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inquiry(R) Fesoterodine CAS:286930-02-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiryFactory supply (R) Fesoterodine CAS NO.286930-02-7 Application:Factory supply (R) Fesoterodine CAS NO.286930-02-7
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inquiryisobutyryl chloride
(R)-2-[3-(diisopropylamino)-1-phenylpropyl]-4-(hydroxymethyl)-phenol
fesoterodine
Conditions | Yield |
---|---|
With sodium hydroxide In water; toluene at 20℃; Product distribution / selectivity; Inert atmosphere; | 98% |
With sodium hydroxide In water; toluene at 20℃; for 0.166667h; Product distribution / selectivity; Inert atmosphere; | 98% |
With sodium hydroxide In water; toluene at 20℃; Inert atmosphere; | 98% |
(R)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-trityloxymethylphenoxyisobutyrate
fesoterodine
Conditions | Yield |
---|---|
With hydrogenchloride In water; acetonitrile at 50℃; for 1h; pH=2 - 2.5; Concentration; Time; | 98% |
fesoterodine
Conditions | Yield |
---|---|
In dichloromethane; water at 20 - 30℃; Product distribution / selectivity; | 92.6% |
2-Methylpropionic anhydride
(R)-2-[3-(diisopropylamino)-1-phenylpropyl]-4-(hydroxymethyl)-phenol
fesoterodine
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran; ethanol at 0 - 20℃; Inert atmosphere; | 83.8% |
(R)-3-(N,N'-diisopropylamino-1-phenyl-propyl)-4-isobutyryloxy-benzoic acid
fesoterodine
Conditions | Yield |
---|---|
With dimethylsulfide borane complex In tetrahydrofuran at 10 - 25℃; | 60.5% |
isobutyryl chloride
(R)-2-[3-(diisopropylamino)-1-phenylpropyl]-4-(hydroxymethyl)-phenol
A
fesoterodine
B
C30H43NO4
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at -10 - -5℃; for 2.5h; Product distribution / selectivity; | |
With triethylamine In dichloromethane at -10 - -5℃; for 2.5h; Product distribution / selectivity; | |
Stage #1: isobutyryl chloride; (R)-2-[3-(diisopropylamino)-1-phenylpropyl]-4-(hydroxymethyl)-phenol In dichloromethane at -10 - -5℃; for 2.5h; Stage #2: With sodium carbonate In dichloromethane; water Product distribution / selectivity; |
2-[(1R)-3-[bis(1-methylethyl)amino]-1-phenylpropyl]-4-hydroxy-methylphenyl isobutyrate mandelate
fesoterodine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In dichloromethane; water for 0.166667h; |
fesoterodine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: ethanol / 20 - 60 °C / Inert atmosphere 2.1: sodium hydrogencarbonate / ethyl acetate / Inert atmosphere 2.2: 3.5 h / 20 °C 2.3: 0.5 h / -10 - 20 °C 3.1: sodium hydroxide / toluene; water / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ethanol / 60 °C / Inert atmosphere 2.1: sodium hydrogencarbonate / ethyl acetate / Inert atmosphere 3.1: lithium aluminium tetrahydride / tetrahydrofuran / 3.5 h / 20 °C 3.2: -10 °C 4.1: sodium hydroxide / toluene; water / 0.17 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: ethanol / 60 °C / Inert atmosphere 2.1: sodium hydrogencarbonate / ethyl acetate; water / Inert atmosphere 3.1: sodium hydroxide / methanol / 0 - 35 °C / Inert atmosphere 3.2: 5 - 25 °C 3.3: 3 h 4.1: sodium hydroxide / toluene; water / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 0 - 30 °C / Inert atmosphere 2.1: D-Malic acid / isopropyl alcohol; di-isopropyl ether / 20 - 80 °C 2.2: pH 10 View Scheme |
methyl 4-hydroxylbenzoate
