Dayang Chem (Hangzhou) Co.,Ltd.
DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:99-08-1
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryHebei yanxi chemical co.,LTD.
Hebei yanxi chemical co., LTD is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low carb
Cas:99-08-1
Min.Order:1 Kilogram
FOB Price: $1.0 / 3.0
Type:Manufacturers
inquiryHefei TNJ chemical industry co.,ltd
Technology: Technology innovation is our eternal pursuit,or we will be left behind.Our technology experts,all from famous universities and institutes,has rich experience and high achievements in chemical research.This makes sure that our technology
Ality Chemical Corporation
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Chemwill Asia Co., Ltd.
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Henan Tianfu Chemical Co., Ltd.
Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Henan Sinotech Import&Export Corporation
roduct Name: 3-Nitrotoluene Synonyms: m-mononitrotoluene;m-nitro-toluen;MNT;nsc9578;Toluene, m-nitro-;toluene,3-nitro-;3-NITROTOLUENE;3-METHYLNITROBENZENE CAS: 99-08-1 MF
Wuhan Kemi-Works Chemical Co., Ltd
Product name: 3-nitrotoluene; m-nitrotoluene CAS No. 99-08-1 Appearance: Yellow orthorhombc cubic crystal. 1.We have been specializing in special fine chemical for long, with strong R&D strength. 2.ISO9001. 3.We have been cooperating wi
Hangzhou Keyingchem Co.,Ltd
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:99-08-1
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryHangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:99-08-1
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryZibo Dorne chemical technology co. LTD
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:99-08-1
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHunan chemfish Pharmaceutical co.,Ltd
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
SAGECHEM LIMITED
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Beijing Greenchem Technology Co.,Ltd. ( Panjin Greenchem Technology Co.Ltd .)
Capability on chemical synthesis1. Beijing High-Tech Enterprises2. Strong R&D Team3. 8 years of experiences in R & D of high-tech Catalyst;4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sales;5. The producti
Kono Chem Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
GIHI CHEMICALS CO.,LIMITED
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
Hangzhou Dingyan Chem Co., Ltd
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
Aecochem Corp.
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Zhuozhou Wenxi import and Export Co., Ltd
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:99-08-1
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryHubei Langyou International Trading Co., Ltd
3-Nitrotoluene CAS. NO.99-08-1 Application:3-Nitrotoluene CAS. NO.99-08-1
Hangzhou ZeErRui Chemical Co., Ltd.
Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an
Cas:99-08-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHunan Longxianng Runhui Trading Co.,Ltd
3-Nitrotoluene CAS. NO.99-08-1Appearance:ask jude for details Storage:Dry and ventilated Package:in foil bag or customized Application:Pharmaceutical intermediates/Food additive Transportation:By express (Door to door) such as FEDEX, DHL, EMS for sma
Cas:99-08-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHunan Russell Chemicals Technology Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
Amadis Chemical Co., Ltd.
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:99-08-1
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryHENAN SUNLAKE ENTERPRISE CORPORATION
Our Services 1.Certificate Of Analysis (COA) 2.Material Safety Data Sheet (MSDS) 3.Route of synthesis (ROS) 4.Method of Aanlysis (MOA) 5.Nuclear Magnetic Resonance (NMR) 6.Packing pictures and loading video before loading 7.Free Sampl
Changzhou Extraordinary Pharmatech co.,LTD
Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa
Zhengzhou Kingorgchem Chemical Technology Co., Ltd.
