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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

Dibenz[b,f][1,4]oxazepine Manufacturer/High quality/Best price/In stock

Cas:257-07-8

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

Dibenz-(b,f)-1,4-oxazephine CAS 257-07-8

Cas:257-07-8

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Dibenz[b,f][1,4]oxazepine

Cas:257-07-8

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

Dibenz-(b,f)-1,4-oxazephine CAS:257-07-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic

Dibenz-(b,f)-1,4-oxazephine CAS:257-07-8

Cas:257-07-8

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Dibenz[b,f][1,4]oxazepine

Cas:257-07-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Dibenz[b,f][1,4]oxazepine

Cas:257-07-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Triumph International Development Limilted

Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis: Trading(Raw Mater

Dibenz[b,f][1,4]oxazepine

Cas:257-07-8

Min.Order:0 Metric Ton

FOB Price: $18.0 / 20.0

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Dibenz[b,f][1,4]oxazepine

Cas:257-07-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Dibenz[b,f][1,4]oxazepine

Cas:257-07-8

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

benzo[b][1,4]benzoxazepine

Cas:257-07-8

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Best OfferDibenz-(b,f)-1,4-oxazephine

Cas:257-07-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

benzo[b][1,4]benzoxazepine

Cas:257-07-8

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

benzo[b][1,4]benzoxazepine

Cas:257-07-8

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

benzo[b][1,4]benzoxazepine

Cas:257-07-8

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Golden Pharma Co., Limited

GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

Dibenz-(b,f)-1,4-oxazephine

Cas:257-07-8

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

benzo[b][1,4]benzoxazepine

Cas:257-07-8

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Hebei Mojin Biotechnology Co.,Ltd

We produce carbomer by our own factory,carbomer 940 is our best seller.It is used for cosmetic and medical.And we also become agent for lubrizol.Our carbomer 940 get high viscosity and good transparency.The price will depond on the market,surely supp

Dibenz[b,f][1,4]oxazepine

Cas:257-07-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

benzo[b][1,4]benzoxazepine

Cas:257-07-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

Dibenz[b,f][1,4]oxazepine

Cas:257-07-8

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

Dibenz[b,f][1,4]oxazepine

Cas:257-07-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

Dibenz-(b,f)-1,4-oxazephine

Cas:257-07-8

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Dibenz[b,f][1,4]oxazepine

Cas:257-07-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Langyou International Trading Co., Ltd

benzo[b][1,4]benzoxazepine Application:benzo[b][1,4]benzoxazepine

benzo[b][1,4]benzoxazepine

Cas:257-07-8

Min.Order:0

Negotiable

Type:Other

inquiry

DB BIOTECH CO., LTD

best seller Application:API

Dibenz-(b,f)-1,4-oxazephine

Cas:257-07-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

Dibenz[b,f][1,4]oxazepine cas 257-07-8Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

Dibenz[b,f][1,4]oxazepine cas 257-07-8

Cas:257-07-8

Min.Order:0

Negotiable

Type:Other

inquiry

Wuhan ZeShanCheng Biomedical Technology Co., Ltd.

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highl

Dibenz[b,f][1,4]oxazepine

Cas:257-07-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

Dibenz-(b,f)-1,4-oxazephine

Cas:257-07-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Muhuang Technology Co., Ltd

best seller Application:API

benzo[b][1,4]benzoxazepine

Cas:257-07-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou ZeErRui Chemical Co., Ltd.

