Dayang Chem (Hangzhou) Co.,Ltd.
DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:88-72-2
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryAntimex Chemical Limied
ProName: High quality O-Nitrotoluene supplier i... CasNo: 88-72-2 Appearance: white-off solid or colorless liquid ( ... Application: Specialty chemical DeliveryTime: Industrial Grade PackAge: 25kgs/fiber drum or 200kgs/UN dru
Cas:88-72-2
Min.Order:500 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquirySimagchem Corporation
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:88-72-2
Min.Order:0 Metric Ton
Negotiable
Type:Manufacturers
inquiryHebei yanxi chemical co.,LTD.
Hebei yanxi chemical co., LTD is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low carb
Cas:88-72-2
Min.Order:1 Kilogram
FOB Price: $1.0 / 3.0
Type:Manufacturers
inquiryHefei TNJ chemical industry co.,ltd
Technology: Technology innovation is our eternal pursuit,or we will be left behind.Our technology experts,all from famous universities and institutes,has rich experience and high achievements in chemical research.This makes sure that our technology
Ality Chemical Corporation
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Wuhan Kemi-Works Chemical Co., Ltd
English name: 2-Nitrotoluene Synonyms:2-Methyl-1-nitrobenzene; 2-Methylnitrobenzene; o-Nitrophenylmethane; 2-Nitrotoluol; alpha-Methylnitrobenz… CAS No. 88-72-2 1.We have been specializing in special fine chemical for long, with strong
Chemwill Asia Co., Ltd.
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Henan Tianfu Chemical Co., Ltd.
Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Henan Sinotech Import&Export Corporation
Product Name: 2-Nitrotoluene Synonyms: O-NITROTOLUENE;o-nitrophenylmethane;1-methyl-2-nitro-benzen;Benzene,1-methyl-2-nitro-;2-NITROTOLUENE,1X1ML, ACN 1000UG/ML;2-NITROTOLUENE OEKANAL, 250 MG;2-NITROTOL
Henan Wentao Chemical Product Co., Ltd.
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Changchun Artel lmport and Export trade company
Price, service, company and transport advantage: 1.place of origin china with super quality by reasonable price. 2. it's customers' right to choose the package (ems, dhl, fedex, ups); 3. it's custo
Hangzhou Keyingchem Co.,Ltd
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Hangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:88-72-2
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHANGZHOU YUNUO CHEMICAL CO.,LTD
superior quality Appearance:light yellow to darker yellow-green liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:As the intermediate of dyes
Zibo Dorne chemical technology co. LTD
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:88-72-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWuhan Fortuna Chemical Co.,Ltd
CAS:88-72-2 EINECS:201-853-3 MW:137.14 MF:C7H7NO2 Melting point:-9 °C Boiling point:225 °C(lit.) Appearance:yellow liquid Package:200kg/Steel drum Transportation:by sea Port:Shanghai
Hangzhou Huarong Pharm Co., Ltd.
Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Hunan chemfish Pharmaceutical co.,Ltd
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
SAGECHEM LIMITED
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Beijing Greenchem Technology Co.,Ltd. ( Panjin Greenchem Technology Co.Ltd .)
Capability on chemical synthesis1. Beijing High-Tech Enterprises2. Strong R&D Team3. 8 years of experiences in R & D of high-tech Catalyst;4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sales;5. The producti
Kono Chem Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
GIHI CHEMICALS CO.,LIMITED
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
Hangzhou Dingyan Chem Co., Ltd
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
Henan Allgreen Chemical Co.,Ltd
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Aecochem Corp.
