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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

4-Chloro-2-nitrobenzoic acid Manufacturer/High quality/Best price/In stock

Cas:6280-88-2

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 4-Chloro-2-Nitrobenzoic Acid with high purity

Cas:6280-88-2

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 4-chloro-2-nitrobenzoic acid

Cas:6280-88-2

Min.Order:1

Negotiable

Type:Other

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Chemwill Asia Co., Ltd.

Chemwill Asia co.,Ltd is one of the leading manufacturer in CHINA. Product quality, process, price and service 4-Chloro-2-nitrobenzoic acid 6280-88-2 Factory IN STOCK CAS 6280-88-2 6280-88-2 CAS 6280-88-2 highly quality and immedaite delivery

4-Chloro-2-nitrobenzoic acid 6280-88-2 Factory IN STOCK CAS 6280-88-2

Cas:6280-88-2

Min.Order:5 Kiloliter

FOB Price: $3.5 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

TIANFUCHEM--6280-88-2--4-Chloro-2-nitrobenzoic acid in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business

TIANFUCHEM--6280-88-2--4-Chloro-2-nitrobenzoic acid in stock

Cas:6280-88-2

Min.Order:1 Metric Ton

FOB Price: $2000.0

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 6280-88-2 with best quality

Cas:6280-88-2

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Shijiazhuang Sdyano Fine Chemical Co., Ltd

1. Best prices with satisfied quality; 2. It's clients' right to choose the package's Courier (EMS, DHL, FedEx, UPS); 3.It's clients' right to choose the packing way for his produccts from many recent effective packing ways;

4-Chloro-2-nitrobenzoic acid

Cas:6280-88-2

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

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Hubei Langyou International Trading Co., Ltd

1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White Crystalline Powder Storage:Store in sealed conta

high quality 6280-88-2 4-Chloro-2-nitrobenzoic acid with best price

Cas:6280-88-2

Min.Order:10 Gram

Negotiable

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Benzoicacid, 4-chloro-2-nitro- 6280-88-2

Cas:6280-88-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:6280-88-2

Cas:6280-88-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

4-Chloro-2-Nitrobenzoic Acid

Cas:6280-88-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

4-Chloro-2-nitrobenzoic acid

Cas:6280-88-2

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

4-Chloro-2-nitrobenzoic acid

Cas:6280-88-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shaanxi Cuicheng Biomedical Technology Co., Ltd.

Why Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu

4-Chloro-2-nitrobenzoic acid

Cas:6280-88-2

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

Siwei Development Group Ltd.

Product name: 4-Chloro-2-Nitrobenzoic Acid CAS No.: 6280-88-2 Molecule Formula:C7H3ClNO4 Molecule Weight:200.56 Purity: 99.0% Package: 25kg/drum Description:Light yellow crystalline powder Manufacture Standards:Enterprise Standard

Lower Price 4-Chloro-2-Nitrobenzoic Acid

Cas:6280-88-2

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, in

4-Chloro-2-nitrobenzoic acid

Cas:6280-88-2

Min.Order:1 Kilogram

FOB Price: $300.0 / 400.0

Type:Lab/Research institutions

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

4-Chloro-2-nitrobenzoic acid

Cas:6280-88-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Sinotech Import&Export Corporation

Product name: 4-Chloro-2-Nitrobenzoic acid CAS No.: 6280-88-2 Molecular formula: C7H4ClNO4 Molecular weight: 201.56 Structural formula:

4-Chloro-2-Nitrobenzoic acid

Cas:6280-88-2

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

inquiry

Shanghai Minstar Chemical Co., Ltd

4-Chloro-2-nitrobenzoic acid Chemical Properties Melting point 141-143 °C (lit.) Boiling point 160.5°C (rough estimate) density 1.5 refractive index 1.6000 (estimate) Fp >100°C storage temp. Sealed in dry,Room T

4-Chloro-2-nitrobenzoic acid

Cas:6280-88-2

Min.Order:1 Gram

FOB Price: $66.0

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

4-Chloro-2-nitrobenzoic acid

Cas:6280-88-2

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

4-Chloro-2-nitrobenzoic acid

Cas:6280-88-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

4-Chloro-2-nitrobenzoic acid

Cas:6280-88-2

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

4-Chloro-2-nitrobenzoic acid

Cas:6280-88-2

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

4-Chloro-2-nitrobenzoic acid cas no. 6280-88-2 98%

Cas:6280-88-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

4-Chloro-2-nitrobenzoic acid

Cas:6280-88-2

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

4-Chloro-2-nitrobenzoicacid

Cas:6280-88-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier

4-Chloro-2-nitrobenzoic acid

Cas:6280-88-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Fortuna Chemical Co.,Ltd

