Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:933-67-5
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:933-67-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:933-67-5
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:Powder Storage:Store in sealed containers at cool & dry pla
Cas:933-67-5
Min.Order:100 Gram
Negotiable
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inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:933-67-5
Min.Order:4 Kilogram
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Type:Lab/Research institutions
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
7-MethylindoleAppearance:good Storage:2-8°C Package:according to customers' requirements Application:blocks;IndolesOxindoles;Indoles and derivatives;Pyrroles & Indoles;Indole;Indoles Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(
superior quality moderate price & quick delivery Appearance:white to slightly beige shiny flakes Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Applica
Product Name:7-MethylindoleSynonyms:7-Methylindol;Indole, 7-methyl-;7-METHYLINDOLE;7-METHYL-1H-INDOLE;7-METHYINDOLE;1H-Indole, 7-methyl-;7-Methylindole,98%;7-MetlylindoleCAS:933-67-5MF:C9H9NMW:131.17EINECS:213-270-1Product Categories:blocks
Cas:933-67-5
Min.Order:1 Metric Ton
FOB Price: $20.0
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
We Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O
1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:933-67-5
Min.Order:1 Metric Ton
FOB Price: $7.0 / 8.0
Type:Trading Company
inquiryProduct Name:7-Methylindol Synonym:7-methyl-indole;7-Me-indole;7-Metlylindole;1H-Indole, 7-methyl-;7-Methyl-indol;Indole,7-methyl; Cas No:933-67-5 Quality standard: Product name 7-Methylindol CAS NO
Cas:933-67-5
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h
Wuhu Nuovo Chemical Technology Co., Ltd. was established in August 2014, mainly engaged in the development, production and sales of ionic liquids, ribose, nucleosides, nucleotides and related chemicals; Products are mainly used in new energy, new ma
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:933-67-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
good quality and cheap price Package:25kg/200kg Application:as indole Transportation:by courier/sea/air
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
2,3-dihydro-7-methylindole
7-methyl-1H-indole
Conditions | Yield |
---|---|
With 6C44H32N6O4Ru(2+)*12Hf(2+)*8O(2-)*14HO(1-)*6C16H22ClCoN5O6(1-) In 2,2,2-trifluoroethanol; acetonitrile at 20℃; for 12h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Irradiation; | 99% |
With H8O20P8Pt2(4-)*4C34H72N(1+) In methanol Inert atmosphere; Irradiation; | 97% |
With tris(bipyridine)ruthenium(II) dichloride hexahydrate; chloropyridinecobaloxime(III) In ethanol at 30℃; for 24h; Inert atmosphere; Schlenk technique; Irradiation; | 89% |
7-methyl-1H-indole
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran; hexane at 40 - 45℃; for 40h; | 93% |
With n-butyllithium; diisopropylamine In tetrahydrofuran; hexanes at -78 - 45℃; for 40h; Inert atmosphere; | 93% |
7-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 7-methyl-1-tosylindoline In tetrahydrofuran at -78℃; for 2h; Stage #2: With oxygen In tetrahydrofuran at 20℃; | 84% |
6-methyl-2-vinylaniline
7-methyl-1H-indole
Conditions | Yield |
---|---|
With p-benzoquinone; lithium chloride; dichloro bis(acetonitrile) palladium(II) In tetrahydrofuran for 10h; Heating; | 82% |
Conditions | Yield |
---|---|