Hangzhou ZeErRui Chemical Co., Ltd. is focused on customization, research and development and production of APIs and advanced intermediates, which can effectively compensate for the deficiencies of traditional CRO and CMO. Priority of high-tech barri

benzo[b][1,4]benzoxazepine

Cas:257-07-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Newgreat Chemical Co., Ltd

Wuhan Xinweiye Chemical Co., Ltd. is mainly engaged in the process development and production of customized synthesis and pharmaceutical intermediates. We have professional researchers in organic synthesis, analytical chemistry and production process

benzo[b][1,4]benzoxazepine

Cas:257-07-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

2-Fluorobenzaldehyde
446-52-6

2-Fluorobenzaldehyde

2-amino-phenol
95-55-6

2-amino-phenol

A

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

B

2-(2-fluorophenyl)benzo[d]oxazole
212758-52-6

2-(2-fluorophenyl)benzo[d]oxazole

Conditions
ConditionsYield
With oxygen; 1,3-diethyl-1H-benzo[d]imidazol-3-ium bromide; sodium hydroxide In o-xylene; para-xylene; m-xylene at 120℃; for 10h; Molecular sieve; Green chemistry;A 25%
B 65%
2-Fluorobenzaldehyde
446-52-6

2-Fluorobenzaldehyde

2-amino-phenol
95-55-6

2-amino-phenol

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
With poly(ethylene glycol)-400; potassium carbonate at 100℃; for 8h; Product distribution; Further Variations:; Reagents; Solvents; Temperatures; time;89%
Stage #1: 2-amino-phenol In polyethylene glycol (300) at 50℃; for 0.5h;
Stage #2: 2-Fluorobenzaldehyde In polyethylene glycol (300) at 50℃; for 10h;
Stage #3: With potassium carbonate In polyethylene glycol (300) at 100℃; for 10h;
80%
With potassium carbonate at 100℃; Sealed tube;58%
2-[(2-chlorobenzylidene)amino]phenol
6266-10-0

2-[(2-chlorobenzylidene)amino]phenol

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
Stage #1: 2-[(2-chlorobenzylidene)amino]phenol With potassium hydroxide In methanol at 20℃; for 0.583333h;
Stage #2: In dimethyl sulfoxide at 120℃; for 2h; Further stages.;
75%
Stage #1: 2-[(2-chlorobenzylidene)amino]phenol With potassium hydroxide In methanol at 20℃; for 1h;
Stage #2: In dimethyl sulfoxide at 150℃; for 6h;
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
View Scheme
2-chloro-benzaldehyde
89-98-5

2-chloro-benzaldehyde

2-amino-phenol
95-55-6

2-amino-phenol

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
With potassium hydroxide In N,N-dimethyl-formamide at 120℃; for 0.1h; Temperature; Reagent/catalyst; Microwave irradiation;87%
Stage #1: 2-chloro-benzaldehyde; 2-amino-phenol In 5,5-dimethyl-1,3-cyclohexadiene for 2h; Reflux;
Stage #2: In 5,5-dimethyl-1,3-cyclohexadiene at 120℃; for 24h;
Stage #3: With sodium In 5,5-dimethyl-1,3-cyclohexadiene for 6h; Reflux;
75%
phenylacetylene
536-74-3

phenylacetylene

2-amino-phenol
95-55-6

2-amino-phenol

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
With tetrabutylammonium acetate; palladium diacetate; 1,2-diamino-benzene In N,N-dimethyl-formamide at 120℃; Microwave irradiation;82%
N-(2-phenoxyphenyl)formamide
2770-12-9

N-(2-phenoxyphenyl)formamide

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
With polyphosphiric acid; trichlorophosphate at 120 - 130℃; for 2h; Cyclization;75%
2-formamido-4'-tert-butyldiphenyl ester

2-formamido-4'-tert-butyldiphenyl ester

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
With polyphosphiric acid; trichlorophosphate at 120 - 130℃; for 2h; Cyclization;56%
benzaldehyde
100-52-7

benzaldehyde

2-amino-phenol
95-55-6

2-amino-phenol

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
With potassium carbonate at 100℃; for 5h;68%
2-amino-phenol
95-55-6

2-amino-phenol

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
3: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
View Scheme
Multi-step reaction with 3 steps
1: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
3: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
View Scheme
Multi-step reaction with 3 steps
1: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
3: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
View Scheme
2-formamido-4'-tert-butyldiphenyl ester