Best service,high quality and cheap price. Storage:Keep away from heat,sparks and flames. Package:25kg/50kg/200kg drum or Customer demand Application:Used as pharmaceutical intermediates Transportation:BY sea/air or by courier

4-Chloro-2-nitrobenzoic acid

Cas:6280-88-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

4-Chloro-2-nitrobenzoic acid, 97%

Cas:6280-88-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

4-Chloro-2-Nitrobenzoic Acid

Cas:6280-88-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Synthetic route

4-chloro-2-nitrobenzonitrile
34662-32-3

4-chloro-2-nitrobenzonitrile

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
With sulfuric acid
With sulfuric acid
With sulfuric acid
Multi-step reaction with 2 steps
1: sulfuric acid
2: sulfuric acid
View Scheme
4-chloro-2-nitrotoluene
89-59-8

4-chloro-2-nitrotoluene

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
With nitric acid at 200℃;
With pyridine; potassium permanganate; water
With potassium permanganate
4-chloro-1-ethyl-2-nitrobenzene
2001-16-3

4-chloro-1-ethyl-2-nitrobenzene

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
With potassium permanganate
4-chloro-2-nitrobenzoic amide
41994-91-6

4-chloro-2-nitrobenzoic amide

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
With sulfuric acid
4-chloro-2-nitrotoluene
89-59-8

4-chloro-2-nitrotoluene

nitric acid
7697-37-2

nitric acid

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

4-chloro-2-nitrotoluene
89-59-8

4-chloro-2-nitrotoluene

potassium permanganate

potassium permanganate

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

4-Chloro-2-nitroaniline
89-63-4

4-Chloro-2-nitroaniline

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: durch Austausch von NH2 gegen CN nach Sandmeyer
2: concentrated sulfuric acid
View Scheme
Multi-step reaction with 2 steps
2: sulfuric acid
View Scheme
Multi-step reaction with 2 steps
1: copper (II)-sulfate; alkali cyanide; water; sulfuric acid; Wasser / Edukt 4: Natriumnitrit
2: aqueous sulfuric acid
View Scheme
4-chloro(ethylbenzene)
622-98-0

4-chloro(ethylbenzene)

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sulfuric acid; nitric acid
2: KMnO4
View Scheme
1-methyl-2-nitrobenzene
88-72-2

1-methyl-2-nitrobenzene

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: SbCl5; chlorine / <40
2: nitric acid / 200 °C
View Scheme
4-Methyl-3-nitroanilin
119-32-4

4-Methyl-3-nitroanilin

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
2: KMnO4
View Scheme
Multi-step reaction with 2 steps
2: nitric acid / 200 °C
View Scheme
para-chlorobenzoic acid
74-11-3

para-chlorobenzoic acid

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

Conditions
ConditionsYield
With nitric acid In water at 60℃; for 6h; Cooling with ice;
4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

4-chloro-2-nitro-benzoyl chloride
41995-04-4

4-chloro-2-nitro-benzoyl chloride

Conditions
ConditionsYield
With thionyl chloride In toluene for 3h; Heating;100%
With thionyl chloride In DMF (N,N-dimethyl-formamide) at 26 - 65℃; for 5h;100%
With thionyl chloride at 80℃; Inert atmosphere;90%
4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

dimethyl sulfate
77-78-1

dimethyl sulfate

methyl 4-chloro-2-nitrobenzoate
42087-80-9

methyl 4-chloro-2-nitrobenzoate

Conditions
ConditionsYield
With potassium carbonate In acetone for 0.5h; Esterification; Heating;100%
4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

4-chloro-2-nitrobenzoic amide
41994-91-6

4-chloro-2-nitrobenzoic amide

Conditions
ConditionsYield
With ammonium hydroxide; thionyl chloride In dichloromethane; ethyl acetate99%
With ammonium hydroxide; thionyl chloride 1.) PhMe, reflux; Multistep reaction;
Multi-step reaction with 2 steps
1: thionyl chloride / toluene; dimethylformamide / Heating
2: 30 percent aq. NH3 / dioxane / 20 °C
View Scheme
4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

