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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

4-Fluoro-3-nitrophenyl azide Identification of 28166-06-5 Name: 4-Fluoro-3-nitrophenyl azide (Related Reference) EINECS: 248-878-6 Molecular Formula: C6H3 F N4 O2 CAS Registry Number: 28166-06-5 Synonyms:

28166-06-5 4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

4-FLUORO-3-NITROPHENYL AZIDE CAS:28166-06-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality orga

4-FLUORO-3-NITROPHENYL AZIDE CAS:28166-06-5

Cas:28166-06-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:0

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

3-Nitro-4-fluorophenylazide

Cas:28166-06-5

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Best Offer4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:0

Negotiable

Type:Trading Company

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TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

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Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

3-Nitro-4-fluorophenylazide

Cas:28166-06-5

Min.Order:0

Negotiable

Type:Manufacturers

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Golden Pharma Co., Limited

GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:1 Kilogram

Negotiable

Type:Other

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HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:colourless or light yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceu

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:1 Gram

Negotiable

Type:Trading Company

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:0

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Type:Lab/Research institutions

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Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:0

Negotiable

Type:Manufacturers

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Wuhan Circle Star Chem-medical Technology co.,Ltd.

1,we produce and sell good chemicals around the world.2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%.3,our staff consists of highly qualified in

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:0

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SAGECHEM LIMITED

3-Nitro-4-fluorophenylazide 28166-06-5 Application:3-Nitro-4-fluorophenylazide 28166-06-5

3-Nitro-4-fluorophenylazide

Cas:28166-06-5

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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DB BIOTECH CO., LTD

best seller Application:API

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:0

Negotiable

Type:Trading Company

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BOC Sciences

We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:clear oily liquid Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as prim

4-FLUORO-3-NITROPHENYL AZIDE

Cas:28166-06-5

Min.Order:0

Negotiable

Type:Trading Company

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Hangzhou Fandachem Co.,Ltd

4-Fluoro-3-nitrophenyl azide cas 28166-06-5Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

4-Fluoro-3-nitrophenyl azide cas 28166-06-5

Cas:28166-06-5

Min.Order:0

Negotiable

Type:Other

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Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers2. Produce products of different specifications and sizes according to your requirements.3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures sta

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:0

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Type:Lab/Research institutions

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Hebei Muhuang Technology Co., Ltd

best seller Application:API

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:0

Negotiable

Type:Trading Company

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Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

3-Nitro-4-fluorophenylazide 28166-06-5

Cas:28166-06-5

Min.Order:0

Negotiable

Type:Trading Company

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Shenzhen Foris Technology Co. LTD

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

3-Nitro-4-fluorophenylazide 28166-06-5

Cas:28166-06-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:0

Negotiable

Type:Trading Company

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Toda Biotechnology Co., Limited.

Todachem specialize in exporting chemicals for 10 years, we manufacture and distribute high quality pharmaceutical APIs, intermediates, special chemicals, active molecule and other fine chemicals. We have our research laboratory and more than 100 n

Factory direct supply 4-Fluoro-3-nitrophenyl azide with best quality

Cas:28166-06-5

Min.Order:1 Kilogram

FOB Price: $90.0 / 100.0

Type:Trading Company

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HuBei Ipure Biotech CO.,ltd

HuBei ipure is a diversified product production and operation enterprise, with API, pharma intermediates, and other fine chemicals as well as R&D and pigments development and sales as one of the large enterprises, with more than 130 acres of pl

3-Nitro-4-fluorophenylazide

Cas:28166-06-5

Min.Order:1 Gram

FOB Price: $1.0

Type:Trading Company

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Shanghai united Scientific Co.,Ltd.

United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Shanghai AngewChem Co., Ltd.

Shanghai AngewChemCo., Ltd. is an innovative enterprise on fine chemicals and pharmaceuticals. Based on Shanghai R&D center and Hunan chemical manufacturing plant, we offer chemical research, process development, and large-scale production. Complete

