As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryHebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryQingdao Greenchem international Trading Co.,Ltd. is the commercial company which is invested by BeiJing Greenchem Technology Co.,Ltd. in Qingdao. It takes charge of export and production promotion, as well as imports and selling relevant produc
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inquiryAbout Product Technical Details CAS: 250285-32-6 MF: C27H37ClN2 MW: 425.05 EINECS: 627-434-9 Product Categories: organic amine;Achiral Nitrogen;Imidazolium Compounds;Lig
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inquiry1,3-BIS(2,6-DIISOPROPYLPHENYL)IMIDAZOLIUM CHLORIDE Basic information Product Name: 1,3-BIS(2,6-DIISOPROPYLPHENYL)IMIDAZOLIUM CHLORIDE Synonyms: 1,3-BIS(2,6-DI-I-PROPYLPHENYL)IMIDAZOLIUM
With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct name 1,3-BIS(2,6-DIISOPROPYLPHENYL)IMIDAZOLIUM CHLORIDE CAS Number 250285-32-6 Synonyms 1,3-Bis(2,6-diisopropylphenyl)imidazoliumchloride,97%;1,3-BIS(2,6-DIISOPROPYLPHENYL)IMIDAZOLI&;1,3-BIS[2,6-BIS
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inquiry1,3-Bis (2,6-diisopropylphenyl) imidazolium chloride CAS:250285-32-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, speciali
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryWhy Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
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inquiry1,3-BIS(2,6-DIISOPROPYLPHENYL)IMIDAZOLIUM CHLORIDE Chemical Properties Melting point 278 °C (dec.)(lit.) form Powder color White, off-white or tan Water Solubility Slightly soluble in water. Sensitive Hygroscopic InChIKey A
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryHunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryC34H50Cl2N4Pd
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With trifluoroacetic acid In chloroform-d1 at 20℃; for 12h; Inert atmosphere; | 100% |
formaldehyd
1,2-bis(2,6-diisopropylphenylimino)ethane
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With chloro-trimethyl-silane In ethyl acetate at 70℃; for 2h; | 97% |
With chloro-trimethyl-silane In ethyl acetate at 70℃; for 2h; Inert atmosphere; Glovebox; | 87% |
With chloro-trimethyl-silane In ethyl acetate at 70℃; for 2.75h; Inert atmosphere; | 86% |
1,2-bis(2,6-diisopropylphenylimino)ethane
ethyl chloromethyl ether
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 24h; Molecular sieve; Inert atmosphere; | 94% |
With air In tetrahydrofuran; water at 40℃; for 16h; Solvent; | 65% |
With water In tetrahydrofuran at 40℃; for 16h; Condensation; | 47% |
formaldehyd
(1E,2E)-N1,N2-bis(2,6-diisopropylphenyl)-ethane-1,2-diimine
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With chloro-trimethyl-silane In ethyl acetate at 70℃; for 2h; | 90% |
With chloro-trimethyl-silane In ethyl acetate at 70℃; for 2h; | 89% |
With hydrogenchloride In 1,4-dioxane; ethyl acetate at 20℃; for 17h; | 86% |
Stage #1: formaldehyd; (1E,2E)-N1,N2-bis(2,6-diisopropylphenyl)-ethane-1,2-diimine In toluene at 100℃; Formylation; Stage #2: With hydrogenchloride In 1,4-dioxane; toluene at 70℃; for 5h; chloridation; | 47% |
With hydrogenchloride In 1,4-dioxane; ethyl acetate at 20℃; Heating; | 41% |
formaldehyd
Glyoxal
2,6-diisopropylbenzenamine
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With hydrogenchloride In methanol for 36h; Reflux; | 84.6% |
chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I)
A
1,3-bis[2,6-di(propan-2-yl)phenyl]-1,3-dihydro-2H-imidazol-2-one
B
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With air In dimethylsulfoxide-d6 at 150℃; for 155h; | A 16% B 81% |
With water; oxygen In dimethylsulfoxide-d6 at 150℃; for 155h; Kinetics; Sealed tube; | A 16 %Spectr. B 81 %Spectr. |
methanol
1,2-bis(2,6-diisopropylphenylimino)ethane
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
Stage #1: methanol; 1,2-bis(2,6-diisopropylphenylimino)ethane With sodium tetrahydroborate In tetrahydrofuran at 0 - 20℃; for 3h; Stage #2: With ammonium chloride In tetrahydrofuran | 80% |