N-cyclohexylglycine t-butyl ester
66937-55-1

N-cyclohexylglycine t-butyl ester

tert-butyl 2-[(4-chloro-2-nitrobenzoyl)cyclohexylamino]acetate

tert-butyl 2-[(4-chloro-2-nitrobenzoyl)cyclohexylamino]acetate

Conditions
ConditionsYield
With triethylamine; HATU In N,N-dimethyl-formamide for 12h;98%
4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

2-chloro-5-bromonitrobenzene
41513-04-6

2-chloro-5-bromonitrobenzene

Conditions
ConditionsYield
With trichloroisocyanuric acid; bromine In tetrachloromethane at 10 - 100℃; for 18h; Photolysis;96%
With copper(l) iodide; oxygen; copper(I) bromide In dimethyl sulfoxide at 160℃; under 760.051 Torr; for 30h; Schlenk technique; Sealed tube;81%
With 2.9-dimethyl-1,10-phenanthroline; oxygen; copper diacetate; silver sulfate; sodium bromide In dimethyl sulfoxide at 160℃; under 760.051 Torr; for 20h; Schlenk technique;64%
tert-butylisonitrile
119072-55-8, 7188-38-7

tert-butylisonitrile

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

4-chlorobenzaldehyde
104-88-1

4-chlorobenzaldehyde

2-(3,4-dimethoxyphenyl)-ethylamine
120-20-7

2-(3,4-dimethoxyphenyl)-ethylamine

N-(2-(tert-butylamino)-1-(4-chlorophenyl)-2-oxoethyl)-4-chloro-N-(3,4-dimethoxyphenethyl)-2-nitrobenzamide

N-(2-(tert-butylamino)-1-(4-chlorophenyl)-2-oxoethyl)-4-chloro-N-(3,4-dimethoxyphenethyl)-2-nitrobenzamide

Conditions
ConditionsYield
In methanol at 20℃; for 24h;95%
tryptamine
61-54-1

tryptamine

tert-butylisonitrile
119072-55-8, 7188-38-7

tert-butylisonitrile

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

4-chlorobenzaldehyde
104-88-1

4-chlorobenzaldehyde

N-(2-(1H-indol-3-yl)ethyl)-N-(2-(tert-butylamino)-1-(4-chlorophenyl)-2-oxoethyl)-4-chloro-2-nitrobenzamide

N-(2-(1H-indol-3-yl)ethyl)-N-(2-(tert-butylamino)-1-(4-chlorophenyl)-2-oxoethyl)-4-chloro-2-nitrobenzamide

Conditions
ConditionsYield
In methanol at 20℃; for 24h;95%
4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

phenethylamine
64-04-0

phenethylamine

4-chloro-2-nitro-N-phenethylbenzamide
284487-93-0

4-chloro-2-nitro-N-phenethylbenzamide

Conditions
ConditionsYield
With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 60℃; for 4h;94%
With pyridine; 2-(1H-9-azabenzotriazol-1-yl)-1,1,3,3-tetramethyluroniumhexafluorophosphate In N,N-dimethyl-formamide for 1h;
4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

N,N-dimethyl-4-chloro-2-nitrobenzamide
2953-58-4

N,N-dimethyl-4-chloro-2-nitrobenzamide

Conditions
ConditionsYield
With trichlorophosphate at 120℃; for 1h; Sealed tube;94%
With trichlorophosphate at 120℃; for 1h;94%
With dipotassium peroxodisulfate; (p-cymene)ruthenium(II) chloride; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene at 160℃; for 24h;37%
With potassium thiosulfate; [RhCl2(p-cymene)]2; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene at 160℃; for 24h; Inert atmosphere; Sealed tube;37%
benzenesulfonamide
98-10-2

benzenesulfonamide

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

N-(2-nitro-4-chloro-benzoyl)-benzenesulfonamide

N-(2-nitro-4-chloro-benzoyl)-benzenesulfonamide

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃;93%
3-quinolylcarboxaldehyde
13669-42-6

3-quinolylcarboxaldehyde

tert-butylisonitrile
119072-55-8, 7188-38-7

tert-butylisonitrile

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

2-(3,4-dimethoxyphenyl)-ethylamine
120-20-7

2-(3,4-dimethoxyphenyl)-ethylamine

N-(2-(tert-butylamino)-2-oxo-1-(quinolin-3-yl)ethyl)-4-chloro-N-(3,4-dimethoxyphenethyl)-2-nitrobenzamide