Zhengzhou Kingorgchem Chemical Technology Co., Ltd. was founded on the basis of Organophosphorus Chemistry Lab of Institute of Chemistry Henan Academy of Sciences in 2015. The laboratory covers 600 m2 and the pilot plant covers 2000 m2. Kingorgchem i
Cas:99-08-1
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryWatson International Ltd
Watson International Ltd' has a very strong R&D and technical capacity supported by FCAD's platform. The subsidiaries under FCAD Group have accumulated much know-how of different fine chemical branches. For example, Apnoke Scientific L
Synthetic route
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate; sodium hydroxide In water at 60℃; for 1.5h; pH=12; Reagent/catalyst; Green chemistry; | 99% |
| With diethylzinc; tetrakis(triphenylphosphine) palladium(0) In hexane; N,N-dimethyl-formamide at 25℃; for 1h; | 63% |
| With lithium aluminium tetrahydride In diethyl ether at 0℃; for 1.5h; | 72 % Turnov. |
-
-
17933-03-8
m-tolylboronic acid
-
-
99-08-1
1-methyl-3-nitrobenzene
| Conditions | Yield |
|---|---|
| With dipotassium peroxodisulfate; bismuth (III) nitrate pentahydrate In toluene at 80℃; for 12h; Inert atmosphere; | 96% |
| With N-Bromosuccinimide; [bis(trifluoroacetoxy)iodo]benzene; sodium nitrite In acetonitrile at 20℃; for 3h; Solvent; regioselective reaction; | 93% |
| With pyridine; copper(I) oxide; sodium nitrite In acetonitrile at 20℃; | 78% |
| Conditions | Yield |
|---|---|
| With 1,9-diperoxynonanedioic acid In acetonitrile at 50℃; for 0.5h; | 95% |
| With dihydrogen peroxide; acetonitrile In aq. buffer at 20℃; for 1h; pH=11; Green chemistry; | 88% |
| With sodium perborate tetrahydrate; cetyltrimethylammonim bromide In water at 60℃; for 12h; silica gel; Micellar solution; Green chemistry; regioselective reaction; | 53% |
| With sulfuric acid Diazotization.Behandlung der neutralisierten Diazoniumsalz-Loesung mit NaNO2 und Kupfer(I)-kupfer(II)-sulfit; | |
| With sulfuric acid Diazotization.Behandlung der neutralisierten Diazoniumsalz-Loesung mit NaNO2, CuSO4 und Cu2O; |
| Conditions | Yield |
|---|---|
| palladium diacetate In tetrahydrofuran at 40℃; for 0.25h; | 90% |
-
-
13506-76-8
2-methyl-6-nitrobenzoic acid
-
-
99-08-1
1-methyl-3-nitrobenzene
| Conditions | Yield |
|---|---|
| With silver carbonate In dimethyl sulfoxide at 120℃; for 16h; | 86% |
| With silver carbonate In dimethyl sulfoxide at 120℃; | |
| Multi-step reaction with 3 steps 1.1: sodium hydroxide / tetrahydrofuran; water / 0.17 h / Darkness 1.2: 0.08 h / Darkness 2.1: acetonitrile / 0.08 h / Darkness 3.1: water / d7-N,N-dimethylformamide / 2 h / 100 °C / Inert atmosphere; Glovebox; Sealed tube; Darkness View Scheme |
| Conditions | Yield |
|---|---|
| With nitric acid; sodium dodecyl-sulfate In acetonitrile at 24.84℃; for 3h; Micellar solution; regioselective reaction; | 85% |
-
-
27329-27-7
4-methyl-2-nitrobenzoic acid
-
-
99-08-1
1-methyl-3-nitrobenzene
| Conditions | Yield |
|---|---|
| With copper(l) iodide; triethylamine In dimethyl sulfoxide at 120℃; under 760.051 Torr; for 20h; Inert atmosphere; Schlenk technique; | 85% |
| With 1-methyl-pyrrolidin-2-one; quinoline; copper(I) oxide; 1,10-Phenanthroline at 100 - 175℃; for 0.5h; Inert atmosphere; Microwave irradiation; | 50% |