1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene
B
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With trichlorosilane In toluene at 25℃; for 12h; Inert atmosphere; | A 79% B n/a |
1,2-bis(2,6-diisopropylphenylimino)ethane
paracetaldehyde
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With chloro-trimethyl-silane In ethyl acetate at 70℃; for 2.75h; | 76% |
formaldehyd
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran; 1,4-dioxane at 40℃; for 72h; | 58% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 140℃; for 20h; Inert atmosphere; Schlenk technique; Sealed tube; | A n/a B 54% |
chloromethyl methyl ether
1,2-bis(2,6-diisopropylphenylimino)ethane
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
at 40℃; for 16h; Sealed tube; | 52% |
at 40℃; for 16h; Sealed tube; | 52% |
2,6-diisopropylbenzenamine
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 77.5 percent / formic acid / ethanol; H2O / 48 h 2.1: toluene / 100 °C 2.2: 47 percent / HCl / toluene; dioxane / 5 h / 70 °C View Scheme | |
Multi-step reaction with 2 steps 1: 90 percent / propan-1-ol; H2O / 1 h / 70 °C 2: 47 percent / water / tetrahydrofuran / 16 h / 40 °C View Scheme | |
Multi-step reaction with 2 steps 1: ethanol / 12 h / 20 °C 2: tetrahydrofuran / 18 h / 40 °C / Inert atmosphere View Scheme |
Glyoxal
2,6-diisopropylbenzenamine
ethyl chloromethyl ether
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
Inert atmosphere; |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
Stage #1: trans-[PdCl2(1,3-diethylimidazole)(1,3-(2,6-(i-Pr)2C6H3)2C3H2N2)] With silver tetrafluoroborate In [D3]acetonitrile at 80℃; for 48h; Inert atmosphere; Stage #2: With lithium chloride In [D3]acetonitrile Inert atmosphere; |
C27H36Cl3N2P
1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene
B
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
at -30 - 20℃; for 50h; Inert atmosphere; |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With chloroform |
1-(2,6-diisopropylphenyl)-1H-imidazole
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
In acetonitrile for 36h; Reflux; Inert atmosphere; Schlenk technique; |
Glyoxal
2,6-diisopropylbenzenamine
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With chloro-trimethyl-silane In formic acid |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 140℃; for 21h; Inert atmosphere; Schlenk technique; Sealed tube; | 21 %Chromat. |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 140℃; for 21h; Inert atmosphere; Schlenk technique; Sealed tube; | 18 %Chromat. |
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 100℃; for 1h; Inert atmosphere; Schlenk technique; Sealed tube; | A 49 %Chromat. B 41 %Chromat. |
In N,N-dimethyl-formamide at 140℃; for 21h; Inert atmosphere; Schlenk technique; Sealed tube; | A 32 %Chromat. B 56 %Chromat. |
Multi-step reaction with 2 steps 1: chloroform-d1 / 24 h / 40 °C / Inert atmosphere; Schlenk technique; Sealed tube 2: N,N-dimethyl-formamide / 1 h / 100 °C / Inert atmosphere; Schlenk technique; Sealed tube View Scheme |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: N,N-dimethyl-formamide / 21 h / 140 °C / Inert atmosphere; Schlenk technique; Sealed tube 2: N,N-dimethyl-formamide / 21 h / 140 °C / Inert atmosphere; Schlenk technique; Sealed tube View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine / chloroform-d1 / 60 °C / Inert atmosphere; Schlenk technique; Sealed tube 2: N,N-dimethyl-formamide / 21 h / 140 °C / Inert atmosphere; Schlenk technique; Sealed tube View Scheme | |
Multi-step reaction with 3 steps 1: chloroform-d1 / 24 h / 40 °C / Inert atmosphere; Schlenk technique; Sealed tube 2: 1,4-dioxane / 0.5 h / 50 °C / Inert atmosphere; Schlenk technique 3: N,N-dimethyl-formamide / 21 h / 140 °C / Inert atmosphere; Schlenk technique; Sealed tube View Scheme | |
Multi-step reaction with 3 steps 1: chloroform-d1 / 24 h / 40 °C / Inert atmosphere; Schlenk technique; Sealed tube 2: 1,4-dioxane / 0.5 h / 50 °C / Inert atmosphere; Schlenk technique 3: N,N-dimethyl-formamide / 21 h / 140 °C / Inert atmosphere; Schlenk technique; Sealed tube View Scheme | |