N-(2-(tert-butylamino)-2-oxo-1-(quinolin-3-yl)ethyl)-4-chloro-N-(3,4-dimethoxyphenethyl)-2-nitrobenzamide

Conditions
ConditionsYield
In methanol at 20℃; for 24h;93%
4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

(4-chloro-2-nitrophenyl)methanol
22996-18-5

(4-chloro-2-nitrophenyl)methanol

Conditions
ConditionsYield
With dimethylsulfide borane complex In tetrahydrofuran at 80℃; for 3h; Inert atmosphere;91%
With dimethylsulfide borane complex In tetrahydrofuran at 80℃; for 3h; Inert atmosphere;52%
With boron dimethyl-trifluoro sulphide In tetrahydrofuran at 0 - 60℃; Inert atmosphere;
With borane-THF In tetrahydrofuran at 0 - 20℃; for 72h;
methanol
67-56-1

methanol

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

methyl 4-chloro-2-nitrobenzoate
42087-80-9

methyl 4-chloro-2-nitrobenzoate

Conditions
ConditionsYield
With thionyl chloride for 6h;90%
With thionyl chloride at 0 - 50℃; for 24h; Inert atmosphere;67%
With sulfuric acid Reflux;
pyridine-2-carbaldehyde
1121-60-4

pyridine-2-carbaldehyde

tert-butylisonitrile
119072-55-8, 7188-38-7

tert-butylisonitrile

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

O-(2-Methoxy-ethyl)-hydroxylamine
54149-39-2

O-(2-Methoxy-ethyl)-hydroxylamine

N-(2-(tert-butylamino)-2-oxo-1-(pyridin-2-yl)ethyl)-4-chloro-N-(2-methoxyethyl)-2-nitrobenzamide

N-(2-(tert-butylamino)-2-oxo-1-(pyridin-2-yl)ethyl)-4-chloro-N-(2-methoxyethyl)-2-nitrobenzamide

Conditions
ConditionsYield
In methanol at 20℃; for 24h;90%
tryptamine
61-54-1

tryptamine

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

4-chloro-N-[2-(1H-indol-3-yl)ethyl]-2-nitrobenzamide
885463-77-4

4-chloro-N-[2-(1H-indol-3-yl)ethyl]-2-nitrobenzamide

Conditions
ConditionsYield
Stage #1: 4-chloro-2-nitro-benzoic acid With benzotriazol-1-ol; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 20℃;
Stage #2: tryptamine In N,N-dimethyl-formamide at 20℃; for 12h;
89%
tert-butylisonitrile
119072-55-8, 7188-38-7

tert-butylisonitrile

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

4-methoxy-benzaldehyde
123-11-5

4-methoxy-benzaldehyde

2,2-dimethoxyethylamine
22483-09-6

2,2-dimethoxyethylamine

N-(2-(tert-butylamino)-1-(4-methoxyphenyl)-2-oxoethyl)-4-chloro-N-(2,2-dimethoxyethyl)-2-nitrobenzamide

N-(2-(tert-butylamino)-1-(4-methoxyphenyl)-2-oxoethyl)-4-chloro-N-(2,2-dimethoxyethyl)-2-nitrobenzamide

Conditions
ConditionsYield
In methanol at 20℃; for 24h;89%
4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

4-chloro-2-nitroiodobenzene
5446-05-9

4-chloro-2-nitroiodobenzene

Conditions
ConditionsYield
With copper(l) iodide; oxygen In dimethyl sulfoxide at 160℃; under 760.051 Torr; for 30h; Reagent/catalyst; Solvent; Schlenk technique; Sealed tube;87%
With 2.9-dimethyl-1,10-phenanthroline; oxygen; copper (I) acetate; silver sulfate; sodium iodide In dimethyl sulfoxide at 160℃; for 24h; Schlenk technique;72%
With 2.9-dimethyl-1,10-phenanthroline; oxygen; copper diacetate; silver sulfate; sodium iodide In dimethyl sulfoxide at 160℃; under 760.051 Torr; for 20h; Schlenk technique;72%
4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