| Multi-step reaction with 3 steps 1: tetrahydrofuran / 2 h / 20 °C / Darkness 2: tetrahydrofuran / Darkness 3: water / d7-N,N-dimethylformamide / 0.83 h / 100 °C / Inert atmosphere; Glovebox; Sealed tube; Darkness View Scheme |
| Conditions | Yield |
|---|---|
| With copper; tetrabutylammonium nitrite; N,N`-dimethylethylenediamine In N,N-dimethyl-formamide at 110℃; for 0.333333h; Inert atmosphere; Microwave irradiation; | 84% |
| With copper bronze; tetrabutylammonium nitrate; N,N`-dimethylethylenediamine In N,N-dimethyl-formamide at 100℃; | 69% |
| With potassium nitrite; copper(II) bis(trifluoromethanesulfonate) In dimethyl sulfoxide at 130℃; for 48h; Inert atmosphere; Sealed tube; regioselective reaction; | 67% |
| Conditions | Yield |
|---|---|
| With dichloro bis(1,4-diazabicyclo[2.2.2]octane)(BH4)Zr(IV); toluene-4-sulfonic acid In sulfolane; N,N-dimethyl-formamide at 110℃; for 7.2h; | 83% |
| Conditions | Yield |
|---|---|
| With palladium diacetate In water at 60 - 70℃; for 4h; | 80% |
| palladium diacetate In water at 60℃; for 4h; | 80 % Chromat. |
-
-
108-88-3
toluene
-
A
-
99-08-1
1-methyl-3-nitrobenzene
-
B
-
99-99-0
1-methyl-4-nitrobenzene
-
C
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| With copper(II) nitrate on K10 montmorillonite; acetic anhydride In tetrachloromethane for 120h; Ambient temperature; | A 1% B 79% C 20% |
| With nitric acid In trifluoroacetic acid at 25℃; Rate constant; | A 0.7% B 66.7% C 32.6% |
| With ortho-methylphenyl iodide; potassium nitrate In trifluoroacetic acid for 0.5h; Product distribution; nitration of aromatic compounds in the presence of aryl iodides; other temperatures, other reagents; | A n/a B 64% C 33% |
| Conditions | Yield |
|---|---|
| With palladium diacetate In N,N-dimethyl-formamide at 60 - 70℃; for 2.5h; | 77% |
| palladium diacetate In N,N-dimethyl-formamide at 60℃; for 2h; | 77 % Chromat. |
| Conditions | Yield |
|---|---|
| With palladium diacetate In N,N-dimethyl-formamide at 60 - 70℃; for 2.5h; | 77% |
| palladium diacetate In N,N-dimethyl-formamide at 60℃; for 2.5h; | 77 % Chromat. |
| Conditions | Yield |
|---|---|
| With [Au(1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene)(O2CAd)] In toluene at 140℃; for 20h; | 71% |
-
-
1809-20-7
diisopropyl hydrogenphosphonate
-
-
3958-57-4
1-bromomethyl-3-nitrobenzene
-
A
-
99-08-1
1-methyl-3-nitrobenzene
| Conditions | Yield |
|---|---|
| With sodium hydride In isopropyl alcohol for 3h; Ambient temperature; | A 21% B 69% |
-
-
108-88-3
toluene
-
A
-
99-08-1
1-methyl-3-nitrobenzene
-
B
-
99-99-0
1-methyl-4-nitrobenzene
-
C
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| Product distribution; Ambient temperature; | A 3% B 32% C 65% |
-
-
594-27-4
tetramethylstannane
-
-
1514-51-8
m-nitrobenzenediazonium hexafluorophosphate
-
-
99-08-1
1-methyl-3-nitrobenzene
| Conditions | Yield |
|---|---|
| palladium diacetate In acetonitrile for 2h; Ambient temperature; | 62% |
-
-
66146-33-6
2-(3-nitrophenyl)acetaldehyde
-
A
-
99-08-1
1-methyl-3-nitrobenzene
-
B
-
99-61-6
3-nitro-benzaldehyde
-
C
-
19829-61-9
3,3'-dinitrobibenzyl
| Conditions | Yield |
|---|---|
| In water; acetonitrile for 48h; Product distribution; Irradiation; | A 60% B 40% C n/a |
-
-
638-03-9
m-toluidine hydrochloride
-
A
-
99-08-1
1-methyl-3-nitrobenzene
-
B
-
13290-74-9