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Enke Pharma-tech Co.,Ltd. （Cangzhou, China ）
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat
Zhuozhou Wenxi import and Export Co., Ltd
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:88-72-2
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryXiamen AmoyChem Co.,Ltd
Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
Synthetic route
| Conditions | Yield |
|---|---|
| copper(I) oxide In acetonitrile at 50℃; | 100% |
| With [Rh(OH)(cod)]2; 1,3-bis-(diphenylphosphino)propane; water; sodium hydroxide In tetrahydrofuran at 90℃; for 24h; Inert atmosphere; | 81% |
| With potassium carbonate In chloroform at 20℃; for 24h; Irradiation; Inert atmosphere; | 75% |
| With copper diacetate; triethylamine at 35℃; for 21h; Sealed tube; | 26 %Spectr. |
| Multi-step reaction with 2 steps 1.1: sodium hydroxide / water / Inert atmosphere 1.2: 2 h / 110 °C / Inert atmosphere 2.1: sodium acetate / 22 h / 35 °C / Sealed tube View Scheme |
-
-
118310-98-8, 118353-84-7
Benzoic acid (1R,6R)-5-methyl-6-nitro-cyclohex-3-enyl ester
-
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| With potassium tert-butylate In benzene | 95% |
-
-
3958-60-9
2-nitrophenylmethyl bromide
-
A
-
16968-19-7
2,2'-dinitrobibenzyl
-
B
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| With tetraethylammonium perchlorate In acetonitrile controlled-potential electrolysis; further solvent - DMFA.; | A 95% B 2% |
| With diisopropyl phosphite; sodium hydride In tetrahydrofuran for 3h; Ambient temperature; | A 86% B 4% |
| With (C2H5)NClO4 In acetonitrile Mechanism; Rate constant; Product distribution; electrolysis; | |
| With N-ethyl-N,N-diisopropylamine In dichloromethane for 5h; Inert atmosphere; Irradiation; | A 73 %Spectr. B 14 %Spectr. |
-
-
16419-60-6
2-Methylphenylboronic acid
-
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide; [bis(trifluoroacetoxy)iodo]benzene; sodium nitrite In acetonitrile at 20℃; for 3h; regioselective reaction; | 90% |
| With bismuth (III) nitrate pentahydrate In toluene at 70 - 80℃; for 2h; Inert atmosphere; | 90% |
| With 1,1,1,3',3',3'-hexafluoro-propanol; N–nitrosaccharin at 60℃; for 19h; Reagent/catalyst; Inert atmosphere; Schlenk technique; | 82% |
| Conditions | Yield |
|---|---|
| With sulfolane; sodium hydrogencarbonate at 200℃; for 2h; | 90% |
| Conditions | Yield |
|---|---|
| With nickel ammonium sulfate; nitric acid In chloroform; water at 20℃; for 4h; | A 88% B 12% |
| With sodium nitrite for 0.0166667h; Reagent/catalyst; Microwave irradiation; | A 82% B 15% |
| With bismuth(III) nitrate In tetrachloromethane | A 80% B n/a |
| Conditions | Yield |
|---|---|
| With nitric acid In neat (no solvent) at 90℃; for 4h; regioselective reaction; | A 9 %Chromat. B 88% |
| With nitric acid In hexane at 90℃; for 4h; regioselective reaction; | A 63.5 %Chromat. B 36.4 %Chromat. |
-
-
108-88-3
toluene
-
A
-
99-99-0
1-methyl-4-nitrobenzene
-
B
-
88-72-2
1-methyl-2-nitrobenzene
-
C
-
65-85-0
benzoic acid
| Conditions | Yield |
|---|---|
| With methanesulfonic acid; 1-butyl-3-methylimidazolium nitrate In water for 48h; Heating / reflux; | A n/a B n/a C 85% |
| With nitric acid; 1-butyl-3-methylimidazolium nitrate In water for 48h; Heating / reflux; | A n/a B n/a C 85% |
| With nitric acid; 1-n-butyl-3-methylimidazolium methanesulfonate In water for 48h; Heating / reflux; | A n/a B n/a C 70% |
| With nitric acid; 1-n-butyl-3-methylimidazolium methanesulfonate In water for 48h; Heating / reflux; | A n/a B n/a C 70% |