4-Fluoro-3-nitrophenyl azide

Cas:28166-06-5

Min.Order:0

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Synthetic route

4-Fluoro-3-nitroaniline
364-76-1

4-Fluoro-3-nitroaniline

4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

Conditions
ConditionsYield
Stage #1: 4-Fluoro-3-nitroaniline With hydrogenchloride; sodium nitrite In water at 70℃;
Stage #2: With sodium azide In water at 70℃;
98%
With sodium azide; tert.-butylnitrite In tert-butyl alcohol at 20℃; for 1h;92%
Stage #1: 4-Fluoro-3-nitroaniline With hydrogenchloride; sodium nitrite In water at 0℃; for 0.25h;
Stage #2: With sodium azide In water at 20℃; for 0.5h;
75%
Stage #1: 4-Fluoro-3-nitroaniline With hydrogenchloride; sodium nitrite In water at 5℃; for 0.5h; Cooling with ice;
Stage #2: With sodium azide In water at 0℃;
73%
(i) aq. H2SO4, NaNO2, (ii) aq. NaN3; Multistep reaction;
sodium azide

sodium azide

4-Fluoro-3-nitroaniline
364-76-1

4-Fluoro-3-nitroaniline

4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

Conditions
ConditionsYield
Stage #1: 4-Fluoro-3-nitroaniline With hydrogenchloride; sodium nitrite In water at 0℃; for 0.166667h;
Stage #2: sodium azide In water at 0℃; for 4.25h;
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

(1R,2R,3S,4R,5S)-4-(2-chloro-6-(prop-2-ynylamino)-9H-purin-9-yl)bicyclo[3.1.0]hexane-2,3-diol
1309943-98-3

(1R,2R,3S,4R,5S)-4-(2-chloro-6-(prop-2-ynylamino)-9H-purin-9-yl)bicyclo[3.1.0]hexane-2,3-diol

(1R,2R,3S,4R,5S)-4-(2-chloro-6-((1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)methylamino)-9H-purin-9-yl)bicyclo[3.1.0]hexane-2,3-diol
1309943-99-4

(1R,2R,3S,4R,5S)-4-(2-chloro-6-((1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)methylamino)-9H-purin-9-yl)bicyclo[3.1.0]hexane-2,3-diol

Conditions
ConditionsYield
With copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine In water; tert-butyl alcohol at 20℃;96%
With sodium ascorbate; copper(II) sulfate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine In dichloromethane; water; tert-butyl alcohol at 20℃; Inert atmosphere;96%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

(1S,2R,3S,4R,5S)-4-[2-chloro-6-(3-(nona-1,8-diynyl)phenylmethylamino)-9H-purin-9-yl]-2,3-dihydroxybicyclo[3.1.0]hexane-1-carboxylic acid N-methylamide
1309943-74-5

(1S,2R,3S,4R,5S)-4-[2-chloro-6-(3-(nona-1,8-diynyl)phenylmethylamino)-9H-purin-9-yl]-2,3-dihydroxybicyclo[3.1.0]hexane-1-carboxylic acid N-methylamide

(1S,2R,3S,4R,5S)-4-[2-chloro-6-(3-(7-(1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)hept-1-ynyl)benzylamino)-9H-purin-9-yl]-2,3-dihydroxybicyclo[3.1.0]hexane-1-carboxylic acid N-methylamide
1309943-77-8

(1S,2R,3S,4R,5S)-4-[2-chloro-6-(3-(7-(1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)hept-1-ynyl)benzylamino)-9H-purin-9-yl]-2,3-dihydroxybicyclo[3.1.0]hexane-1-carboxylic acid N-methylamide

Conditions
ConditionsYield
With sodium ascorbate; copper(II) sulfate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine In dichloromethane; water; tert-butyl alcohol at 20℃; Inert atmosphere;96%
thiobenzoic acid
98-91-9

thiobenzoic acid

4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

N-(4-fluoro-3-nitrophenyl)-benzylamide
228425-41-0

N-(4-fluoro-3-nitrophenyl)-benzylamide

Conditions
ConditionsYield
With 2,6-dimethylpyridine In methanol at 25℃; for 15h;95%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

(1R,2R,3S,4R,5S)-4-(2-chloro-6-(3-(octa-1,7-diynyl)benzylamino)-9H-purin-9-yl)bicyclo[3.1.0]hexane-2,3-diol
1309943-87-0

(1R,2R,3S,4R,5S)-4-(2-chloro-6-(3-(octa-1,7-diynyl)benzylamino)-9H-purin-9-yl)bicyclo[3.1.0]hexane-2,3-diol

(1R,2R,3S,4R,5S)-4-(2-chloro-6-(3-(6-(1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)hex-1-ynyl)benzylamino)-9H-purin-9-yl)bicyclo[3.1.0]hexane-2,3-diol
1309943-90-5

