-1,3-benzothiazole
chloroform
A
1,3-Benzothiazole
B
diallyl disulphide
C
diallyl sulphide
Conditions | Yield |
---|---|
With sodium hydroxide; tetrabutylammomium bromide at 45 - 55℃; for 25h; Rearrangement; disproportionation; Further byproducts given; | A 24% B 24% C 15% D n/a |
2-allylmercapto-1,3-benzothiazole
chloroform
A
1,3-Benzothiazole
B
diallyl disulphide
C
diallyl sulphide
D
2,2'-benzothiazolyl
Conditions | Yield |
---|---|
With sodium hydroxide; tetrabutylammomium bromide at 45 - 55℃; for 25h; Rearrangement; disproportionation; Further byproducts given; | A 24% B 24% C 15% D 2% |
diallyl disulphide
acetylene
A
diallyl sulphide
B
Vinyl propen-1-yl sulfide
C
(E)-allyl(prop-1-en-1-yl)sulfane
D
1-vinylthio-3-(1-propenylthio)-1-propene
Conditions | Yield |
---|---|
With potassium hydroxide; hydroquinone In water; dimethyl sulfoxide at 40 - 45℃; under 9880 - 15200 Torr; for 4h; Further byproducts given; | A 0.7% B 17.8% C 1.4% D 19.6% |
Conditions | Yield |
---|---|
With potassium hydroxide at 200℃; |
Conditions | Yield |
---|---|
at 117℃; Disproportionierung im geschlossenen Gefaess; |
3,3'-thiodipropanol
diallyl sulphide
Conditions | Yield |
---|---|
With potassium hydroxide at 200℃; |
Conditions | Yield |
---|---|
With sodium sulfide; ethanol | |
With potassium hydrosulfide | |
With polyglycol; sodium sulfide In water at 70 - 80℃; for 2h; | 99 % Chromat. |
With bis(tributyltin)sulfide In chloroform at 110℃; for 12h; | 98 % Chromat. |
Conditions | Yield |
---|---|
With potassium hydrosulfide | |
With potassium sulphide; ethanol; water at 50℃; zuletzt bei Siedetemperatur; | |
With sodium sulfide; tetrabutylammomium bromide In water at 70 - 80℃; for 2h; | 89 % Chromat. |
Conditions | Yield |
---|---|
With potassium sulfide at 120℃; |
diallyl disulphide
A
3-vinyl-4H-<1,2>-dithiin
B
diallyl sulphide
C
diallyl trisulfide
D
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 50℃; for 168h; Further byproducts given; | A 0.7 % Chromat. B 3 % Chromat. C 9.7 % Chromat. D 0.47 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
D
5-methyl-4,7-dithiadeca-1,9-diene
Conditions | Yield |
---|---|
at 80℃; for 240h; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D 0.45 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
D
2‐ethenyl‐4H‐1,3‐dithiine
Conditions | Yield |
---|---|
at 50℃; for 168h; Further byproducts given; | A 3 % Chromat. B 9.7 % Chromat. C 0.47 % Chromat. D 0.3 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D 0.68 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D 0.42 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D 0.86 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Yield given. Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D n/a |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Yield given. Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D n/a |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D 2.3 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D 0.2 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D 0.7 % Chromat. |
diallyl disulphide
A
diallyl sulphide
B
diallyl trisulfide
C
diallyl tetrasulfide
Conditions | Yield |
---|---|
at 80℃; for 240h; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 5.5 % Chromat. D 0.25 % Chromat. |
Conditions | Yield |
---|---|
With 1,1,3,3-tetramethyl-2-thiourea; sodium hydride 1) DMF, room temp., 1 h; 2) DMF, hexane, room temp., 10 min.; Yield given. Multistep reaction; |