Multi-step reaction with 3 steps 1: chloroform-d1 / 24 h / 40 °C / Inert atmosphere; Schlenk technique; Sealed tube 2: N,N-dimethyl-formamide / 1 h / 100 °C / Inert atmosphere; Schlenk technique; Sealed tube 3: N,N-dimethyl-formamide / 21 h / 140 °C / Inert atmosphere; Schlenk technique; Sealed tube View Scheme |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1,4-dioxane / 0.5 h / 50 °C / Inert atmosphere; Schlenk technique 2: N,N-dimethyl-formamide / 21 h / 140 °C / Inert atmosphere; Schlenk technique; Sealed tube View Scheme | |
Multi-step reaction with 2 steps 1: 1,4-dioxane / 0.5 h / 50 °C / Inert atmosphere; Schlenk technique 2: N,N-dimethyl-formamide / 21 h / 140 °C / Inert atmosphere; Schlenk technique; Sealed tube View Scheme | |
Multi-step reaction with 2 steps 1: N,N-dimethyl-formamide / 1 h / 100 °C / Inert atmosphere; Schlenk technique; Sealed tube 2: N,N-dimethyl-formamide / 21 h / 140 °C / Inert atmosphere; Schlenk technique; Sealed tube View Scheme |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 100℃; for 1h; Inert atmosphere; Schlenk technique; Sealed tube; | A 33 %Chromat. B 38 %Chromat. |
1-bromomethyl-4-nitro-benzene
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
1,3-bis(2,6-diisopropylphenyl)-2-(4-nitrobenzylidene)-2,3-dihydro-1H-imidazole
Conditions | Yield |
---|---|
Stage #1: 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride With potassium tert-butylate In tetrahydrofuran at 20℃; for 8h; Inert atmosphere; Stage #2: 1-bromomethyl-4-nitro-benzene In tetrahydrofuran at 20℃; for 38h; Inert atmosphere; | 100% |
Stage #1: 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride With potassium tert-butylate; sodium hydride In tetrahydrofuran at 25℃; for 0.25h; Schlenk technique; Inert atmosphere; Stage #2: 1-bromomethyl-4-nitro-benzene In tetrahydrofuran at 48℃; for 72h; Schlenk technique; Inert atmosphere; | 61% |
bis(benzonitrile)palladium(II) dichloride
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With KO(tBu) In tetrahydrofuran Ar; Pd compd.(2.5 mmol), ligand (2.5 mmol), and KO(tBu) (2.5 mmol) in THF, stirred at room temp. for 12 h, THF soln. of NaCp (5 mmol) added, mixt. stirred overnight at room temp.; chromd.; | 99% |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
1,3-bis(2,6-diisopropylphenyl)-1H-imidazole-2(3H)-thione
Conditions | Yield |
---|---|
Stage #1: 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride With sulfur In acetone at 40℃; for 0.25h; Stage #2: With triethylamine In acetone at 60℃; | 99% |
With potassium carbonate; sulfur In acetone at 60℃; for 16h; Reagent/catalyst; | 99% |
With potassium tert-butylate; sulfur In tetrahydrofuran at 20℃; | 87% |
2-Picolinic acid
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran for 12h; Inert atmosphere; Reflux; | 99% |
With caesium carbonate In 1,4-dioxane at 80℃; for 20h; Schlenk technique; Inert atmosphere; | 65% |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
In acetone at 60℃; for 1h; | 99% |
In neat (no solvent) for 0.0833333h; Solvent; Green chemistry; | 99% |
In acetone at 60℃; for 1h; | 99% |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
In acetone at 60℃; for 1h; | 99% |
In acetone at 60℃; for 1h; | 99% |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
In neat (no solvent) for 0.0833333h; Green chemistry; | 99% |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
In neat (no solvent) for 0.0833333h; Green chemistry; | 99% |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
In neat (no solvent) for 0.0833333h; Green chemistry; | 99% |
7,8-benzoquinoline
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran at 50℃; for 18h; Inert atmosphere; | 99% |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
for 0.0833333h; | 99% |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
for 0.0833333h; | 99% |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