1-chloro-2-methyl-4-nitrobenzene
| Conditions | Yield |
|---|---|
| With 3,3-dimethyldioxirane In acetone at 20℃; | A 45% B 55% |
-
-
5326-38-5
2-iodo-5-nitrotoluene
-
A
-
99-08-1
1-methyl-3-nitrobenzene
-
B
-
59517-20-3
2,2'-dimethyl-4,4'-dinitro-biphenyl
| Conditions | Yield |
|---|---|
| With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 12h; Catalytic behavior; Ullmann Condensation; Inert atmosphere; Green chemistry; | A 10% B 55% |
-
-
3958-57-4
1-bromomethyl-3-nitrobenzene
-
A
-
99-08-1
1-methyl-3-nitrobenzene
-
B
-
19829-61-9
3,3'-dinitrobibenzyl
| Conditions | Yield |
|---|---|
| With diisopropyl phosphite; sodium hydride In tetrahydrofuran for 3h; Ambient temperature; | A 5% B 28% C 52% |
-
-
108-88-3
toluene
-
A
-
99-08-1
1-methyl-3-nitrobenzene
-
B
-
99-99-0
1-methyl-4-nitrobenzene
-
C
-
88-72-2
1-methyl-2-nitrobenzene
-
D
-
121-14-2
2,4-dinitrotoluene
| Conditions | Yield |
|---|---|
| With trinitratooxovanadium(V) In dichloromethane for 0.05h; Ambient temperature; Further byproducts given; | A 3% B 47% C 50% D n/a |
| With trinitratooxovanadium(V) In dichloromethane for 0.1h; Ambient temperature; Further byproducts given; | A 2% B 41% C 35% D 19% |
| Conditions | Yield |
|---|---|
| With tert.-butylhydroperoxide; ammonium iodide; water In dimethyl sulfoxide at 90℃; for 4h; Sealed tube; | 38% |
-
-
108-88-3
toluene
-
A
-
99-08-1
1-methyl-3-nitrobenzene
-
B
-
99-99-0
1-methyl-4-nitrobenzene
-
C
-
88-72-2
1-methyl-2-nitrobenzene
-
D
-
100-52-7
benzaldehyde
| Conditions | Yield |
|---|---|
| With ammonium cerium(IV) nitrate In water; trifluoroacetic acid for 72h; Ambient temperature; Yield given; | A n/a B n/a C n/a D 24.5% |
| With nitric acid at 90 - 100℃; for 4h; Product distribution; Further Variations:; Temperatures; Reagents; | |
| With nitrogen dioxide at 70℃; for 6h; Reagent/catalyst; Autoclave; Green chemistry; |
-
-
13238-16-9
dibenzylphosphine oxide
-
-
3958-57-4
1-bromomethyl-3-nitrobenzene
-
A
-
99-08-1
1-methyl-3-nitrobenzene
-
B
-
19829-61-9
3,3'-dinitrobibenzyl
| Conditions | Yield |
|---|---|
| With sodium hydride 1.) THF, 2.) THF, RT, 3 h; Yield given. Multistep reaction; | A 2% B 21% C n/a |
| Conditions | Yield |
|---|---|
| at 170℃; im geschlossenen Rohr; |
-
-
2229-07-4
methyl radical
-
-
98-95-3
nitrobenzene
-
A
-
99-08-1
1-methyl-3-nitrobenzene
-
B
-
99-99-0
1-methyl-4-nitrobenzene
-
C
-
88-72-2
1-methyl-2-nitrobenzene
| Conditions | Yield |
|---|---|
| at 143℃; |
| Conditions | Yield |
|---|---|
| With hydrogenchloride Diazotization.Behandlung der Diazoniumsalz-Loesung mit wss.-alkal. Natriumstannit-Loesung bei -10grad; | |
| Diazotization.Erwaermen des Diazoniumsulfats mit Alkohol; | |
| With formamide; triethylamine; trifluoroacetic acid; sodium nitrite 1.) formamide/water, r.t.; 2.) water, r.t.; Yield given. Multistep reaction; |
| Conditions | Yield |
|---|---|
| durch Entamidierung; | |
| With hydrogenchloride Diazotization.Behandlung der Diazoniumsalz-Loesung mit H3PO2; | |
| Diazotization.Kochen des Diazoniumsulfats mit absol. Alkohol; |
| Conditions | Yield |
|---|---|
| With laccase from Coriolus versicolor MTCC-138; 2,2'-azino-bis(3-ethylbenzothiazoline-6-sulfonic acid) diammonium salt In 1,4-dioxane for 1h; pH=4.5; Green chemistry; Enzymatic reaction; | 100% |