diallyl disulphide
acetylene
A
(E,E)-bis-(1-propenyl) sulfide
B
diallyl sulphide
C
Vinyl propen-1-yl sulfide
D
1,2-bis(1-propylenylthio)ethene
E
1-vinylthio-3-allylthio-1-propene
F
1-vinylthio-3-(1-propenylthio)-1-propene
Conditions | Yield |
---|---|
With potassium hydroxide; hydroquinone In dimethyl sulfoxide at 40℃; under 6840 - 13680 Torr; for 4h; Product distribution; other temperatures, times, amount of potassium hydroxide, inhibitors and the conc. of water in DMSO; |
diallyl sulphide
diallyl sulfoxide
Conditions | Yield |
---|---|
With Mn(III) Schiff-base; dihydrogen peroxide In water; acetic acid at 20℃; for 0.0666667h; | 100% |
With 2-hydroperoxyhexafluoro-2-propanol In dichloromethane at -78℃; for 2h; | 98% |
With dihydrogen peroxide; Amberlyst 15 In methanol at 20℃; for 0.5h; | 98% |
diallyl sulphide
diallyl sulfone
Conditions | Yield |
---|---|
With sodium tungstate (VI) dihydrate; dihydrogen peroxide In methanol; water at 40℃; | 100% |
With 1H-imidazole; tetra-n-butylammonium hydrogen monopersulfate In dichloromethane at 25℃; for 0.0333333h; chemoselective reaction; | 100% |
With tert.-butylhydroperoxide; [Mo2(O)4{[2,2'-(1,3-phenylene)bis(4,5-dihydrooxazole-4,2-diyl)]dimethanol}(acac)2] In 1,2-dichloro-ethane for 0.416667h; Reflux; | 100% |
N-chloro-succinimide
diallyl sulphide
2-propenyl 3-chloro-1-propenyl sulfide
Conditions | Yield |
---|---|
In tetrachloromethane at 4℃; for 10h; | 100% |
Conditions | Yield |
---|---|
With tungsten In octane; chlorobenzene at 80℃; for 1h; | A 100% B n/a |
With chloroaryloxide neopentylidene complex of tungsten (1) | A 90% B n/a |
(2,6-Ph2C6H3O)2W(Cl)=CHC(CH3)3*OEt2 In chlorobenzene at 80℃; for 3h; | A 88% B n/a |
diallyl sulphide
2-propenyl 3-chloro-1-propenyl sulfide
Conditions | Yield |
---|---|
With N-chloro-succinimide In tetrachloromethane at 0℃; | 100% |
diallyl sulphide
2,2-difluoroethyl triflate
Conditions | Yield |
---|---|
In neat (no solvent) at 60℃; for 24h; Inert atmosphere; Sealed tube; | 99% |
diallyl sulphide
trifluoromethanesulfonic acid 2-fluoroethyl ester
Conditions | Yield |
---|---|
In neat (no solvent) at 20℃; for 15h; Inert atmosphere; Sealed tube; | 99% |
Conditions | Yield |
---|---|
at 60℃; for 15h; Inert atmosphere; | 99% |
diallyl sulphide
pyridazine-4,5-dicarbonitrile
Conditions | Yield |
---|---|
In chloroform at 110℃; Diels-Alder reaction; | 97% |
diallyl sulphide
Conditions | Yield |
---|---|
In methanol N2-atmosphere; evapn., extg. (CH2Cl2), filtering, pptn. on ether addn. (0°C), filtering, washing (ether), drying (vac.); | 97% |
Conditions | Yield |
---|---|
at 60℃; for 15h; Inert atmosphere; | 96% |
diallyl sulphide
Conditions | Yield |
---|---|
In methanol N2-atmosphere; refluxing (18 h); evapn., extg. (CH2Cl2), filtering, pptn. on ether addn. (0°C), filtering, washing (ether), drying (vac.); elem. anal.; | 94% |
tetrafluoroboric acid diethyl ether
diallyl sulphide
Conditions | Yield |
---|---|
In chlorobenzene cooling (-45°C), stirring; dissolving (acetone), filtration (celite), rinsing (acetone), concentration, evaporation, stirring (ether), filtration, drying (vac.); elem. anal.; | 93% |
diallyl sulphide
3,5-bis(chloromethyl)-1,4-thiaselenane
Conditions | Yield |
---|---|
With selenium(II) chloride In acetonitrile at 0℃; for 2h; Solvent; regioselective reaction; | 93% |
diallyl sulphide
2-(3-oxo-3-phenyl-prop-1-ynyl)-cyclohex-1-enecarbaldehyde