2-formamido-4'-tert-butyldiphenyl ester

A

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

B

2-tert-butyl-dibenzo[b,f][1,4]oxazepine

2-tert-butyl-dibenzo[b,f][1,4]oxazepine

Conditions
ConditionsYield
With polyphosphiric acid; trichlorophosphate at 120 - 130℃; for 2h; Cyclization;A 23%
B 31%
2-Fluorobenzaldehyde
446-52-6

2-Fluorobenzaldehyde

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
3: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
View Scheme
Multi-step reaction with 3 steps
1: potassium tert-butylate / N,N-dimethyl-formamide / 140 °C / Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
3: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
View Scheme
Multi-step reaction with 3 steps
1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 140 °C / Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
3: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
View Scheme
2-(2-nitrophenoxy)benzaldehyde
66961-19-1

2-(2-nitrophenoxy)benzaldehyde

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
With iron In methanol; water for 6h; Reflux;
2-phenoxybenzamide
72084-13-0

2-phenoxybenzamide

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
With PPA at 120 - 130℃; Cyclization;
C13H9FNO(1-)*K(1+)

C13H9FNO(1-)*K(1+)

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 140℃; Microwave irradiation;
C13H9FNO(1-)*Na(1+)

C13H9FNO(1-)*Na(1+)

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 140℃; Microwave irradiation;
C13H10FNO

C13H10FNO

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 140℃; Microwave irradiation;
C13H10ClNO

C13H10ClNO

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 140℃; Microwave irradiation;
C13H10BrNO

C13H10BrNO

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 140℃; Microwave irradiation;
C13H10INO

C13H10INO

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 140℃; Microwave irradiation;
2-chloro-benzaldehyde
89-98-5

2-chloro-benzaldehyde

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
3: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
View Scheme
ortho-bromobenzaldehyde
6630-33-7

ortho-bromobenzaldehyde

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
3: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
View Scheme
2-iodobenzaldehyde
26260-02-6

2-iodobenzaldehyde

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
3: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
View Scheme
C13H9FNO(1-)*K(1+)

C13H9FNO(1-)*K(1+)

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
View Scheme
C13H9FNO(1-)*Na(1+)

C13H9FNO(1-)*Na(1+)

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
View Scheme
GRI 378898
2805-76-7

GRI 378898

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
View Scheme
2-Hydroxy-N-<2-brom-benzyliden>-anilin
36456-43-6

2-Hydroxy-N-<2-brom-benzyliden>-anilin

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
View Scheme
C13H10INO
218280-60-5

C13H10INO

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
2: N,N-dimethyl-formamide / 140 °C / Microwave irradiation
View Scheme
S-phenyl 2-diazoethanethiolate
72228-26-3

S-phenyl 2-diazoethanethiolate

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

(+/-)-trans-2-phenylthioazeto[1,2-d]dibenzo[b,f]oxazepin-1-one

(+/-)-trans-2-phenylthioazeto[1,2-d]dibenzo[b,f]oxazepin-1-one

Conditions
ConditionsYield
In toluene at 80℃; for 1.5h; Staudinger reaction;99%
In benzene at 80℃; for 1h;99%
indole
120-72-9

indole

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

2-(2-(di(1H-indol-3-yl)methyl)phenoxy)aniline

2-(2-(di(1H-indol-3-yl)methyl)phenoxy)aniline

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane at 20℃; for 3h; Catalytic behavior; Solvent; Friedel-Crafts Alkylation;99%
5-benzyloxy-1H-indole
1215-59-4

5-benzyloxy-1H-indole

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

2-(2-(bis(5-(benzyloxy)-1H-indol-3-yl)methyl)phenoxy)aniline

2-(2-(bis(5-(benzyloxy)-1H-indol-3-yl)methyl)phenoxy)aniline

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane at 20℃; for 3h; Friedel-Crafts Alkylation;99%
7-methyl-1H-indole
933-67-5

7-methyl-1H-indole

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

2-(2-(bis(7-methyl-1H-indol-3-yl)methyl)phenoxy)aniline

2-(2-(bis(7-methyl-1H-indol-3-yl)methyl)phenoxy)aniline

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane at 20℃; for 3h; Friedel-Crafts Alkylation;99%
dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