5-bromo-2-chloro-4-(piperazin-1-yl)pyrimidine dihydrochloride

5-bromo-2-chloro-4-(piperazin-1-yl)pyrimidine dihydrochloride

(4-(5-bromo-2-chloropyrimidin-4-yl)piperazin-1-yl)(4-chloro-2-nitrophenyl)methanone

(4-(5-bromo-2-chloropyrimidin-4-yl)piperazin-1-yl)(4-chloro-2-nitrophenyl)methanone

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 0 - 30℃; for 16h;87%
tert-butylisonitrile
119072-55-8, 7188-38-7

tert-butylisonitrile

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

4-methoxy-benzaldehyde
123-11-5

4-methoxy-benzaldehyde

2-(3,4-dimethoxyphenyl)-ethylamine
120-20-7

2-(3,4-dimethoxyphenyl)-ethylamine

N-(2-(tert-butylamino)-1-(4-methoxyphenyl)-2-oxoethyl)-4-chloro-N-(3,4-dimethoxyphenethyl)-2-nitrobenzamide

N-(2-(tert-butylamino)-1-(4-methoxyphenyl)-2-oxoethyl)-4-chloro-N-(3,4-dimethoxyphenethyl)-2-nitrobenzamide

Conditions
ConditionsYield
In methanol at 20℃; for 24h;87%
4-methylphenylglyoxal
1075-47-4

4-methylphenylglyoxal

Cyclohexyl isocyanide
931-53-3

Cyclohexyl isocyanide

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

3-bromopropylamine hydrochloride
5003-71-4

3-bromopropylamine hydrochloride

1-(4-chloro-2-nitrobenzoyl)-N-cyclohexyl-2-(4-methylbenzoyl)pyrrolidine-2-carboxamide

1-(4-chloro-2-nitrobenzoyl)-N-cyclohexyl-2-(4-methylbenzoyl)pyrrolidine-2-carboxamide

Conditions
ConditionsYield
Stage #1: 4-methylphenylglyoxal; Cyclohexyl isocyanide; 4-chloro-2-nitro-benzoic acid; 3-bromopropylamine hydrochloride With sodium hydroxide In methanol at 20℃; for 24h;
Stage #2: With caesium carbonate In methanol at 20℃; for 1h;
87%
Cyclohexyl isocyanide
931-53-3

Cyclohexyl isocyanide

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

3-bromopropylamine hydrochloride
5003-71-4

3-bromopropylamine hydrochloride

p-methoxyphenylglyoxal
1076-95-5

p-methoxyphenylglyoxal

1-(4-chloro-2-nitrobenzoyl)-N-cyclohexyl-2-(4-methoxybenzoyl)pyrrolidine-2-carboxamide

1-(4-chloro-2-nitrobenzoyl)-N-cyclohexyl-2-(4-methoxybenzoyl)pyrrolidine-2-carboxamide

Conditions
ConditionsYield
Stage #1: Cyclohexyl isocyanide; 4-chloro-2-nitro-benzoic acid; 3-bromopropylamine hydrochloride; p-methoxyphenylglyoxal With sodium hydroxide In methanol at 20℃; for 24h;
Stage #2: With caesium carbonate In methanol at 20℃; for 1h;
86%
tert-butylisonitrile
119072-55-8, 7188-38-7

tert-butylisonitrile

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

4-methoxy-benzaldehyde
123-11-5

4-methoxy-benzaldehyde

O-(2-Methoxy-ethyl)-hydroxylamine
54149-39-2

O-(2-Methoxy-ethyl)-hydroxylamine

N-(2-(tert-butylamino)-1-(4-methoxyphenyl)-2-oxoethyl)-4-chloro-N-(2-methoxyethyl)-2-nitrobenzamide

N-(2-(tert-butylamino)-1-(4-methoxyphenyl)-2-oxoethyl)-4-chloro-N-(2-methoxyethyl)-2-nitrobenzamide

Conditions
ConditionsYield
In methanol at 20℃; for 24h;84%
4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

allyl alcohol
107-18-6

allyl alcohol

allyl 4-chloro-2-nitrobenzoate

allyl 4-chloro-2-nitrobenzoate

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; Steglich Esterification;83%
2-methylfuran
534-22-5

