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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our advantage: 1: High quality and Competitive price 2: Quality control, GC&HPLC&NMR or as your requested 3: Packing as your requested, and double check before shipment 4: Prompt shipment with professional documents 5: Excellent after-
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:Powder Storage:Store in sealed containers at cool & dry pla
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inquiry7-Bromoindole CAS:51417-51-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediat
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcing and qua
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:51417-51-7
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:51417-51-7
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inquiry7-bromoindoleAppearance:Pls see the Details Storage:Keep away of light, hot, water, Store in dry, dark and ventilated place Package:according to customers' requirements Application:Steroids, Cosmetics Ingredients, APIs, Intermediates, OLED&Battery In
7-BROMO-1H-INDOLE; 7-BROMOINDOLE; RARECHEM AH BS 0083; 7-Bromoindole 98%; 7-Bromoindole, 97%; 3-CYANO-7-CHLORO INDOLE; 7-BROMOCHROMANONE; 7-broMo-4H-indole CAS No: 51417-51-7 Molecular formula: C8H6BrN Molecular weight: 196.04 7-bromoin
Product name: 7-Bromoindole CAS No.:51417-51-7 Molecule Formula:C8H6BrN Molecule Weight:196.04 Purity: 96.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS SPEC
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inquiry1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea
Cas:51417-51-7
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inquiryProduct Name: 7-Bromoindole Synonyms: 7-BROMO-1H-INDOLE;7-BROMOINDOLE;RARECHEM AH BS 0083;7-Bromoindole,97%;3-CYANO-7-CHLORO INDOLE;7-Bromoindole98%;7-BROMOCHROMANONE;7-broMo-4H-indole CAS: 51417-51-7
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Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Shanghai Finebiotech Co.,Ltd.was established in 2020, which providing professional chemical services. As a customer-oriented company, we have distinguished ourself from others in providing worldwide customers with cost-effective and efficient service
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiry7-bromo-N-(4-toluenesulfonyl)-1H-indole
7-bromo-1H-indole
Conditions | Yield |
---|---|
With formic acid; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 24h; Inert atmosphere; Sealed tube; Irradiation; | 87% |
1-(2-amino-3-bromophenyl)-2-chloroethan-1-one
7-bromo-1H-indole
Conditions | Yield |
---|---|
With sodium tetrahydroborate In 1,4-dioxane; water for 1h; Heating; | 84% |
7-bromo-1H-indole
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol; dimethyl sulfoxide at 90℃; for 5h; Sealed tube; Inert atmosphere; | 79% |
(2-Bromo-6-trimethylsilanylethynyl-phenyl)-carbamic acid tert-butyl ester
7-bromo-1H-indole
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol for 2h; Heating; | 77% |
7-bromoisatin
7-bromo-1H-indole
Conditions | Yield |
---|---|
With potassium borohydride; dimethyl sulfate In toluene at -10 - -5℃; Inert atmosphere; | 74% |
With borane-THF In tetrahydrofuran at 0 - 20℃; for 48h; | 32% |
7-bromo-2,3-dihydroindole
7-bromo-1H-indole
Conditions | Yield |
---|---|
With salcomine; oxygen In methanol at 20℃; for 3h; | 73% |
With salcomine In methanol for 11h; Ambient temperature; | 72% |
With oxygen In N,N-dimethyl acetamide at 20℃; Schlenk technique; Irradiation; | 41% |
Conditions | Yield |
---|---|
In tetrahydrofuran at -45 - -40℃; for 25h; | 72% |
In tetrahydrofuran at -45℃; for 0.583333h; | 72% |