| With laccase at 20℃; Reagent/catalyst; Green chemistry; Enzymatic reaction; | 100% |
| With laccase of Pleurotus ostreatus MTCC-1801; 2,2'-azino-bis(3-ethylbenzothiazoline-6-sulfonic acid) diammonium salt In 1,4-dioxane at 20℃; pH=4.5; Enzymatic reaction; | 98% |
| Conditions | Yield |
|---|---|
| With [1-butyl-2,3-dimethylimidazolium][tppm] stabilized rhodium nanoarticles at 50℃; under 22502.3 Torr; for 5h; Ionic liquid; Autoclave; chemoselective reaction; | 100% |
| With cadmium sulphide; ammonium formate In water at 20℃; for 14h; Inert atmosphere; Irradiation; Sealed tube; | 100% |
| With water; oxalic acid; titanium(IV) oxide for 3h; Wavelength; Irradiation; Inert atmosphere; Sealed tube; Green chemistry; chemoselective reaction; | 100% |
-
-
109-74-0
propyl cyanide
-
-
99-08-1
1-methyl-3-nitrobenzene
-
A
-
60995-75-7
N-butyl-m-toluidine
-
B
-
74878-72-1
N-butyl-N-(3-methyl-n-propyl)-m-toluidine
| Conditions | Yield |
|---|---|
| Stage #1: 1-methyl-3-nitrobenzene With ammonium formate; palladium on activated charcoal In methanol; water at 20℃; Stage #2: propyl cyanide In methanol; water | A 100% B n/a |
| Conditions | Yield |
|---|---|
| With ammonium formate; palladium on activated charcoal In water; isopropyl alcohol at 20℃; for 1h; | 100% |
-
-
99-08-1
1-methyl-3-nitrobenzene
-
-
110-13-4
2,5-hexanedione
-
-
32570-10-8
N-(3′-methylphenyl)-2,5-dimethylpyrrole
| Conditions | Yield |
|---|---|
| With formic acid for 12h; Autoclave; Inert atmosphere; Green chemistry; | 100% |
| With indium; acetic acid In toluene at 80℃; for 3h; Inert atmosphere; | 97% |
| Conditions | Yield |
|---|---|
| Stage #1: 1-methyl-3-nitrobenzene With hydrogen In ethanol at 25℃; under 11172.7 Torr; Flow reactor; Stage #2: With hydrogenchloride In ethanol Flow reactor; chemoselective reaction; | 99% |
| With hydrogenchloride; tin(ll) chloride In ethanol; water at 30℃; Rate constant; Mechanism; various concentration of HCl; | |
| Stage #1: 1-methyl-3-nitrobenzene With phosgene; sodium tetrahydroborate; copper(II) sulfate In methanol at 20℃; Stage #2: With hydrogenchloride In methanol; diethyl ether | 550 mg |
| Conditions | Yield |
|---|---|
| With indium; acetic acid In methanol at 20℃; for 1h; | 99% |
| Stage #1: 1-methyl-3-nitrobenzene With sodium tetrahydroborate In water at 60 - 70℃; Green chemistry; Stage #2: acetic anhydride In water at 60 - 70℃; Green chemistry; | 94% |
| Stage #1: 1-methyl-3-nitrobenzene In water for 0.0833333h; Stage #2: With sodium tetrahydroborate In water at 65℃; for 0.05h; Stage #3: acetic anhydride In water at 65℃; for 0.0333333h; Catalytic behavior; | 93% |
-
-
14040-11-0
tungsten hexacarbonyl
-
-
99-08-1
1-methyl-3-nitrobenzene
-
-
616-38-6
carbonic acid dimethyl ester
-
-
537-92-8
3-Methylacetanilide
| Conditions | Yield |
|---|---|
| With di(rhodium)tetracarbonyl dichloride; 1,3-bis-(diphenylphosphino)propane; sodium phosphate; sodium iodide In water at 120℃; for 24h; Inert atmosphere; Sealed tube; | 99% |
| Conditions | Yield |
|---|---|
| With 1,3-bis(N',N'-dimethyl-4-aminopyridinium)propane diiodide; sodium hydride In N,N-dimethyl-formamide; paraffin oil at 20℃; for 0.25h; Inert atmosphere; | 98% |
| With potassium hydroxide In water; isopropyl alcohol at 35℃; under 760.051 Torr; for 8h; Inert atmosphere; | 95% |