(1R,2R,3S,4R,5S)-4-(2-chloro-6-(3-(6-(1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)hex-1-ynyl)benzylamino)-9H-purin-9-yl)bicyclo[3.1.0]hexane-2,3-diol

Conditions
ConditionsYield
With sodium ascorbate; copper(II) sulfate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine In dichloromethane; water; tert-butyl alcohol at 20℃; Inert atmosphere;95%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

thioacetic acid
507-09-5

thioacetic acid

N-(4-fluoro-3-nitrophenyl)acetamide
351-32-6

N-(4-fluoro-3-nitrophenyl)acetamide

Conditions
ConditionsYield
With 2,6-dimethylpyridine In methanol at 25℃; for 15h;94%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

(1'S,2'R,3'S,4'R,5'S)-4'-[6-(3-chlorobenzylamino)-2-(1,7-octadiynyl)-9H-purin-9-yl]-2',3'-dihydroxybicyclo[3.1.0]hexane-1'-carboxylic acid N-methylamide
1213770-15-0

(1'S,2'R,3'S,4'R,5'S)-4'-[6-(3-chlorobenzylamino)-2-(1,7-octadiynyl)-9H-purin-9-yl]-2',3'-dihydroxybicyclo[3.1.0]hexane-1'-carboxylic acid N-methylamide

MRS5223
1217299-58-5

MRS5223

Conditions
ConditionsYield
With copper(II) sulphate hydrate; sodium L-ascorbate In tetrahydrofuran; water at 20℃; regioselective reaction;94%
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In tetrahydrofuran; water at 20℃;94%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

(1S,2R,3S,4R,5S)-4-[2-chloro-6-(3-(octa-1,7-diynyl)phenylmethylamino)-9H-purin-9-yl]-2,3-dihydroxybicyclo[3.1.0]hexane-1-carboxylic acid N-methylamide
1309944-05-5

(1S,2R,3S,4R,5S)-4-[2-chloro-6-(3-(octa-1,7-diynyl)phenylmethylamino)-9H-purin-9-yl]-2,3-dihydroxybicyclo[3.1.0]hexane-1-carboxylic acid N-methylamide

(1S,2R,3S,4R,5S)-4-[2-chloro-6-(3-(6-(1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)hex-1-ynyl)benzylamino)-9H-purin-9-yl]-2,3-dihydroxybicyclo[3.1.0]hexane-1-carboxylic acid N-methylamide
1309943-76-7

(1S,2R,3S,4R,5S)-4-[2-chloro-6-(3-(6-(1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)hex-1-ynyl)benzylamino)-9H-purin-9-yl]-2,3-dihydroxybicyclo[3.1.0]hexane-1-carboxylic acid N-methylamide

Conditions
ConditionsYield
With sodium ascorbate; copper(II) sulfate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine In dichloromethane; water; tert-butyl alcohol at 20℃; Inert atmosphere;94%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

(1S,2R,3S,4R,5S)-4-(2-chloro-6-(prop-2-ynylamino)-9H-purin-9-yl)-2,3-dihydroxy-N-methylbicyclo[3.1.0]hexane-1-carboxamide
1309943-94-9

(1S,2R,3S,4R,5S)-4-(2-chloro-6-(prop-2-ynylamino)-9H-purin-9-yl)-2,3-dihydroxy-N-methylbicyclo[3.1.0]hexane-1-carboxamide

(1S,2R,3S,4R,5S)-4-(2-chloro-6-((1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)methylamino)-9H-purin-9-yl)-2,3-dihydroxy-N-methylbicyclo[3.1.0]hexane-1-carboxamide
1309943-95-0

(1S,2R,3S,4R,5S)-4-(2-chloro-6-((1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)methylamino)-9H-purin-9-yl)-2,3-dihydroxy-N-methylbicyclo[3.1.0]hexane-1-carboxamide

Conditions
ConditionsYield
With copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine In water; tert-butyl alcohol at 20℃;92%
With sodium ascorbate; copper(II) sulfate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine In dichloromethane; water; tert-butyl alcohol at 20℃; Inert atmosphere;92%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

17α-aminomethyl-3,3-(dimethoxy)-5α-androstan-17β-ol
300350-92-9

17α-aminomethyl-3,3-(dimethoxy)-5α-androstan-17β-ol

17α-[(N-4-azido-2-nitrophenyl)aminomethyl]-3,3-dimethoxy-5α-androstan-17β-ol
300351-06-8