Stage #1: 2-nitrophenyl bromide; vinyl magnesium bromide In tetrahydrofuran at -40 - 0℃; for 2.5h; Inert atmosphere; Stage #2: With hydrogenchloride; pivalaldehyde In tetrahydrofuran; water at 0℃; for 72h; Inert atmosphere; | 70% |
(S)-7-bromo-tryptophan
7-bromo-1H-indole
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; tryptophanase TnaA at 25℃; pH=7.4; Enzymatic reaction; | 63.2% |
2-nitrophenyl bromide
vinyl magnesium bromide
A
2-oxoindole
B
7-bromo-1H-indole
Conditions | Yield |
---|---|
In tetrahydrofuran at -40℃; | A 30% B 62% |
Conditions | Yield |
---|---|
In tetrahydrofuran at -70℃; for 3h; Cycloaddition; | 53% |
7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)-1H-indole
7-bromo-1H-indole
Conditions | Yield |
---|---|
With copper(ll) bromide In methanol; water at 80℃; for 4h; | 40% |
[(E)-2-(3-Bromo-2-nitro-phenyl)-vinyl]-dimethyl-amine
7-bromo-1H-indole
Conditions | Yield |
---|---|
With zinc In acetic acid at 85℃; for 2h; | 29% |
7-bromo-1H-indole-2-carboxylic acid
7-bromo-1H-indole
Conditions | Yield |
---|---|
With quinoline; copper(I) bromide at 250℃; |
2,6-dibromoaniline
tributyl-((Z)-2-ethoxy-vinyl)-stannane
7-bromo-1H-indole
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; tetraethylammonium chloride; oxalic acid 1.) MeCN, reflux, 4 h, 2.) MeCN, reflux, 3 h; Multistep reaction; |
7-bromo-N-formylindoline
7-bromo-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 94 percent / aq. NaOH / methanol / 0.5 h / 75 °C 2: 73 percent / salcomine; O2 / methanol / 3 h / 20 °C View Scheme |
1-indoline
7-bromo-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: 94 percent / EDCI; pyridine / 24 h / 20 °C 2.1: trifluoroacetic acid; thallium trifluoroacetate / 11 h / 20 °C 2.2: 73 percent / CuBr2 / dimethylformamide / 2 h / 135 °C 3.1: 94 percent / aq. NaOH / methanol / 0.5 h / 75 °C 4.1: 73 percent / salcomine; O2 / methanol / 3 h / 20 °C View Scheme |
N-formylindoline
7-bromo-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: trifluoroacetic acid; thallium trifluoroacetate / 11 h / 20 °C 1.2: 73 percent / CuBr2 / dimethylformamide / 2 h / 135 °C 2.1: 94 percent / aq. NaOH / methanol / 0.5 h / 75 °C 3.1: 73 percent / salcomine; O2 / methanol / 3 h / 20 °C View Scheme |
2-iodophenylamine
7-bromo-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 86 percent / tetrahydrofuran / 114 h / Heating 2: 95 percent / triethylamine, Pd(PPh3)2Cl2, CuI / 0.25 h / Ambient temperature 3: 1.) tert-butyllithium, 2.) 1,2-dibromoethane / 1.) Et2O, pentane, -20 deg C, 3 h, 2.) Et2O, pentane, -100 deg C to r.t., overnight 4: 77 percent / sodium ethoxide / ethanol / 2 h / Heating View Scheme |
2-bromo-N-(tert-butoxycarbonyl)aniline
7-bromo-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 50 percent / triethylamine, Pd(PPh3)2Cl2, CuI / 13 h / 100 °C 2: 1.) tert-butyllithium, 2.) 1,2-dibromoethane / 1.) Et2O, pentane, -20 deg C, 3 h, 2.) Et2O, pentane, -100 deg C to r.t., overnight 3: 77 percent / sodium ethoxide / ethanol / 2 h / Heating View Scheme |
tert-butyl 2-iodophenylcarbamate
7-bromo-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 95 percent / triethylamine, Pd(PPh3)2Cl2, CuI / 0.25 h / Ambient temperature 2: 1.) tert-butyllithium, 2.) 1,2-dibromoethane / 1.) Et2O, pentane, -20 deg C, 3 h, 2.) Et2O, pentane, -100 deg C to r.t., overnight 3: 77 percent / sodium ethoxide / ethanol / 2 h / Heating View Scheme |
2-bromoaniline