| With Piperonyl butoxide; ammonium formate In methanol for 1.25h; Heating; | 94% |
-
-
99-08-1
1-methyl-3-nitrobenzene
-
-
21871-44-3
5-(3-nitrophenyl)-1H-tetrazole
| Conditions | Yield |
|---|---|
| With sodium azide; hydroxylamine hydrochloride In water at 20℃; for 4.16667h; | 97% |
-
-
451-40-1
phenyl benzyl ketone
-
-
99-08-1
1-methyl-3-nitrobenzene
-
-
123848-41-9
2-(3-methylphenyl)-1,2-diphenylethanone
| Conditions | Yield |
|---|---|
| With potassium phosphate; bis(acetylacetonato)palladium(II); dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine In cyclohexane at 130℃; for 24h; Inert atmosphere; | 97% |
| Conditions | Yield |
|---|---|
| With gold nano particles supported on rutile TiO2 In toluene at 70℃; under 750.075 Torr; for 3h; Inert atmosphere; chemoselective reaction; | 96% |
| With cobalt nanoparticles anchoring on nitrogen doped carbon, pyrolysis at 700 °C In acetonitrile at 110℃; under 750.075 Torr; for 5h; Inert atmosphere; chemoselective reaction; | 96.2% |
| With palladium(II) trifluoroacetate; triphenylphosphine In water at 80℃; for 0.333333h; Sealed tube; Green chemistry; | 92% |
| With [PdCl4]2-ion-exchanged imidazolium IL containing triethylene glycol-tagged onto silica-coated iron oxide nanoparticles In water at 90℃; for 24h; Inert atmosphere; Green chemistry; | |
| With palladium particles distributed over the surface of fibrous silica nanospheres modified via aminopropyltriethoxysilane In toluene at 70℃; for 3h; | 98 %Chromat. |
| Conditions | Yield |
|---|---|
| With methyldiazene In acetonitrile at 28℃; for 1.33333h; Irradiation; Sealed tube; Inert atmosphere; | 95% |
| With sodium tetrahydroborate; palladium diacetate In ethanol; dichloromethane; water at 20℃; for 0.0833333h; | 88% |
| With rhodium contaminated with carbon; hydrazine hydrate In tetrahydrofuran at 0 - 20℃; for 3h; | 85% |
-
-
99-08-1
1-methyl-3-nitrobenzene
-
A
-
108-44-1
1-amino-3-methylbenzene
-
B
-
621-26-1
3,3'-dimethylhydrazobenzene
| Conditions | Yield |
|---|---|
| With potassium hydroxide; aluminium In methanol at 20℃; for 0.25h; Reduction; Reductive coupling; | A 3% B 95% |
| Conditions | Yield |
|---|---|
| With hydrogen In toluene at 140℃; under 30003 Torr; for 3h; chemoselective reaction; | 95% |
-
-
99-08-1
1-methyl-3-nitrobenzene
-
-
19618-06-5, 71297-97-7, 116723-90-1
3,3'-dimethylazoxybenzene
| Conditions | Yield |
|---|---|
| With oxygen; ammonium chloride; zinc In [bmim][BF4]; water at 20℃; for 16h; | 94% |
| With potassium hydroxide In methanol; toluene for 24h; Heating; | 90% |
| Stage #1: 1-methyl-3-nitrobenzene With sodium tetrahydroborate; palladium diacetate In ethanol; dichloromethane; water at 20℃; Stage #2: With oxygen In ethanol; dichloromethane; water | 90% |
-
-
99-08-1
1-methyl-3-nitrobenzene
-
-
16712-16-6, 64165-14-6, 65387-22-6, 70179-79-2, 540-69-2
ammonium formate
-
-
3085-53-8
N-formyl-m-toluidine
| Conditions | Yield |
|---|---|
| With cobalt nanoparticles coated by N,P-codoped carbon shell pyrolyzed at 800°C In tetrahydrofuran at 120℃; for 12h; Schlenk technique; Inert atmosphere; | 94% |
| With zinc for 0.05h; microwave irradiation; | 80% |
-
-
99-08-1
1-methyl-3-nitrobenzene
-
-
583-05-1
1-phenylpentane-1,4-dione
-
-
357988-79-5
2-methyl-5-phenyl-1-m-tolyl-1H-pyrrole
| Conditions | Yield |
|---|---|