17α-[(N-4-azido-2-nitrophenyl)aminomethyl]-3,3-dimethoxy-5α-androstan-17β-ol

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran; diethyl ether; ethanol91%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

(1R,2R,3S,4R,5S)-4-(2-chloro-6-(3-(hepta-1,6-diynyl)benzylamino)-9H-purin-9-yl)bicyclo[3.1.0]hexane-2,3-diol
1309943-86-9

(1R,2R,3S,4R,5S)-4-(2-chloro-6-(3-(hepta-1,6-diynyl)benzylamino)-9H-purin-9-yl)bicyclo[3.1.0]hexane-2,3-diol

(1R,2R,3S,4R,5S)-4-(2-chloro-6-(3-(5-(1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)pent-1-ynyl)benzylamino)-9H-purin-9-yl)bicyclo[3.1.0]hexane-2,3-diol
1309943-89-2

(1R,2R,3S,4R,5S)-4-(2-chloro-6-(3-(5-(1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)pent-1-ynyl)benzylamino)-9H-purin-9-yl)bicyclo[3.1.0]hexane-2,3-diol

Conditions
ConditionsYield
With copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine In dichloromethane; water; tert-butyl alcohol at 20℃;91%
With sodium ascorbate; copper(II) sulfate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine In dichloromethane; water; tert-butyl alcohol at 20℃; Inert atmosphere;91%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

(1R,2R,3S,4R,5S)-4-(2-chloro-6-(3-(nona-1,8-diynyl)benzylamino)-9H-purin-9-yl)bicyclo[3.1.0]hexane-2,3-diol
1309943-88-1

(1R,2R,3S,4R,5S)-4-(2-chloro-6-(3-(nona-1,8-diynyl)benzylamino)-9H-purin-9-yl)bicyclo[3.1.0]hexane-2,3-diol

(1R,2R,3S,4R,5S)-4-(2-chloro-6-(3-(7-(1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)hept-1-ynyl)benzylamino)-9H-purin-9-yl)bicyclo[3.1.0]hexane-2,3-diol
1309943-91-6

(1R,2R,3S,4R,5S)-4-(2-chloro-6-(3-(7-(1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)hept-1-ynyl)benzylamino)-9H-purin-9-yl)bicyclo[3.1.0]hexane-2,3-diol

Conditions
ConditionsYield
With sodium ascorbate; copper(II) sulfate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine In dichloromethane; water; tert-butyl alcohol at 20℃; Inert atmosphere;91%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

(1S,2R,3S,4R,5S)-4-[2-chloro-6-(3-(hepta-1,6-diynyl)phenylmethylamino)-9H-purin-9-yl]-2,3-dihydroxybicyclo[3.1.0]hexane-1-carboxylic acid N-methylamide
1309944-03-3

(1S,2R,3S,4R,5S)-4-[2-chloro-6-(3-(hepta-1,6-diynyl)phenylmethylamino)-9H-purin-9-yl]-2,3-dihydroxybicyclo[3.1.0]hexane-1-carboxylic acid N-methylamide

(1S,2R,3S,4R,5S)-4-[2-chloro-6-(3-(5-(1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)pent-1-ynyl)benzylamino)-9H-purin-9-yl]-2,3-dihydroxybicyclo[3.1.0]hexane-1-carboxylic acid N-methylamide
1309943-75-6

(1S,2R,3S,4R,5S)-4-[2-chloro-6-(3-(5-(1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)pent-1-ynyl)benzylamino)-9H-purin-9-yl]-2,3-dihydroxybicyclo[3.1.0]hexane-1-carboxylic acid N-methylamide

Conditions
ConditionsYield
With copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine In dichloromethane; water; tert-butyl alcohol at 20℃;90%
With sodium ascorbate; copper(II) sulfate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine In dichloromethane; water; tert-butyl alcohol at 20℃; Inert atmosphere;90%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

ethylenediamine
107-15-3

ethylenediamine

4-(2-aminoethyl)amino-3-nitro-phenylazide (napa)
64309-07-5

4-(2-aminoethyl)amino-3-nitro-phenylazide (napa)

Conditions
ConditionsYield
In dichloromethane for 24h; Ambient temperature;89%
In dichloromethane for 0.5h; Ambient temperature; in the dark;70%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