7-bromo-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 89 percent / tetrahydrofuran / 91 h / Heating 2: 50 percent / triethylamine, Pd(PPh3)2Cl2, CuI / 13 h / 100 °C 3: 1.) tert-butyllithium, 2.) 1,2-dibromoethane / 1.) Et2O, pentane, -20 deg C, 3 h, 2.) Et2O, pentane, -100 deg C to r.t., overnight 4: 77 percent / sodium ethoxide / ethanol / 2 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: 1.) BCl4, AlCl3, 2.) 2 N HCl / 1.) C6H6, CH2Cl2, reflux, 3 h, 2.) C6H6, CH2Cl2, 80 deg C, 45 min 2: 84 percent / NaBH4 / dioxane; H2O / 1 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1.1: hydroxylamine hydrochloride; hydrogenchloride; sodium sulfate / water / 0.08 h / 20 °C 1.2: 4.25 h / 20 - 90 °C 2.1: sulfuric acid / 0.5 h / 50 - 65 °C 3.1: borane-THF / tetrahydrofuran / 48 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 4 steps 1: hydrogenchloride / water 2: sodium sulfate; hydroxylamine hydrochloride / water / 3 h / 35 - 85 °C 3: sulfuric acid / 0.08 h / 60 - 80 °C 4: potassium borohydride; dimethyl sulfate / toluene / -10 - -5 °C / Inert atmosphere View Scheme |
2-((trimethylsilyl)ethynyl)phenylaminocarboxylic acid tert-butyl ester
7-bromo-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) tert-butyllithium, 2.) 1,2-dibromoethane / 1.) Et2O, pentane, -20 deg C, 3 h, 2.) Et2O, pentane, -100 deg C to r.t., overnight 2: 77 percent / sodium ethoxide / ethanol / 2 h / Heating View Scheme |
1-Acetyl-2,3-dihydro-1H-indole
7-bromo-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.) thallium tris-trifluoroacetate (TTFA); 2.) CuBr2 / 1.) TFA, room temp., 3 h; 2.) DMF, room temp., 3 h 2: 96 percent / NaOH (40percent) / H2O; methanol / 0.5 h / Heating 3: 72 percent / salcomine / methanol / 11 h / Ambient temperature View Scheme |
1-acetyl-2,3-dihydro-7-bromoindole
7-bromo-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 96 percent / NaOH (40percent) / H2O; methanol / 0.5 h / Heating 2: 72 percent / salcomine / methanol / 11 h / Ambient temperature View Scheme |
1-acetyl-2,3-dihydro-7-iodoindole
7-bromo-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 14 percent / Et3N / Pd(OAc)2 / dimethylformamide / 0.5 h / 115 °C 2: 1.) thallium tris-trifluoroacetate (TTFA); 2.) CuBr2 / 1.) TFA, room temp., 3 h; 2.) DMF, room temp., 3 h 3: 96 percent / NaOH (40percent) / H2O; methanol / 0.5 h / Heating 4: 72 percent / salcomine / methanol / 11 h / Ambient temperature View Scheme | |
Multi-step reaction with 4 steps 1: 14 percent / Et3N, methyl acrylate / Pd(OAc)2 / dimethylformamide / 0.5 h / 115 °C 2: 1.) thallium tris-trifluoroacetate (TTFA); 2.) CuBr2 / 1.) TFA, room temp., 3 h; 2.) DMF, room temp., 3 h 3: 96 percent / NaOH (40percent) / H2O; methanol / 0.5 h / Heating 4: 72 percent / salcomine / methanol / 11 h / Ambient temperature View Scheme |
1-bromo-3-methyl-2-nitro-benzene
7-bromo-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: pyrrolidine / dimethylformamide / 110 °C 2: 29 percent / Zn / acetic acid / 2 h / 85 °C View Scheme |
ethyl 7-bromo-1H-indole-2-carboxylate
7-bromo-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ethanolic alkaline solution 2: copper (I)-bromide; quinoline / 250 °C View Scheme |
7-bromo-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ethanolic H2SO4 2: polyphosphoric acid 3: ethanolic alkaline solution 4: copper (I)-bromide; quinoline / 250 °C View Scheme |
7-bromo-1H-indole
o-fluorophenylboronic acid
7-(2-FLUOROPHENYL)-1H-INDOLE
Conditions | Yield |
---|---|
With sodium carbonate; lithium chloride; tetrakis(triphenylphosphine) palladium(0) In 1,2-dimethoxyethane at 75℃; for 12h; | 100% |
7-bromo-1H-indole
di-tert-butyl dicarbonate
Conditions | Yield |
---|---|
With dmap In acetonitrile at 20℃; for 72h; | 100% |
With dmap; triethylamine In dichloromethane at 20℃; for 16h; | 90% |
With dmap; triethylamine In dichloromethane at 0℃; for 0.666667h; Inert atmosphere; | 90% |
With dmap In acetonitrile for 1h; | 38% |