With triphenylphosphine; tin(ll) chloride; ruthenium trichloride In 1,4-dioxane; water at 180℃; for 20h; Cyclization; | 80% |
With tin(ll) chloride; ruthenium trichloride; triphenylphosphine In 1,4-dioxane; water at 180℃; for 20h; | 80% |
C9H8N2O4
7-methyl-1H-indole
Conditions | Yield |
---|---|
With indium; acetic acid In benzene at 80℃; for 5h; Inert atmosphere; | 76% |
7-methyl-1-(phenylsulfonyl)-1H-indole
7-methyl-1H-indole
Conditions | Yield |
---|---|
With potassium hydroxide In methanol; 1,2-dimethoxyethane for 24h; Heating; | 75% |
7-methyl-2-trimethylsilanyl-indole-1-carboxylic acid diethylamide
7-methyl-1H-indole
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol for 12h; Heating; | 75% |
Conditions | Yield |
---|---|
In tetrahydrofuran at -45 - -40℃; Cyclization; Bartoli reaction; | 71% |
In tetrahydrofuran at -40℃; for 0.333333h; | 67% |
In tetrahydrofuran at -40℃; for 1h; Inert atmosphere; | 34% |
1-(2-amino-3-methylphenyl)-2-chloroethan-1-one
7-methyl-1H-indole
Conditions | Yield |
---|---|
With sodium tetrahydroborate In 1,4-dioxane; water for 2h; Heating; | 71% |
Conditions | Yield |
---|---|
With phosphorus pentachloride; zinc(II) chloride for 0.0666667h; microwave irradiation; | 71% |
1-methyl-2-nitrobenzene
vinyl magnesium bromide
A
7-methyl-1H-indole
B
acetaldehyde
C
2,2'-dimethylazobenzene
D
o-toluidine
E
N,N'-Di-o-tolyl-diazene N-oxide
Conditions | Yield |
---|---|
In tetrahydrofuran at -40℃; for 0.333333h; other nitroarenes and vinyl Grignard reagents; | A 67% B n/a C n/a D 5% E n/a |
7-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: (E)-1-(3-methyl-2-nitrostyryl)pyrrolidine With iron(III) chloride; pyrographite In methanol for 0.166667h; Heating; Stage #2: With hydrazine hydrate In methanol for 3h; Heating; Further stages.; | 67% |
Conditions | Yield |
---|---|
With tin(ll) chloride; ruthenium trichloride; triphenylphosphine In 1,4-dioxane at 180℃; for 20h; | 66% |
Conditions | Yield |
---|---|
With o-toluidine In acetonitrile | 64.3% |
A
7-methyl-1H-indole
B
2,5-dimethylquinoxaline
D
2,8-dimethylquinoxaline
Conditions | Yield |
---|---|
at 650℃; under 0.01 Torr; | A 62% B 7% C n/a D 11% |
A
7-methyl-1H-indole
B
2,7-dimethyl-1H-indole
C
2,5-dimethylquinoxaline
D
2,8-dimethylquinoxaline
Conditions | Yield |
---|---|
at 650℃; under 0.01 Torr; | A 62% B 3% C 7% D 11% |
Conditions | Yield |
---|---|
With nickel(II) iodide; 4,4'-dimethyl-2,2'-bipyridines; tetra-(n-butyl)ammonium iodide; magnesium chloride; zinc In N,N-dimethyl acetamide at 20℃; for 12h; Inert atmosphere; Schlenk technique; Sealed tube; | 60% |
Conditions | Yield |
---|---|
In tetrahydrofuran at -45 - -40℃; Cyclization; Bartoli reaction; | 58% |
Conditions | Yield |
---|---|
With dimethylsulfide borane complex In tetrahydrofuran BH3*THF or LAH; | 55% |
A
7-methyl-1H-indole
B
2,7-dimethyl-1H-indole
C
2,5-dimethylquinoxaline
D
2,8-dimethylquinoxaline
Conditions | Yield |
---|---|
at 650℃; under 0.01 Torr; | A 55% B 5% C 4% D 17% |
2,6-dimethylnitrobenzene
N,N-dimethyl-formamide dimethyl acetal
7-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 2,6-dimethylnitrobenzene; N,N-dimethyl-formamide dimethyl acetal With pyrrolidine In 1,4-dioxane at 102℃; for 22h; Leimgruber-Batcho Indole Synthesis; Reflux; Inert atmosphere; Stage #2: With hydrazine hydrate In 1,4-dioxane at 45℃; for 1h; Leimgruber-Batcho Indole Synthesis; | 53% |
7-methyl-1H-indole-5-carboxylic acid
7-methyl-1H-indole
Conditions | Yield |
---|---|
With copper(I) oxide In quinoline at 230℃; for 4h; Decarboxylation; | 50% |
A
7-methyl-1H-indole