(1'S,2'R,3'S,4'R,5'S)-4'-[6-(3-chlorobenzylamino)-2-(1,6-heptadiynyl)-9H-purin-9-yl]-2',3'-dihydroxybicyclo[3.1.0]hexane-1'-carboxylic acid N-methylamide
1217299-55-2

(1'S,2'R,3'S,4'R,5'S)-4'-[6-(3-chlorobenzylamino)-2-(1,6-heptadiynyl)-9H-purin-9-yl]-2',3'-dihydroxybicyclo[3.1.0]hexane-1'-carboxylic acid N-methylamide

(1S,2R,3S,4R,5S)-4-(6-(3-chlorobenzylamino)-2-(5-(1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)pent-1-ynyl)-9H-purin-9-yl)-2,3-dihydroxybicyclo[3.1.0]hexane-1-carboxylic acid N-methylamide
1217299-57-4

(1S,2R,3S,4R,5S)-4-(6-(3-chlorobenzylamino)-2-(5-(1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)pent-1-ynyl)-9H-purin-9-yl)-2,3-dihydroxybicyclo[3.1.0]hexane-1-carboxylic acid N-methylamide

Conditions
ConditionsYield
With copper(II) sulphate hydrate; sodium L-ascorbate In tetrahydrofuran; water at 20℃; regioselective reaction;89%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

C16H14O7
1285718-33-3

C16H14O7

C22H17FN4O9
1285718-37-7

C22H17FN4O9

Conditions
ConditionsYield
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In dichloromethane; water at 20℃;87%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

6-methyl-2-oxo-1-(prop-2-yn-1-yl)-4-(trifluoromethyl)-1,2-dihydropyridine-3-carbonitrile
1582270-75-4

6-methyl-2-oxo-1-(prop-2-yn-1-yl)-4-(trifluoromethyl)-1,2-dihydropyridine-3-carbonitrile

1-((1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)methyl)-6-methyl-2-oxo-4-(trifluoromethyl)-1,2-dihydropyridine-3-carbonitrile
1582270-94-7

1-((1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)methyl)-6-methyl-2-oxo-4-(trifluoromethyl)-1,2-dihydropyridine-3-carbonitrile

Conditions
ConditionsYield
Stage #1: 6-methyl-2-oxo-1-(prop-2-yn-1-yl)-4-(trifluoromethyl)-1,2-dihydropyridine-3-carbonitrile With copper(l) iodide In tetrahydrofuran at 20℃; for 0.5h;
Stage #2: 4-fluoro-3-nitrophenylazide In tetrahydrofuran for 12h;
86%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

6-phenyl-2-(prop-2-yn-1-yloxy)-4-(trifluoromethyl)nicotinonitrile
1336913-39-3

6-phenyl-2-(prop-2-yn-1-yloxy)-4-(trifluoromethyl)nicotinonitrile

2-((1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)methoxy)-6-phenyl-4-(trifluoromethyl)nicotinonitrile
1582270-81-2

2-((1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)methoxy)-6-phenyl-4-(trifluoromethyl)nicotinonitrile

Conditions
ConditionsYield
Stage #1: 6-phenyl-2-(prop-2-yn-1-yloxy)-4-(trifluoromethyl)nicotinonitrile With copper(l) iodide In tetrahydrofuran at 20℃; for 0.5h;
Stage #2: 4-fluoro-3-nitrophenylazide In tetrahydrofuran for 12h;
85%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

ethyl 2-(prop-2-ynyloxy)-2-(trifluoromethyl)-2H-chromene-3-carboxylate
1591994-08-9

ethyl 2-(prop-2-ynyloxy)-2-(trifluoromethyl)-2H-chromene-3-carboxylate

ethyl 2-((1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazole-4-yl)methoxy)-2-(trifluoromethyl)-2H-chromene-3-carboxylate
1591994-28-3

ethyl 2-((1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazole-4-yl)methoxy)-2-(trifluoromethyl)-2H-chromene-3-carboxylate

Conditions
ConditionsYield
Stage #1: ethyl 2-(prop-2-ynyloxy)-2-(trifluoromethyl)-2H-chromene-3-carboxylate With copper(l) iodide In tetrahydrofuran at 20℃; for 0.5h; Inert atmosphere;
Stage #2: 4-fluoro-3-nitrophenylazide In tetrahydrofuran at 20℃;
82%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