| With indium; acetic acid In toluene for 0.5h; Inert atmosphere; Reflux; | 94% |
| Conditions | Yield |
|---|---|
| With ruthenium trichloride; sodium hypochlorite; tetrabutylammomium bromide In 1,2-dichloro-ethane at 25℃; for 2h; | 93% |
| With chromium(VI) oxide; periodic acid In acetonitrile at 20℃; for 1h; | 93% |
| With oxygen; acetic acid; 1N,3N,5N-trihydroxy-1,3,5-triazin-2,4,6[1H,3H,5H]-trione; cobalt(II) acetate; manganese(II) acetate at 100℃; under 760 Torr; for 14h; | 88% |
-
-
99-08-1
1-methyl-3-nitrobenzene
-
-
51437-67-3
trans-3,3'-dimethylazobenzene
| Conditions | Yield |
|---|---|
| With ammonium acetate; lead In methanol at 20℃; | 93% |
| With isopropyl alcohol; sodium hydroxide at 30℃; for 2h; Catalytic behavior; Inert atmosphere; UV-irradiation; | 88% |
| With ethanolamine; potassium hydroxide at 55℃; for 1h; Sonication; Microwave irradiation; | 88% |
| Conditions | Yield |
|---|---|
| With formic acid; Au/TiO2-R In water at 80℃; under 760.051 Torr; for 4h; Inert atmosphere; Green chemistry; chemoselective reaction; | 93% |
| With hydrogen In ethanol at 120℃; under 15001.5 Torr; for 8.5h; Autoclave; | 87% |
| Stage #1: 1-methyl-3-nitrobenzene With triethylsilane; palladium In methanol at 20℃; under 760.051 Torr; for 2h; Stage #2: benzaldehyde In methanol | 70% |
| Conditions | Yield |
|---|---|
| With potassium tert-butylate at 130℃; for 24h; Sealed tube; | 93% |
| With [(N,N′-bis(diisopropylphosphino)-2,6-diaminopyridine)Mn(CO)3][Br]; potassium hydroxide at 110℃; for 16h; Molecular sieve; Sealed tube; | 80% |
| With [Ru(2-(6-methoxypyridin-2-yl)-1,10-phenanthroline)(MeCN)2Cl]Cl; sodium methylate at 110℃; for 12h; Green chemistry; | 87 %Chromat. |
| With platinum on carbon; potassium tert-butylate; hydrogen at 150℃; under 1500.15 Torr; for 24h; Autoclave; | 93 %Chromat. |
-
-
99-08-1
1-methyl-3-nitrobenzene
-
-
1160967-80-5
2,2,2-trifluoro-N-(2-iodophenyl)acetimidoyl chloride
-
-
13939-06-5, 199620-15-0
molybdenum hexacarbonyl
| Conditions | Yield |
|---|---|
| With 1,3-bis-(diphenylphosphino)propane; sodium carbonate; palladium dichloride In 1,4-dioxane at 120℃; for 24h; Inert atmosphere; Sealed tube; | 93% |
| Conditions | Yield |
|---|---|
| With N-acetoxyphthalimide; cobalt(II) acetate; manganese(II) acetate In acetic acid at 130℃; under 7600 Torr; for 14h; | A 5% B 92% |
| With Coprinus sp. peroxidase; tartaric acid buffer; dihydrogen peroxide In water; acetone at 20℃; pH=5; |
| Conditions | Yield |
|---|---|
| With samarium diiodide In tetrahydrofuran at 20℃; for 0.5h; | 92% |
| Conditions | Yield |
|---|---|
| With palladium diacetate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1-methyl-pyrrolidin-2-one at 150℃; for 24h; Inert atmosphere; Sealed vessel; | 92% |
| With N/O-doped porous carbon (on base of polypyrrole) supported nanopalladium at 80℃; Inert atmosphere; | 70% |
-
-
99-08-1
1-methyl-3-nitrobenzene
-
A
-
588-04-5
3,3'-dimethylazobenzene
-
B
-
19618-06-5, 71297-97-7, 116723-90-1
3,3'-dimethylazoxybenzene
| Conditions | Yield |
|---|---|
| With sodium hydroxide; sodium tetrahydroborate; diphenyl ditelluride In ethanol for 20h; Heating; | A 90% B 10% |
| With sodium tetrahydroborate; water In ethanol at 30℃; for 3h; chemoselective reaction; | A n/a B 78% |
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