B
1-dimethylethyl (3R)-3-hydroxy-4-(7-methyl-1H-indol-3-yl)-3,6-dihydro-1(2H)-pyridinecarboxylate
Conditions | Yield |
---|---|
With potassium hydroxide In methanol at 70℃; | A 48% B 36% |
A
7-methyl-1H-indole
B
5-methylquinoxaline
Conditions | Yield |
---|---|
at 650℃; under 0.01 Torr; | A 32% B 40% |
at 650℃; under 0.01 Torr; Product distribution; Mechanism; also 15N labelled; |
ethylene glycol
o-toluidine
A
7-methyl-1H-indole
B
2-(2-tolylamino)ethan-1-ol
C
1,2-bis[(2-methylphenyl)amino]ethane
D
1,4-di-o-tolyl-piperazine
Conditions | Yield |
---|---|
With palladium on activated charcoal; zinc(II) oxide In water at 150℃; for 24h; Sealed tube; | A 20% B 28% C n/a D n/a |
7-methyl-1H-indole
Conditions | Yield |
---|---|
With calcium hydroxide; kieselguhr; water; nickel at 30 - 40℃; under 132391 Torr; Hydrogenation; |
7-methyl-1H-indole
Conditions | Yield |
---|---|
at 225 - 240℃; Vakuum; |
2,6-dimethylphenyl isonitrile
7-methyl-1H-indole
Conditions | Yield |
---|---|
With n-butyllithium; diisopropylamine Yield given. Multistep reaction; | |
Ru(H)2(1,2-bis(dimethylphosphino)ethane)2 In benzene-d6 at 140℃; for 25h; in a sealed tube; | 98 % Spectr. |
Conditions | Yield |
---|---|
Stage #1: 7-methyl-1H-indole With sodium hydride In DMF (N,N-dimethyl-formamide) at 20℃; for 0.25h; Stage #2: methyl iodide In DMF (N,N-dimethyl-formamide) at 30℃; for 1h; | 100% |
With sodium hydroxide In dimethyl sulfoxide at 20℃; | 99% |
Stage #1: 7-methyl-1H-indole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere; Stage #2: methyl iodide In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere; | 97% |
7-methyl-1H-indole
2,3-dihydro-7-methylindole
Conditions | Yield |
---|---|
Stage #1: 7-methyl-1H-indole With sodium cyanoborohydride; acetic acid In N,N-dimethyl-formamide at 20℃; for 2h; Stage #2: With water; sodium hydroxide In N,N-dimethyl-formamide | 99% |
With tetrahydroxydiboron; palladium on activated carbon In 2,2,2-trifluoroethanol; water at 40℃; for 24h; Schlenk technique; | 99% |
With sodium cyanoborohydride In acetic acid; ethyl acetate | 94% |
7-methyl-1H-indole
1,1,1-trifluoroacetophenone
(R)-2,2,2-trifluoro-1-(7-methyl-1H-indol-3-yl)-1-phenylethanol
Conditions | Yield |
---|---|
With (S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate In dichloromethane at 25℃; for 48h; optical yield given as %ee; enantioselective reaction; | 99% |
Conditions | Yield |
---|---|
With cupreidine 9-O-(4-(perfluoro-n-octyl)benzyl) ether In 1,1,1,3,3-pentafluorobutane; toluene at 20℃; for 1h; Friedel-Crafts alkylation; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
Stage #1: 7-methyl-1H-indole With C43H64N4O4; scandium tris(trifluoromethanesulfonate); ortho-chlorobenzoic acid In dichloromethane at 30℃; for 1h; Inert atmosphere; Stage #2: glyoxylic acid ethyl ester In dichloromethane at -20℃; for 12h; Friedel Crafts alkylation; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 90% |
7-methyl-1H-indole
methyl 4-phenyl-2-oxo-3-butenoate
Conditions | Yield |
---|---|
With C35H48N4O4; samarium(III) trifluoromethanesulfonate In dichloromethane at -20℃; for 27h; asymmetric Friedel-Crafts alkylation; Inert atmosphere; optical yield given as %ee; | 99% |
7-methyl-1H-indole
ethyl-3,3,3-trifluoropyruvate
3,3,3-trifluoro-2-hydroxy-2-(7-methyl-1H-indol-3-yl)-propionic acid ethyl ester
Conditions | Yield |
---|---|
Stage #1: 7-methyl-1H-indole With C33H52N4O4; zinc trifluoromethanesulfonate In dichloromethane at 35℃; for 0.5h; Stage #2: ethyl-3,3,3-trifluoropyruvate In dichloromethane at 0℃; for 0.5h; Friedel Crafts alkylation; optical yield given as %ee; enantioselective reaction; | 99% |