for 0.0833333h; | 99% |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
Milling; | 99% |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
Milling; | 99% |
acetic acid
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With Amberlyst A26 hydroxide In methanol; water at 70℃; | 98.9% |
3-Chloropyridine
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With sodium carbonate at 80℃; for 16h; Product distribution / selectivity; | 98% |
With caesium carbonate at 80℃; for 16h; Reactivity; | 93% |
With potassium carbonate at 80℃; for 16h; Product distribution / selectivity; | 80% |
chloroacetonitrile
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
[1,3-bis(2,6-diisopropylphenyl)-2,3-dihydro-1H-imidazol-2-ylidene]acetonitrile
Conditions | Yield |
---|---|
Stage #1: 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride With potassium tert-butylate In tetrahydrofuran at 20℃; for 1.5h; Inert atmosphere; Sonication; Stage #2: chloroacetonitrile In tetrahydrofuran at 20℃; for 72h; Inert atmosphere; | 98% |
With potassium tert-butylate In tetrahydrofuran-d8 at 20℃; anaerobic conditions; ultrasonification; |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With ammonium hexafluorophosphate In water at 20℃; for 0.166667h; Inert atmosphere; | 98% |
With potassium hexafluorophosphate In water at 20℃; Inert atmosphere; Glovebox; |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 60℃; for 5h; | 98% |
With potassium carbonate In ethanol at 60℃; for 5h; Green chemistry; | 98% |
Stage #1: bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride In acetone at 60℃; Stage #2: With triethylamine In acetone at 60℃; | 77% |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With N-iodo-succinimide In dichloromethane at 40℃; for 3h; Sealed tube; | 98% |
vinyl acetate
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
2-(1-acetoxy-1-ethyl)-1,3-bis(2,6-diisopropylphenyl)imidazolium chloride
Conditions | Yield |
---|---|
Stage #1: 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride With potassium tert-butylate In tetrahydrofuran for 0.166667h; Stage #2: vinyl acetate In tetrahydrofuran | 97% |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With dimethylsulfide gold(I) chloride; potassium carbonate In acetone at 60℃; for 1h; Reagent/catalyst; Solvent; Temperature; Time; | 97% |
Multi-step reaction with 2 steps 1: dichloromethane / 0.25 h 2: potassium carbonate / dichloromethane / 1.5 h View Scheme | |
Multi-step reaction with 2 steps 1: dimethyl sulfoxide; methanol / Schlenk technique; Inert atmosphere 2: dimethyl sulfoxide; methanol / 4 h / 20 °C / Schlenk technique; Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: dichloromethane / Darkness 2: dichloromethane View Scheme | |
Multi-step reaction with 2 steps 1: acetone / 0.17 h / 60 °C 2: sodium acetate / acetone / 0.83 h / 60 °C View Scheme |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
Milling; | 97% |
In neat (no solvent, solid phase) for 0.166667h; Milling; |
tetrakis(actonitrile)copper(I) hexafluorophosphate
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
With sodium t-butanolate In tetrahydrofuran (Ar); glovebox; mixt. of Cu complex, ligand and NaO-t-Bu in THF was stirred for 6 h; filtered through Celite (THF); filtrate mixed with hexane; filtered; elem. anal.; | 96% |
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
In dichloromethane byproducts: LiCl; under inert gas, imidazolinium-compd. dissolved in CH2Cl2, aluminate-compd. in CH2Cl2 added whilst stirring; filtered through Celite, washed with CH2Cl2, solv. removed, elem. anal.; | 96% |
(tetrahydrothiophene)gold(I) chloride
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
1,3-bis(2,6-diisopropylphenyl)-1H-imidazol-3-ium dichloroaurate(I)
Conditions | Yield |
---|---|
In dichloromethane for 0.25h; | 96% |
bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]
potassium carbonate
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane at 24 - 60℃; for 34h; Inert atmosphere; | 96% |
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