With dmap; N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃; |
7-bromo-1H-indole
3,4-(methylenedioxy)-benzeneboronic acid
7-(3,4-methylenedioxyphenyl)indole
Conditions | Yield |
---|---|
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; toluene for 96h; Heating; | 99% |
7-bromo-1H-indole
carbon monoxide
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; bis(benzonitrile)palladium(II) dichloride; triethylamine In toluene at 130℃; under 18751.5 Torr; for 20h; | 99% |
Conditions | Yield |
---|---|
Stage #1: 7-bromo-1H-indole With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.75h; Stage #2: isopropyl bromide In N,N-dimethyl-formamide for 18h; | 99% |
With potassium hydroxide In N,N-dimethyl-formamide at 20℃; for 2h; |
Conditions | Yield |
---|---|
With [2-(2-aminoethyl)phenyl]-chloro-palladium di-tert-butyl-[2-(2,4,6-triisopropylphenyl)phenyl]phosphane; sodium t-butanolate In tetrahydrofuran at 85℃; for 12h; Inert atmosphere; | 98.79% |
Conditions | Yield |
---|---|
Stage #1: 7-bromo-1H-indole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 0.5h; Stage #2: benzyl bromide In N,N-dimethyl-formamide; mineral oil at 20℃; for 0.0833333h; | 98% |
With potassium hydroxide In N,N-dimethyl-formamide at 20℃; | 88% |
With sodium hydride In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 67.9% |
Conditions | Yield |
---|---|
With caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 In tetrahydrofuran for 12h; Suzuki-Miyaura cross-coupling; Heating; | 97% |
9-hydroxyxanthene
7-bromo-1H-indole
6-bromo-3-(9H-xanthen-9-yl)-1H-indole
Conditions | Yield |
---|---|
With 1,3-dichloro-1,1,3,3-tetrabutylstannoxane In dichloromethane at 20℃; for 10h; | 97% |
7-bromo-1H-indole
benzalacetophenone
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In acetonitrile at 50℃; for 24h; Schlenk technique; Inert atmosphere; Sealed tube; | 97% |
7-bromo-1H-indole
(2-trimethylethylsilylethoxy)methyl chloride
7-bromo-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-indole
Conditions | Yield |
---|---|
Stage #1: 7-bromo-1H-indole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 1h; Stage #2: (2-trimethylethylsilylethoxy)methyl chloride In N,N-dimethyl-formamide at 0℃; for 3h; | 96% |
Stage #1: 7-bromo-1H-indole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 1h; Stage #2: (2-trimethylethylsilylethoxy)methyl chloride In N,N-dimethyl-formamide at 0℃; for 3h; | 96% |
Stage #1: 7-bromo-1H-indole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: (2-trimethylethylsilylethoxy)methyl chloride In N,N-dimethyl-formamide at 15℃; for 20h; | 72.7% |
Conditions | Yield |
---|---|
In acetonitrile at 70℃; for 0.5h; | 95% |
Conditions | Yield |
---|---|
With cobalt(II) tetrafluoroborate hexahydrate; tris(2-diphenylphosphinoethyl)phosphine; potassium carbonate at 100℃; for 24h; Autoclave; Glovebox; Inert atmosphere; | 95% |
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; potassium tert-butylate at 140℃; for 17h; | 85% |
With trimethylamine-N-oxide; tricarbonyl(η4-1,3-bis(trimethylsilyl)-4,5,6,7-tetrahydro-2H-inden-2-one)iron; potassium carbonate at 80℃; for 24h; | 82% |
7-bromo-1H-indole
benzaldehyde
3,3’-(phenylmethylene)bis(7-bromo-1H-indole)
Conditions | Yield |
---|---|
With 1,3-bis(mesityl)imidazolium chloride In dichloromethane at 20℃; for 1h; Schlenk technique; | 95% |
7-bromo-1H-indole
N,N-dimethyl-formamide
7-bromo-1 H-indole-3-carbaldehyde
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl-formamide With trichlorophosphate at 0℃; for 0.666667h; Stage #2: 7-bromo-1H-indole at 0 - 20℃; for 5.5h; | 94% |
With trichlorophosphate | 93% |
With trichlorophosphate at 0 - 20℃; for 6h; Vilsmeier-Haack reaction; | 89% |