With (3aR,11aR,14aS,16bS)-2,2,13,13-tetra-isopropyl-3a,11a,14a,16b-tetrahydro-bis(1,3-dioxolano[4',5':3,4]pyrrolo)[1,2-a:1',2'-a]naphtho[1,2-d:8,7-d']diimidazole; copper(II) bis(trifluoromethanesulfonate) at 0℃; for 1h; Friedel-Crafts Alkylation; Inert atmosphere; Schlenk technique; stereoselective reaction; | 97.6% |
7-methyl-1H-indole
ethyl-3,3,3-trifluoropyruvate
3,3,3-trifluoro-2-hydroxy-2-(7-methyl-1H-indol-3-yl)-propionic acid ethyl ester
Conditions | Yield |
---|---|
In 1,1,1,3,3-pentafluorobutane at 20℃; for 0.5h; Inert atmosphere; | 99% |
With triethylamine In dichloromethane at 0℃; Friedel Crafts alkylation; | |
With copper(II) bis(trifluoromethanesulfonate) In chloroform at 25℃; for 16h; Friedel-Crafts Alkylation; Inert atmosphere; Schlenk technique; |
Conditions | Yield |
---|---|
With cupreine 9-O-(4-(perfluoro-n-octyl)benzyl) ether In 1,1,1,3,3-pentafluorobutane; toluene at 20℃; for 1h; Friedel-Crafts alkylation; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
7-methyl-1H-indole
dimethyl 2-(2,2,2-trifluoroethylidene)malonate
dimethyl (R)-2-(2,2,2-trifluoro-1-(7-methyl-1H-indol-3-yl)ethyl)malonate
Conditions | Yield |
---|---|
Stage #1: dimethyl 2-(2,2,2-trifluoroethylidene)malonate With copper(II) bis(trifluoromethanesulfonate); 2,2-bis[(4S)-4-isopropyloxazolin-2-yl]propane In diethyl ether at 20℃; for 0.333333h; Inert atmosphere; Stage #2: 7-methyl-1H-indole In diethyl ether at -35℃; for 10h; Friedel-Crafts alkylation; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
7-methyl-1H-indole
chloromethyl methyl ether
1-methoxymethyl-7-methylindole
Conditions | Yield |
---|---|
Stage #1: 7-methyl-1H-indole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 0.5h; Inert atmosphere; Stage #2: chloromethyl methyl ether In N,N-dimethyl-formamide; mineral oil for 1h; Inert atmosphere; | 99% |
7-methyl-1H-indole
diethyl benzalmalonate
(S)-ethyl 2-ethoxycarbonyl-3-[3-(7-methylindolyl)]-3-phenylpropanoate
Conditions | Yield |
---|---|
Stage #1: diethyl benzalmalonate With 1,1-bis[(S)-4-benzyloxazolin-2-yl]-2,2-diphenylethene; copper(II) bis(trifluoromethanesulfonate) In ethanol at 20℃; for 0.5h; Friedel-Crafts alkylation; Inert atmosphere; Stage #2: 7-methyl-1H-indole In ethanol at 20℃; for 24h; Friedel-Crafts alkylation; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
7-methyl-1H-indole
C11H10N2O4
Conditions | Yield |
---|---|
With 1,1,1,3',3',3'-hexafluoro-propanol; 6-bromo-2-(((((4S,5S)-4,5-diphenyl-1-tosyl-4,5-dihydro-1H-imidazol-2-yl)methyl)((S)-1-phenylethyl)amino)methyl)-4-nitrophenol; copper(I) triflate In toluene at 20℃; for 7h; Friedel-Crafts Alkylation; Inert atmosphere; enantioselective reaction; | 99% |
7-methyl-1H-indole
C11H10N2O3
Conditions | Yield |
---|---|
With 1,1,1,3',3',3'-hexafluoro-propanol; 6-bromo-2-(((((4S,5S)-4,5-diphenyl-1-tosyl-4,5-dihydro-1H-imidazol-2-yl)methyl)((S)-1-phenylethyl)amino)methyl)-4-nitrophenol; copper(I) triflate In toluene at 20℃; for 1h; Friedel-Crafts Alkylation; Inert atmosphere; enantioselective reaction; | 99% |
7-methyl-1H-indole
ethyl 5-methyl-2-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazine-3-carboxylate
ethyl (R)-5-methyl-3-(7-methyl-1H-indol-3-yl)-2-oxo-3,4-dihydro-2H-benzo[b][1,4]oxazine-3-carboxylate
Conditions | Yield |
---|---|
With C38H33O4P In toluene at -78℃; for 5h; enantioselective reaction; | 99% |
pyrrolidine
7-methyl-1H-indole
4-cyanobenzaldehyde