| Conditions | Yield |
|---|---|
| palladium diacetate In tetrahydrofuran at 40℃; for 3h; | 85% |
-
-
594-27-4
tetramethylstannane
-
-
49732-37-8
2-Nitrobenzenediazonium Bisulfate
-
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| palladium diacetate In water; acetonitrile at 20℃; for 2h; | 84% |
| With palladium diacetate In water; acetonitrile at 20℃; for 2h; | 72% |
-
-
103240-13-7
(S)-(o-nitrobenzyl)-6-thioguanine
-
A
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| With hydrogen; platinum(IV) oxide In ethanol under 1551.4 Torr; for 24h; Product distribution; effect of presence of morpholine; | A n/a B 80% |
-
-
108-88-3
toluene
-
A
-
99-08-1
1-methyl-3-nitrobenzene
-
B
-
99-99-0
1-methyl-4-nitrobenzene
-
C
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| With copper(II) nitrate on K10 montmorillonite; acetic anhydride In tetrachloromethane for 120h; Ambient temperature; | A 1% B 79% C 20% |
| With nitric acid In trifluoroacetic acid at 25℃; Rate constant; | A 0.7% B 66.7% C 32.6% |
| With ortho-methylphenyl iodide; potassium nitrate In trifluoroacetic acid for 0.5h; Product distribution; nitration of aromatic compounds in the presence of aryl iodides; other temperatures, other reagents; | A n/a B 64% C 33% |
-
-
190788-59-1
2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)nitrobenzene
-
-
74-88-4
methyl iodide
-
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| With C21H30ClNPPd; potassium tert-butylate In tert-Amyl alcohol at 65℃; for 18h; Sealed tube; Inert atmosphere; Glovebox; | 78% |
-
-
10565-14-7
Diethyl 2-(2-nitrophenyl)propanedioate
-
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| With magnesium chloride In N,N-dimethyl acetamide at 140 - 150℃; for 24h; Decarboxylation; Krapcho's reaction; | 77% |
-
-
1809-20-7
diisopropyl hydrogenphosphonate
-
-
3958-60-9
2-nitrophenylmethyl bromide
-
A
-
16968-19-7
2,2'-dinitrobibenzyl
-
B
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| With sodium hydride In isopropyl alcohol for 3h; Ambient temperature; | A 74% B 18% C 6% |
| Conditions | Yield |
|---|---|
| With sulfuric acid; nitric acid at 70℃; for 2h; | 70% |
| With nitramide; sulfuric acid In water at -15 - -2℃; for 2.25h; | 18% |
| With sulfuric acid; nitric acid at 20℃; |
-
-
17876-76-5
trimethyl(2-nitrobenzyl)silane
-
-
100-52-7
benzaldehyde
-
A
-
88-72-2
1-methyl-2-nitrobenzene
-
B
-
16764-13-9
α-phenyl-2-nitrophenethyl alcohol
| Conditions | Yield |
|---|---|
| With hydrogenchloride; potassium fluoride; 18-crown-6 or silica-supported tetrabutylammonium fluoride In tetrahydrofuran at 20℃; for 12h; Yields of byproduct given; | A n/a B 70% |
-
-
41252-98-6
2-iodo-6-nitrotoluene
-
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| With palladium diacetate; caesium carbonate; triphenylphosphine; benzyl alcohol In 1,2-dimethoxyethane at 90℃; Inert atmosphere; | 70% |
-
-
108-88-3
toluene
-
A
-
99-08-1
1-methyl-3-nitrobenzene
-
B
-
99-99-0
1-methyl-4-nitrobenzene
-
C
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| Product distribution; Ambient temperature; | A 3% B 32% C 65% |
-
-
17876-76-5
trimethyl(2-nitrobenzyl)silane
-
-
100-39-0
benzyl bromide
-
A
-
88-72-2
1-methyl-2-nitrobenzene
-
B
-
6796-01-6
1-nitro-2-phenethylbenzene
| Conditions | Yield |
|---|---|
| With hydrogenchloride; potassium fluoride; 18-crown-6 or silica-supported tetrabutylammonium fluoride In tetrahydrofuran at 20℃; for 12h; Yields of byproduct given; | A n/a B 60% |
| Conditions | Yield |
|---|---|