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; bis(benzonitrile)palladium(II) dichloride; triethylamine In toluene at 130℃; under 18751.5 Torr; for 20h; | 94% |
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; bis(benzonitrile)palladium(II) dichloride; triethylamine In toluene at 130℃; under 18751.5 Torr; for 20h; | 94% |
Conditions | Yield |
---|---|
With triethylsilane; trichloroacetic acid In toluene at 70℃; | 94% |
7-bromo-1H-indole
1-bromomethyl-3-trifluoromethylbenzene
7-bromo-1-[3-(trifluoromethyl)benzyl]-1H-indole
Conditions | Yield |
---|---|
Stage #1: 7-bromo-1H-indole With potassium hydroxide In dimethyl sulfoxide for 0.5h; Stage #2: 1-bromomethyl-3-trifluoromethylbenzene In dimethyl sulfoxide | 94% |
7-bromo-1H-indole
methyl 3-hydroxy-1H-indole-2-carboxylate
methyl-2-(7-bromo-1H-indol-3-yl)-3-oxoindoline-2-carboxylate
Conditions | Yield |
---|---|
With C44H58CuN2O2; oxygen In 1,2-dichloro-ethane at 50℃; for 22h; Sealed tube; Inert atmosphere; | 94% |
With ammonium cerium (IV) nitrate; sodium hydrogencarbonate In acetonitrile at 0 - 20℃; | 66% |
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; manganese; nickel(II) bromide 2-methoxyethyl ether complex; zirconium(IV) chloride In N,N-dimethyl acetamide at 20 - 35℃; | 94% |
7-bromo-1H-indole
3,7-dibromoindole
Conditions | Yield |
---|---|
With pyridinium hydrobromide perbromide In pyridine at 0℃; | 93% |
7-bromo-1H-indole
3,4-Dimethoxyphenylboronic acid
7-(3,4-Dimethoxy-phenyl)-1H-indole
Conditions | Yield |
---|---|
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; toluene for 96h; Heating; | 93% |
7-bromo-1H-indole
acetyl chloride
1-(7-bromo-1H-indol-3-yl)ethan-1-one
Conditions | Yield |
---|---|
Stage #1: 7-bromo-1H-indole With diethylaluminium chloride In dichloromethane at 0℃; for 0.416667h; Stage #2: acetyl chloride In dichloromethane at 0℃; for 1 - 3h; | 93% |
With tin(IV) chloride In toluene | 90% |
Stage #1: 7-bromo-1H-indole With diethylaluminium chloride In hexane; dichloromethane at 0℃; for 0.5h; Inert atmosphere; Stage #2: acetyl chloride In hexane; dichloromethane at 0℃; Inert atmosphere; | |
Stage #1: 7-bromo-1H-indole; acetyl chloride In toluene at 0℃; for 0.166667h; Stage #2: With tin(IV) chloride In toluene for 12h; | |
With tin(IV) chloride In toluene at 0 - 20℃; for 2h; |
Conditions | Yield |
---|---|
With bismuth(lll) trifluoromethanesulfonate In methanol; acetonitrile at 80℃; for 24h; | 93% |
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; potassium hydroxide at 20℃; | 93% |
7-bromo-1H-indole
indole
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In toluene at 110℃; for 12h; | 92% |
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; cesium acetate; isopropyl alcohol at 100℃; Schlenk technique; Inert atmosphere; | 65% |
Conditions | Yield |
---|---|
Stage #1: 7-bromo-1H-indole With sodium hydride In tetrahydrofuran; mineral oil at 0 - 20℃; for 1.75h; Inert atmosphere; Stage #2: methyl iodide In tetrahydrofuran; mineral oil at 0 - 20℃; Inert atmosphere; | 92% |
Stage #1: 7-bromo-1H-indole With sodium hydride In tetrahydrofuran; mineral oil at 0 - 20℃; for 0.5h; Stage #2: methyl iodide In tetrahydrofuran; mineral oil at 20℃; for 0.0833333h; | 85% |
Stage #1: 7-bromo-1H-indole With sodium hydride In tetrahydrofuran at 0℃; for 1h; Stage #2: methyl iodide In tetrahydrofuran | 85% |
Conditions | Yield |
---|---|
With phosphomolybdic acid In ethylenediamine at 60℃; for 1h; | 92% |
7-bromo-1H-indole
5-Hydroxy-2-pentanone
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate In 1,2-dichloro-ethane at 40℃; | 92% |
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