2-methylfuran

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

2-methyl-5-(4-chloro-2-nitrophenyl)-furan
1045704-63-9

2-methyl-5-(4-chloro-2-nitrophenyl)-furan

Conditions
ConditionsYield
With palladium(II) trifluoroacetate; triphenylphosphine; silver carbonate In 1,2-dimethoxyethane; dimethyl sulfoxide at 120℃; for 24h; Inert atmosphere; Glovebox;83%
4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

ethyl 1,2,3,4-tetrahydro-β-carboline-3-carboxylate
84518-77-4

ethyl 1,2,3,4-tetrahydro-β-carboline-3-carboxylate

2-(4-Chloro-2-nitro-benzoyl)-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid ethyl ester
130472-81-0

2-(4-Chloro-2-nitro-benzoyl)-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid ethyl ester

Conditions
ConditionsYield
With dicyclohexyl-carbodiimide In dichloromethane for 3h; Ambient temperature;82%
4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

4,4'-dichloro-2,2'-dinitrobiphenyl
56978-50-8

4,4'-dichloro-2,2'-dinitrobiphenyl

Conditions
ConditionsYield
With copper(l) iodide In dimethyl sulfoxide at 140℃; for 20h; Catalytic behavior; Solvent; Reagent/catalyst; Inert atmosphere;82%
With triphenylphosphine; silver carbonate; palladium dichloride In dimethyl sulfoxide at 130℃; for 6h; Inert atmosphere;77%
benzoxazole
273-53-0

benzoxazole

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

2-(4-chloro-2-nitrophenyl)benzo[d]oxazole

2-(4-chloro-2-nitrophenyl)benzo[d]oxazole

Conditions
ConditionsYield
With 1,10-Phenanthroline; caesium carbonate; copper(l) chloride; silver(l) oxide In N,N-dimethyl-formamide at 110℃; for 23h; Inert atmosphere;81%
With 1,10-Phenanthroline; di-tert-butyl peroxide; oxygen; potassium carbonate; copper(I) bromide In toluene at 140℃; for 24.25h; Molecular sieve; Schlenk technique; Sealed tube; regioselective reaction;78%
With bis(tricyclohexylphosphine)nickel(II) dichloride; N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride; silver carbonate; p-benzoquinone at 170℃; for 24h; Sealed tube;72%
4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

thiophenol
108-98-5

thiophenol

4-chloro-2-nitrophenyl phenyl sulfide
4548-56-5

4-chloro-2-nitrophenyl phenyl sulfide

Conditions
ConditionsYield
With copper(l) iodide; 1,10-Phenanthroline; oxygen; potassium carbonate In dimethyl sulfoxide at 140℃; for 24h; Molecular sieve;81%
2-fluoro-5-nitrobenzoic acid
7304-32-7

2-fluoro-5-nitrobenzoic acid

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

C12H6ClFN2O4
1393456-33-1

C12H6ClFN2O4

Conditions
ConditionsYield
With dichloro bis(acetonitrile) palladium(II); silver carbonate; tricyclohexylphosphine In 1,2-dimethoxyethane; dimethyl sulfoxide at 120℃; for 24h; Inert atmosphere;80%
tert-butylisonitrile
119072-55-8, 7188-38-7

tert-butylisonitrile

4-chloro-2-nitro-benzoic acid
6280-88-2

4-chloro-2-nitro-benzoic acid

glycine ethyl ester hydrochloride
5680-79-5

glycine ethyl ester hydrochloride

2-<2-(1,3-dioxolanyl)>benzaldehyde
59259-01-7

2-<2-(1,3-dioxolanyl)>benzaldehyde

4-(2-(tert-butyl)-3-oxo-2,3-dihydroisoquinolin-4-yl)-8-chloro-3,4-dihydro-1H-benzo[e][1,4]diazepine-2,5-dione
1426688-04-1

4-(2-(tert-butyl)-3-oxo-2,3-dihydroisoquinolin-4-yl)-8-chloro-3,4-dihydro-1H-benzo[e][1,4]diazepine-2,5-dione

Conditions
ConditionsYield
Stage #1: tert-butylisonitrile; 4-chloro-2-nitro-benzoic acid; glycine ethyl ester hydrochloride; 2-<2-(1,3-dioxolanyl)>benzaldehyde With sodium carbonate In methanol at 20℃; for 12h; Ugi Condensation; Inert atmosphere;
Stage #2: With perchloric acid In water; acetonitrile at 20℃; for 8h; Inert atmosphere;
Stage #3: With acetic acid; zinc In water; acetonitrile at 60℃; for 8h; Inert atmosphere;
80%

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