10H-dibenzo[b,f][1,4]oxazepin-11-one
3158-85-8

10H-dibenzo[b,f][1,4]oxazepin-11-one

Conditions
ConditionsYield
With dipotassium peroxodisulfate In ethanol; N,N-dimethyl-formamide at 50℃; for 1h; Time; Reagent/catalyst;98%
5-methoxylindole
1006-94-6

5-methoxylindole

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

2-(2-(bis(5-methoxy-1H-indol-3-yl)methyl)phenoxy)aniline

2-(2-(bis(5-methoxy-1H-indol-3-yl)methyl)phenoxy)aniline

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane at 20℃; for 1.5h; Friedel-Crafts Alkylation;98%
1,5,7-trimethyl-3-diazooxindole

1,5,7-trimethyl-3-diazooxindole

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

spiro[5,7-dimethyloxindole-imidazo-bis(tetrahydro-dibenzo[1,4]oxazepine)]

spiro[5,7-dimethyloxindole-imidazo-bis(tetrahydro-dibenzo[1,4]oxazepine)]

Conditions
ConditionsYield
With toluene-4-sulfonic acid In tetrahydrofuran at 15 - 20℃; for 24h; diastereoselective reaction;93%
3-diazo-1-methyl-1,3-dihydro-indol-2-one
3265-14-3

3-diazo-1-methyl-1,3-dihydro-indol-2-one

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

spiro[1-methyloxindole-imidazo-bis(tetrahydro-dibenzo[1,4]oxazepine)]

spiro[1-methyloxindole-imidazo-bis(tetrahydro-dibenzo[1,4]oxazepine)]

Conditions
ConditionsYield
With toluene-4-sulfonic acid In tetrahydrofuran at 15 - 20℃; for 24h; diastereoselective reaction;93%
3-diazo-1-methyl-1,3-dihydro-indol-2-one
3265-14-3

3-diazo-1-methyl-1,3-dihydro-indol-2-one

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

C35H25N3O3

C35H25N3O3

Conditions
ConditionsYield
With p-toluenesulfonic acid monohydrate In tetrahydrofuran at 20℃; for 24h; Reagent/catalyst; diastereoselective reaction;93%
C10H9N3O
1416060-68-8

C10H9N3O

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

C36H27N3O3

C36H27N3O3

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 24h; diastereoselective reaction;93%
trimethylsilyl cyanide
7677-24-9

trimethylsilyl cyanide

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

(R)-10,11-dihydrodibenzo[b,f][1,4]oxazepine-11-carbonitrile

(R)-10,11-dihydrodibenzo[b,f][1,4]oxazepine-11-carbonitrile

Conditions
ConditionsYield
With 1-[3,5-bis(trifluoromethyl)phenyl]-3-{(S)[(2S,4S,5R)-5-ethyl-1-aza-bicyclo[2.2.2]oct-2-yl]-(6-methoxy-4-quinolinyl)methyl}thiourea; 2,2,2-trifluoroethanol In 1,2-dichloro-ethane at 4℃; for 30h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; enantioselective reaction;93%
1-ethenylcyclohexene
931-49-7

1-ethenylcyclohexene

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

(R)-11-(cyclohexenylethynyl)-10,11-dihydrodibenzo[b,f][1,4]oxazepine

(R)-11-(cyclohexenylethynyl)-10,11-dihydrodibenzo[b,f][1,4]oxazepine

Conditions
ConditionsYield
With (S)-CPA; silver(I) acetate In 1,4-dioxane at 15℃; for 72h; enantioselective reaction;92%
butanone
78-93-3

butanone

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

(R)-1-(10,11-dihydrodibenzo[b,f][1,4]oxazepin-11-yl)butan-2-one

(R)-1-(10,11-dihydrodibenzo[b,f][1,4]oxazepin-11-yl)butan-2-one

Conditions
ConditionsYield
With L-proline In N,N-dimethyl-formamide at 20℃; Molecular sieve; enantioselective reaction;92%
dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