4-((7-methyl-1H-indol-3-yl)(pyrrolidin-1-yl)methyl)benzonitrile
Conditions | Yield |
---|---|
In methanol at 30℃; for 72h; | 99% |
7-methyl-1H-indole
celastrol
Conditions | Yield |
---|---|
With aluminium(III) chloride hexahydrate In dichloromethane at 20℃; for 3h; Friedel-Crafts Alkylation; Sealed tube; | 99% |
With scandium tris(trifluoromethanesulfonate) In dichloromethane at 20℃; for 24h; Friedel-Crafts Alkylation; |
7-methyl-1H-indole
(2-nitroethenyl)benzene
7-methyl-3-(2-nitro-1-phenylethyl)-1H-indole
Conditions | Yield |
---|---|
With 2,6-bis(2,2-dimethylpropionylamino)benzoic acid In chloroform at 40℃; for 24h; Friedel-Crafts Alkylation; | 99% |
7-methyl-1H-indole
ammonium thiocyanate
7-methyl-3-thiocyanato-1H-indole
Conditions | Yield |
---|---|
With oxygen In tetrahydrofuran at 25℃; under 750.075 Torr; for 7h; Irradiation; | 99% |
With copper(II) choride dihydrate; oxygen In ethanol at 20℃; for 24h; Irradiation; | 93% |
With TiO2/MoS2 In acetonitrile at 20℃; for 16h; Irradiation; | 90% |
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 20℃; for 3h; Friedel-Crafts Alkylation; | 99% |
7-methyl-1H-indole
Conditions | Yield |
---|---|
With (R)-2,6-bis(naphthalen-2-yl)-4-oxo-3,5-dioxa-4λ5-phosphacyclohepta[2,1-a;3,4-a']dinapthalen-4-ol In 1,2-dichloro-ethane at 20℃; for 16h; enantioselective reaction; | 99% |
7-methyl-1H-indole
Conditions | Yield |
---|---|
With (R)-2,6-bis(naphthalen-2-yl)-4-oxo-3,5-dioxa-4λ5-phosphacyclohepta[2,1-a;3,4-a']dinapthalen-4-ol In 1,2-dichloro-ethane at 20℃; for 16h; enantioselective reaction; | 99% |
Conditions | Yield |
---|---|
With oxygen In tetrahydrofuran at 20℃; under 760.051 Torr; Irradiation; | 99% |
With iridium(III) bis[2-(4,6-difluorophenyl)pyridinato]picolinate In acetonitrile at 25℃; Irradiation; Green chemistry; | 90% |
With iridium(III) bis[2-(4,6-difluorophenyl)pyridinato]picolinate In acetonitrile at 20℃; Irradiation; Green chemistry; | 90% |
With 3-chloro-benzenecarboperoxoic acid; sodium bromide In acetonitrile at 20℃; for 24h; regioselective reaction; | 61% |
Conditions | Yield |
---|---|
With cerium(III) chloride; silver(l) oxide In 1,2-dichloro-ethane at 20℃; Darkness; | 99% |
7-methyl-1H-indole
ethyl 3,3,3-trifluoro-2-iminopropionate
ethyl (S)-2-amino-3,3,3-trifluoro-2-(7-methyl-1H-indol-3-yl)propanoate
Conditions | Yield |
---|---|
With (S)-3-(anthracen-9-yl)-1,1'-binaphthyl-2,2'-diyl hydrogen phosphate In chloroform at -60℃; for 1h; Inert atmosphere; enantioselective reaction; | 99% |
7-methyl-1H-indole
N-(4-bromobenzylidene)-4-methylbenzenesulfonamide
Conditions | Yield |
---|---|
With (Rp)-4,12-di(4-(3',5'-bis(trifluoromethyl))-phenyl-3-yl)-[2.2]paracyclophane-hydrogenphosphate In toluene at -20℃; for 12h; Molecular sieve; enantioselective reaction; | 99% |
7-methyl-1H-indole
Conditions | Yield |
---|---|
With (11aR)-3,7-di-9-anthracenyl-10,11,12,13-tetrahydro-5-hydroxy-5-oxide diindeno[7,1de:10,70-fg][1,3,2] dioxaphosphocin In toluene at 60℃; for 3h; enantioselective reaction; | 99% |
7-methyl-1H-indole
Conditions | Yield |
---|---|
With C55H51F3N4O3PdS In toluene at 40℃; Inert atmosphere; Alkaline conditions; enantioselective reaction; | 99% |
7-methyl-1H-indole
9-phenyl-fluoren-9-ol
Conditions | Yield |
---|---|
With scandium tris(trifluoromethanesulfonate) In dichloromethane at 60℃; for 4h; Sealed tube; | 99% |
7-methyl-1H-indole
Conditions | Yield |
---|---|
With Diphenylphosphinic chloride In acetonitrile at 60℃; for 1h; Schlenk technique; Inert atmosphere; | 99% |
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