| (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In 1,4-dioxane for 3h; Heating; | 60% |
-
-
41252-98-6
2-iodo-6-nitrotoluene
-
A
-
88-72-2
1-methyl-2-nitrobenzene
-
B
-
31354-19-5
2,2'-dimethyl-3,3'-dinitrobiphenyl
| Conditions | Yield |
|---|---|
| With copper In N,N-dimethyl-formamide at 190℃; for 24h; | A n/a B 53% |
-
-
108-88-3
toluene
-
A
-
99-99-0
1-methyl-4-nitrobenzene
-
B
-
88-72-2
1-methyl-2-nitrobenzene
-
C
-
121-14-2
2,4-dinitrotoluene
| Conditions | Yield |
|---|---|
| With sulfuric acid; nitric acid at 20℃; for 0.00416667h; | A 37.8% B 52.2% C 4.3% |
| With di-tert-butyl dicarbonate; nitric acid at 4℃; for 50h; Product distribution / selectivity; | A 47% B 45% C 5.5% |
| With butanoic acid anhydride; nitric acid at 50℃; for 4h; |
| Conditions | Yield |
|---|---|
| With tetraethylammonium perchlorate In acetonitrile preparative electrolyse, - 0.89 V; | A 52% B n/a C 18% |
| Conditions | Yield |
|---|---|
| With tetraethylammonium perchlorate In acetonitrile at 20℃; Rate constant; electrolyse, -0.89 V; | A 52% B 18% |
-
-
55289-35-5
2-bromo-6-nitrotoluene
-
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| With 0.60mol% Pd/C; hydrogen; sodium hydrogencarbonate In methanol at 20℃; for 0.583333h; regioselective reaction; | 52% |
-
-
3740-52-1
2-(2-nitrophenyl)acetic acid
-
A
-
88-72-2
1-methyl-2-nitrobenzene
-
B
-
552-89-6
2-nitro-benzaldehyde
| Conditions | Yield |
|---|---|
| With oxygen; copper diacetate In dimethyl sulfoxide at 120℃; for 18h; Sealed tube; | A 52% B 46% |
-
-
1316859-98-9
potassium 2-(2-nitrophenyl)acetate
-
A
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| With bis(η3-allyl-μ-chloropalladium(II)); XPhos In diethylene glycol dimethyl ether at 140℃; for 2h; Inert atmosphere; | A n/a B 52% |
| Conditions | Yield |
|---|---|
| With dihydrogen peroxide; bromine In dichloromethane; water for 4h; Reflux; | 100% |
| Stage #1: 1-methyl-2-nitrobenzene With 2,2'-azobis(isobutyronitrile) In 1,2-dichloro-ethane for 0.333333h; Stage #2: With hydrogen bromide; dihydrogen peroxide In 1,2-dichloro-ethane at 72 - 75℃; for 2h; Solvent; Temperature; | 98.5% |
| With sodium hypochlorite; 2,2'-azobis(isobutyronitrile); hydrogen bromide In chlorobenzene at 85℃; for 7h; Temperature; Solvent; | 97% |
| Conditions | Yield |
|---|---|
| With hydrogen; palladium In methanol at 25℃; under 2327.2 Torr; for 1.5h; | 100% |
| With hydrogen; Pd in AV-17-8-Pd In ethanol at 40℃; | 100% |
| With hydrogen; Pd in AV-17-8-Pd In ethanol at 40℃; under 760 Torr; Rate constant; | 100% |
-
-
88-72-2
1-methyl-2-nitrobenzene
-
-
956-31-0, 51284-68-5, 116723-89-8
N,N'-Di-o-tolyl-diazene N-oxide
| Conditions | Yield |
|---|---|
| With bismuth for 1.5h; | 100% |
| With sodium tetrahydroborate; water In ethanol at 30℃; for 6h; chemoselective reaction; | 92% |
| With oxygen; ammonium chloride; zinc In [bmim][BF4]; water at 20℃; for 18h; | 88% |
| Conditions | Yield |
|---|---|
| Stage #1: 1-methyl-2-nitrobenzene With ammonium formate; palladium on activated charcoal In methanol; water at 20℃; for 4.5h; Stage #2: propyl cyanide In methanol; water | 100% |
| Conditions | Yield |
|---|---|
| Stage #1: 1-methyl-2-nitrobenzene With ammonium formate; palladium on activated charcoal In methanol; water at 20℃; Stage #2: propiononitrile In methanol; water | 100% |
-
-
88-72-2
1-methyl-2-nitrobenzene
-
-
95-92-1
oxalic acid diethyl ester
-
-
3740-52-1
2-(2-nitrophenyl)acetic acid
| Conditions | Yield |
|---|---|