1-benzyl-3-diazo-1,3-dihydro-2H-indol-2-one
461677-71-4

1-benzyl-3-diazo-1,3-dihydro-2H-indol-2-one

spiro[1-benzyloxindole-imidazo-bis(tetrahydro-dibenzo[1,4]oxazepine)]

spiro[1-benzyloxindole-imidazo-bis(tetrahydro-dibenzo[1,4]oxazepine)]

Conditions
ConditionsYield
With toluene-4-sulfonic acid In tetrahydrofuran at 15 - 20℃; for 24h; diastereoselective reaction;92%
dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

1-benzoyl-3- diazoindolin-2-one
20352-79-8

1-benzoyl-3- diazoindolin-2-one

spiro[1-benzoyloxindole-imidazo-bis(tetrahydro-dibenzo[1,4]oxazepine)]

spiro[1-benzoyloxindole-imidazo-bis(tetrahydro-dibenzo[1,4]oxazepine)]

Conditions
ConditionsYield
With toluene-4-sulfonic acid In tetrahydrofuran at 15 - 20℃; for 24h; diastereoselective reaction;92%
dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

1-benzyl-3-diazo-1,3-dihydro-2H-indol-2-one
461677-71-4

1-benzyl-3-diazo-1,3-dihydro-2H-indol-2-one

C41H29N3O3

C41H29N3O3

Conditions
ConditionsYield
With p-toluenesulfonic acid monohydrate In diethyl ether at 20℃; for 24h; Reagent/catalyst; Solvent; diastereoselective reaction;92%
dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

1-benzoyl-3- diazoindolin-2-one
20352-79-8

1-benzoyl-3- diazoindolin-2-one

C41H27N3O4

C41H27N3O4

Conditions
ConditionsYield
In para-xylene at 20℃; for 24h; diastereoselective reaction;92%
5-methoxylindole
1006-94-6

5-methoxylindole

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

11-(5-methoxy-1H-indol-3-yl)-10,11-dihydrodibenzo[b,f][1,4]oxazepine

11-(5-methoxy-1H-indol-3-yl)-10,11-dihydrodibenzo[b,f][1,4]oxazepine

Conditions
ConditionsYield
With trifluoroacetic acid In tetrahydrofuran at 20℃; for 0.5h; Friedel-Crafts Alkylation;91%
1-methylindole
603-76-9

1-methylindole

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

11-(1-methyl-1H-indol-3-yl)-10,11-dihydrodibenzo[b,f][1,4]oxazepine

11-(1-methyl-1H-indol-3-yl)-10,11-dihydrodibenzo[b,f][1,4]oxazepine

Conditions
ConditionsYield
With trifluoroacetic acid In tetrahydrofuran at 20℃; for 1.5h; Friedel-Crafts Alkylation;91%
3-diazo-indolin-2-one
3265-29-0

3-diazo-indolin-2-one

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

spiro[oxindole-imidazo-bis(tetrahydro-dibenzo[1,4]oxazepine)]

spiro[oxindole-imidazo-bis(tetrahydro-dibenzo[1,4]oxazepine)]

Conditions
ConditionsYield
With toluene-4-sulfonic acid In tetrahydrofuran at 15 - 20℃; for 24h; Solvent; Temperature; Reagent/catalyst; diastereoselective reaction;91%
tert-butyl 3-diazo-2-oxoindoline-1-carboxylate
1419184-25-0

tert-butyl 3-diazo-2-oxoindoline-1-carboxylate

dibenz[b,f][1,4]oxazepine
257-07-8

dibenz[b,f][1,4]oxazepine

spiro[tert-butyl-1-carboxylateoxindole-imidazo-bis(tetrahydro-dibenzo[1,4]oxazepine)]

spiro[tert-butyl-1-carboxylateoxindole-imidazo-bis(tetrahydro-dibenzo[1,4]oxazepine)]

Conditions
ConditionsYield
With toluene-4-sulfonic acid In tetrahydrofuran at 15 - 20℃; for 24h; diastereoselective reaction;91%

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