Conditions | Yield |
---|---|
dirhodium tetraacetate In 1,2-dichloro-ethane at 80℃; for 72h; | 92% |
diallyl sulphide
trifluoromethanesulfonic acid 2-fluoroethyl ester
Conditions | Yield |
---|---|
In neat (no solvent) at 60℃; for 15h; Inert atmosphere; Sealed tube; | 92% |
diallyl sulphide
3,5-bis(bromomethyl)-1,4-thiaselenane
Conditions | Yield |
---|---|
With selenium dibromide In acetonitrile at 0℃; for 2h; Solvent; regioselective reaction; | 91% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; [Mo2(O)4{[2,2'-(1,3-phenylene)bis(4,5-dihydrooxazole-4,2-diyl)]dimethanol}(acac)2] In 1,2-dichloro-ethane for 0.0833333h; Reflux; | A 90% B 10% |
With dihydrogen peroxide; methyltrioxorhenium(VII) In ethanol for 2h; Ambient temperature; | A 81% B 2% |
With 1H-imidazole; (TMPP)MnOAc; tetrabutylammonium periodite In dichloromethane at 20℃; for 4h; Reagent/catalyst; | A 17.3% B 26.6% |
diallyl sulphide
(2-formyl-cyclohex-1-enyl)-propynoic acid methyl ester
Conditions | Yield |
---|---|
dirhodium tetraacetate In dichloromethane for 120h; Heating; | A n/a B 90% |
diallyl sulphide
2-(trimethylsilyl)phenyl trifluoromethanesulfonate
hexa-1,5-dien-3-yl(phenyl)sulfane
Conditions | Yield |
---|---|
With cesium fluoride In acetonitrile at 70℃; for 18h; Solvent; Reagent/catalyst; Schlenk technique; Inert atmosphere; | 90% |
ethyl 2-phenyldiazoacetate
diallyl sulphide
ethyl 2-phenyl-2-(allylthio)-4-pentenoate
Conditions | Yield |
---|---|
With Rh2[(N-(4-dodecylphenyl)sulfonyl)-(S)-prolinate]4 | 89% |
With silver trifluoromethanesulfonate In dichloromethane at 35℃; for 21h; Doyle-Kirmse reaction; Inert atmosphere; chemoselective reaction; | 84% |
diethyl (1-diazo-2,2,2-trifluoroethyl)phosphonate
diallyl sulphide
diethyl [1-(allylthio)-1-(trifluoromethyl)but-3-en-1-yl]phosphonate
Conditions | Yield |
---|---|
With bis(1,1,1-trifluoroacetylacetonato)copper(II) In toluene at 100℃; Inert atmosphere; | 89% |
diallyl sulphide
diazoethane
Conditions | Yield |
---|---|
rhodium(II) acetate at 25℃; for 0.333333h; | A 11% B 87% |
(η5-cyclopentadienyl)Re(NO)(P(C6H5)3)(CF3SO3)
diallyl sulphide
Conditions | Yield |
---|---|
In chlorobenzene 48 h; volatiles removal (vac.), dissolving (acetone), filtration, washing (ether and pentane), drying; elem. anal.; | 86% |
In not given elem. anal., (1)H-, (13)C-, (31)P-NMR; | 79-86 |
diallyl sulphide
monochloroborane dimethyl sulfide complex
5-chloro-1-thia-5-boracyclooctane
Conditions | Yield |
---|---|
In pentane to a mixt. of diallyl sulfide in pentane (dry ice-acetone bath) is added dropwise a chloroborane-dimethyl sulfide complex to the vigorously-stirred soln. over a period of 2 h (-20°C), mixt. is warmed to room temp. and stirred (2 h); solvent is removed, residue is heated to 150°C and then distd. under reduced pressure, elem. anal.; | 84.8% |
diallyl sulphide
methyl 2-diazo-2-(dimethoxyphosphoryl)acetate
Conditions | Yield |
---|---|
dirhodium tetraacetate In dichloromethane Heating; | 84% |
Conditions | Yield |
---|---|
With cetyltrimethylammonim bromide; 4,4'-dicyano-4,4'-azo-di-valeric acid In water at 80℃; for 4h; | 84% |
Conditions | Yield |
---|---|
In chloroform-d1 Ar atmosphere, addn. of butadiyne to soln. of Ru complex, 30 min, addn. of S(C3H5)2, 30 min; removement of solvent (vacuum), concn. of mother liquor, recrystn. (CH2Cl2/Et2O); elem. anal.; | 84% |
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