| Stage #1: 1-methyl-2-nitrobenzene; oxalic acid diethyl ester With sodium In ethanol at 20 - 45℃; for 3h; Stage #2: With water In ethanol at 60℃; for 1h; Reagent/catalyst; | 99.8% |
| Stage #1: 1-methyl-2-nitrobenzene; oxalic acid diethyl ester With sodium In ethanol at 45℃; for 3h; Stage #2: With water In ethanol at 60℃; for 1h; | 99.8% |
| Conditions | Yield |
|---|---|
| With sodium hydroxide In water; dimethyl sulfoxide at 50℃; for 1h; Large scale reaction; | 99.5% |
| 64% | |
| With potassium hydroxide In water; dimethyl sulfoxide at 0℃; for 5h; | 46% |
-
-
88-72-2
1-methyl-2-nitrobenzene
-
-
10542-55-9
nitrobenzotrichloride
| Conditions | Yield |
|---|---|
| With chlorine at 120℃; for 6h; Temperature; | 99.2% |
| Conditions | Yield |
|---|---|
| With hydrazine hydrate In ethanol; water; 1,2-dichloro-ethane at 45℃; for 2h; Catalytic behavior; Temperature; | 99% |
| With hydrazine hydrate In ethanol; dichloromethane at 0 - 2℃; for 6h; Solvent; Temperature; | 91.8% |
| With sodium tetrahydroborate; palladium diacetate In ethanol; dichloromethane; water at 20℃; for 0.133333h; | 84% |
| Conditions | Yield |
|---|---|
| Stage #1: 1-methyl-2-nitrobenzene With hydrogen In ethanol at 25℃; under 11172.7 Torr; Flow reactor; Stage #2: With hydrogenchloride In ethanol Flow reactor; chemoselective reaction; | 99% |
| With hydrogenchloride; tin(ll) chloride In ethanol; water at 30℃; Rate constant; Mechanism; various concentration of HCl; different amounts of H2O as solvent; | |
| Stage #1: 1-methyl-2-nitrobenzene With phosgene; sodium tetrahydroborate; copper(II) sulfate In methanol at 20℃; Stage #2: With hydrogenchloride In methanol; diethyl ether | 545 mg |
| Conditions | Yield |
|---|---|
| With bis(acetylacetonato)palladium(II); potassium phosphate tribasic trihydrate; 2-(2,6-diethyl-4-methylphenyl)-5-(2,4,6-triisopropylphenyl)imidazo[1,5-a]pyridin-2-ium chloride In 1,4-dioxane at 130℃; for 24h; Inert atmosphere; | 99% |
-
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| Stage #1: 1-methyl-2-nitrobenzene With chlorosulfonic acid at 115℃; for 4h; Stage #2: With sodium carbonate In water at 20℃; | 98.6% |
-
-
88-72-2
1-methyl-2-nitrobenzene
-
-
4637-24-5
N,N-dimethyl-formamide dimethyl acetal
-
-
32991-03-0
trans-β-dimethylamino-2-nitrostyrene
| Conditions | Yield |
|---|---|
| With copper(l) iodide; N,N-dimethyl-formamide at 180℃; under 6000.6 - 7500.75 Torr; for 2h; microwave irradiation; | 98% |
| In N,N-dimethyl-formamide at 140℃; for 24h; | 88% |
| In N,N-dimethyl-formamide for 26h; Heating; | 86% |
| Conditions | Yield |
|---|---|
| With nitric acid; acetic anhydride at 50℃; for 4h; | 97% |
| bei der Nitrierung; | |
| With Nitroethane; boron trifluoride-dinitrogen tetraoxide |
-
-
76-18-6
2-Chloro-F-propane
-
-
88-72-2
1-methyl-2-nitrobenzene
-
-
238098-38-9
heptafluoroisopropyl-3-methyl-4-nitrobenzene
| Conditions | Yield |
|---|---|
| With hydrogen fluoride; antimony pentafluoride at 80℃; for 2h; Friedel-Crafts Alkylation; Autoclave; Industrial scale; | 97% |
| Conditions | Yield |
|---|---|
| With hydrogen In toluene at 80℃; under 15001.5 Torr; for 18h; Autoclave; | 96% |
| With formic acid; Au/TiO2-R In water at 80℃; under 760.051 Torr; for 9h; Inert atmosphere; Green chemistry; chemoselective reaction; | 91% |
| With hydrogen In methanol at 20℃; under 760.051 Torr; for 6h; | 88% |
| Conditions | Yield |
|---|---|
| With gold nano particles supported on rutile TiO2 In toluene at 70℃; under 750.075 Torr; for 3.5h; Inert atmosphere; chemoselective reaction; | 96% |
| With palladium(II) trifluoroacetate; triphenylphosphine In water at 80℃; for 0.333333h; Sealed tube; Green chemistry; | 80% |