12-Aminododecanoic acid
693-57-2

12-Aminododecanoic acid

C18H27N5O4
58775-40-9

C18H27N5O4

Conditions
ConditionsYield
In methanol; N,N-dimethyl-formamide at 80℃;80%
1,6-Hexanediamine
124-09-4

1,6-Hexanediamine

4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

N'-(4-azido-2-nitrophenyl)hexane-1,6-diamine
64309-09-7

N'-(4-azido-2-nitrophenyl)hexane-1,6-diamine

Conditions
ConditionsYield
In methanol at 20℃; for 12h; Inert atmosphere;80%
Geraniol
106-24-1

Geraniol

4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

p-azido-o-nitrophenyl geranyl ether
106929-46-8

p-azido-o-nitrophenyl geranyl ether

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran for 14h; Ambient temperature;76%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

diethylamine
109-89-7

diethylamine

4-(N,N-diethylamino)-3-nitrophenylazide

4-(N,N-diethylamino)-3-nitrophenylazide

Conditions
ConditionsYield
In acetonitrile at 40℃; for 3h;67%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

(8R,9S,13S,14S,16S)-16-(4-Amino-but-2-ynyl)-3-(tert-butyl-dimethyl-silanyloxy)-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one
234765-89-0

(8R,9S,13S,14S,16S)-16-(4-Amino-but-2-ynyl)-3-(tert-butyl-dimethyl-silanyloxy)-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one

16α-(4-(4-azido-2-nitrophenylamino)-2-butynyl)estra-1,3,5(10)-triene-3,17β-diol

16α-(4-(4-azido-2-nitrophenylamino)-2-butynyl)estra-1,3,5(10)-triene-3,17β-diol

Conditions
ConditionsYield
With triethylamine In N,N-dimethyl-formamide for 44h; Ambient temperature;59.9%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

histamine dichloride
56-92-8

histamine dichloride

water ethanol
180330-54-5

water ethanol

sodium carbonate
497-19-8

sodium carbonate

4(5)-[2-(4-azido-2-nitroanilino)ethyl]imidazole hydrochloride
79412-26-3

4(5)-[2-(4-azido-2-nitroanilino)ethyl]imidazole hydrochloride

Conditions
ConditionsYield
With hydrogenchloride58%
6-amino-1-hexanol
4048-33-3

6-amino-1-hexanol

4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

6-(4-Azido-2-nitro-phenylamino)-hexan-1-ol

6-(4-Azido-2-nitro-phenylamino)-hexan-1-ol

Conditions
ConditionsYield
With triethylamine In 1,4-dioxane at 20℃; for 2h;55%
In 1,4-dioxane
Stage #1: 6-amino-1-hexanol; 4-fluoro-3-nitrophenylazide In 1,4-dioxane at 20℃; for 0.333333h;
Stage #2: With triethylamine In 1,4-dioxane at 20 - 55℃; for 16h;
16 g
4-pyrrol-1-yl-butylamine
98492-69-4

4-pyrrol-1-yl-butylamine

4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

C14H20N6O2

C14H20N6O2

Conditions
ConditionsYield
In tetrahydrofuran for 0.5h;54%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

3,3-(dimethoxy)-17α-aminopropyl-17β-hydroxy-5α-androstan-3-one
300350-96-3

3,3-(dimethoxy)-17α-aminopropyl-17β-hydroxy-5α-androstan-3-one

17α-[(N-4-azido-2-nitrophenyl)aminopropyl]-3,3-dimethoxy-5α-androstan-17β-ol
300351-12-6

17α-[(N-4-azido-2-nitrophenyl)aminopropyl]-3,3-dimethoxy-5α-androstan-17β-ol

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran; diethyl ether; ethanol47%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

N-(2-aminoethyl)-N'-cyano-N''-<3-<3-(1-piperidinylmethyl)phenoxy>propyl>guanidine
140872-99-7

N-(2-aminoethyl)-N'-cyano-N''-<3-<3-(1-piperidinylmethyl)phenoxy>propyl>guanidine

C25H32N10O3
140873-16-1

C25H32N10O3

Conditions
ConditionsYield
With sodium carbonate In ethanol for 15h; Heating;45%
4-fluoro-3-nitrophenylazide
28166-06-5

4-fluoro-3-nitrophenylazide

C20H32N6O
140900-93-2

C20H32N6O

C26H34N10O3
140873-20-7

C26H34N10O3

Conditions
ConditionsYield
With sodium carbonate In ethanol for 15h; Heating;44%

Raw Materials

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