| With palladium particles distributed over the surface of fibrous silica nanospheres modified via aminopropyltriethoxysilane In toluene at 70℃; for 3h; | 96 %Chromat. |
| Conditions | Yield |
|---|---|
| With 2,3,4,5,7,8,9,10-octahydropyrimido[1,2-a]azepin-1-ium acetate In methanol at 60℃; for 3h; Temperature; Solvent; | 95.9% |
-
-
67-56-1
methanol
-
-
88-72-2
1-methyl-2-nitrobenzene
-
-
108-95-2
phenol
-
-
41317-15-1
4-phenylamino-3-methyl-1-methoxybenzene
| Conditions | Yield |
|---|---|
| Stage #1: methanol; 1-methyl-2-nitrobenzene With 3 % platinum on carbon; hydrogen In water at 50℃; under 750.075 Torr; for 8h; Autoclave; Inert atmosphere; Stage #2: phenol With 3 % platinum on carbon In cyclohexanone at 250℃; under 7500.75 Torr; for 2h; Autoclave; Inert atmosphere; | 95.4% |
-
-
88-72-2
1-methyl-2-nitrobenzene
-
-
16968-19-7
2,2'-dinitrobibenzyl
| Conditions | Yield |
|---|---|
| Stage #1: 1-methyl-2-nitrobenzene With potassium tert-butylate In tetrahydrofuran at 0℃; for 0.0333333h; Inert atmosphere; Stage #2: With bromine In tetrahydrofuran at 20℃; for 0.0833333h; Inert atmosphere; | 95% |
| With 5-chloro-1-methyl-1H-pyrazole-4-carbaldehyde; potassium hydroxide In N,N-dimethyl-formamide at 120℃; for 2h; Inert atmosphere; | 88% |
| With sodium; formic acid ethyl ester In hexane at 0 - 5℃; for 24h; | 70.4% |
| Conditions | Yield |
|---|---|
| With ruthenium trichloride; sodium hypochlorite; tetrabutylammomium bromide In 1,2-dichloro-ethane at 25℃; for 2h; Rate constant; pH 9; | 95% |
| With ruthenium trichloride; sodium hypochlorite; tetrabutylammomium bromide In 1,2-dichloro-ethane at 25℃; for 2h; | 95% |
| With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid; sodium bromide at 40℃; for 12h; Temperature; | 94.2% |
-
-
88-72-2
1-methyl-2-nitrobenzene
-
-
4637-24-5
N,N-dimethyl-formamide dimethyl acetal
-
-
20973-67-5
N,N-dimethyl-2-(2-nitrophenyl)ethenylamine
| Conditions | Yield |
|---|---|
| In chloroform; N,N-dimethyl-formamide at 175℃; under 11251.1 Torr; for 2h; Solvent; Temperature; Pressure; | 95% |
| In N,N-dimethyl-formamide at 175℃; under 3750.38 Torr; for 2h; | 91% |
| In N,N-dimethyl-formamide for 26h; Heating; | 86% |
| Conditions | Yield |
|---|---|
| Stage #1: 1-methyl-2-nitrobenzene With sodium tetrahydroborate In water at 60 - 70℃; Green chemistry; Stage #2: acetic anhydride In water at 60 - 70℃; Green chemistry; | 95% |
| Stage #1: 1-methyl-2-nitrobenzene In water for 0.0833333h; Stage #2: With sodium tetrahydroborate In water at 65℃; for 0.05h; Stage #3: acetic anhydride In water at 65℃; for 0.0333333h; Catalytic behavior; | 95% |
| With sodium tetrahydroborate at 60℃; for 0.15h; | 93% |
| With samarium; acetic acid In methanol at 20℃; for 1.5h; | 88% |
| Conditions | Yield |
|---|---|
| With nitric acid; Chloroacetic anhydride at 50℃; for 4h; | A 94% B 5% |
| With dinitrogen pentoxide; H-faujasite zeolite F-712 In dichloromethane | A 77% B 15% |
| With nitric acid at 50℃; for 3h; | A 71.5% B 28.5% |
| Conditions | Yield |
|---|---|
| With nickel-doped graphene carbon nitride nanoparticles; air In ethanol at 25℃; for 8h; Irradiation; Green chemistry; | 94% |
| Stage #1: 1-methyl-2-nitrobenzene With bromine In propan-1-ol at 20℃; for 0.25h; UV-irradiation; Stage #2: With sodium hydrogencarbonate In propan-1-ol for 2h; Solvent; Reflux; UV-irradiation; | 89% |
| With oxygen In acetonitrile at 20℃; for 12h; Irradiation; | 80% |
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