fesoterodine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: methanesulfonic acid / 50 - 55 °C / Inert atmosphere 2.1: ethanol / 20 - 60 °C / Inert atmosphere 3.1: sodium hydrogencarbonate / ethyl acetate / Inert atmosphere 3.2: 3.5 h / 20 °C 3.3: 0.5 h / -10 - 20 °C 4.1: sodium hydroxide / toluene; water / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 5 steps 1.1: methanesulfonic acid / water / 50 - 55 °C / Inert atmosphere 2.1: ethanol / 60 °C / Inert atmosphere 3.1: sodium hydrogencarbonate / ethyl acetate / Inert atmosphere 4.1: lithium aluminium tetrahydride / tetrahydrofuran / 3.5 h / 20 °C 4.2: -10 °C 5.1: sodium hydroxide / toluene; water / 0.17 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 5 steps 1.1: methanesulfonic acid / 50 - 55 °C / Inert atmosphere 2.1: ethanol / 60 °C / Inert atmosphere 3.1: sodium hydrogencarbonate / ethyl acetate; water / Inert atmosphere 4.1: sodium hydroxide / methanol / 0 - 35 °C / Inert atmosphere 4.2: 5 - 25 °C 4.3: 3 h 5.1: sodium hydroxide / toluene; water / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 5 steps 1.1: 1-methyl-piperazine / toluene / 25 - 110 °C 1.2: 5 h / 60 - 65 °C 2.1: hydrogen / 5%-palladium/activated carbon / methanol / 25 - 50 °C / 10343.2 Torr / Autoclave 3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 0 - 30 °C / Inert atmosphere 4.1: D-Malic acid / isopropyl alcohol; di-isopropyl ether / 20 - 80 °C 4.2: pH 10 View Scheme |
3-(N,N-diisopropylamino)-1-phenylpropan-1-ol
fesoterodine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: methanesulfonic acid / 50 - 55 °C / Inert atmosphere 2.1: ethanol / 20 - 60 °C / Inert atmosphere 3.1: sodium hydrogencarbonate / ethyl acetate / Inert atmosphere 3.2: 3.5 h / 20 °C 3.3: 0.5 h / -10 - 20 °C 4.1: sodium hydroxide / toluene; water / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 5 steps 1.1: methanesulfonic acid / water / 50 - 55 °C / Inert atmosphere 2.1: ethanol / 60 °C / Inert atmosphere 3.1: sodium hydrogencarbonate / ethyl acetate / Inert atmosphere 4.1: lithium aluminium tetrahydride / tetrahydrofuran / 3.5 h / 20 °C 4.2: -10 °C 5.1: sodium hydroxide / toluene; water / 0.17 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 5 steps 1.1: methanesulfonic acid / 50 - 55 °C / Inert atmosphere 2.1: ethanol / 60 °C / Inert atmosphere 3.1: sodium hydrogencarbonate / ethyl acetate; water / Inert atmosphere 4.1: sodium hydroxide / methanol / 0 - 35 °C / Inert atmosphere 4.2: 5 - 25 °C 4.3: 3 h 5.1: sodium hydroxide / toluene; water / 20 °C / Inert atmosphere View Scheme |
fesoterodine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: lithium aluminium tetrahydride / tetrahydrofuran / 3.5 h / 20 °C 1.2: -10 °C 2.1: sodium hydroxide / toluene; water / 0.17 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1.1: sodium hydroxide / methanol / 0 - 35 °C / Inert atmosphere 1.2: 5 - 25 °C 1.3: 3 h 2.1: sodium hydroxide / toluene; water / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran / 2 h / 0 - 5 °C / Inert atmosphere 2: sodium hydrogencarbonate / dichloromethane; water / 0.5 h / 0 - 5 °C / Inert atmosphere View Scheme |
methyl (R)-(-)-3-(3-diisopropylamino-1-phenyl-propyl)-4-hydroxy-benzoate 2,3-dibenzoyl-D-tartaric acid salt
fesoterodine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium hydrogencarbonate / ethyl acetate / Inert atmosphere 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 3.5 h / 20 °C 2.2: -10 °C 3.1: sodium hydroxide / toluene; water / 0.17 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: sodium hydrogencarbonate / ethyl acetate; water / Inert atmosphere 2.1: sodium hydroxide / methanol / 0 - 35 °C / Inert atmosphere 2.2: 5 - 25 °C 2.3: 3 h 3.1: sodium hydroxide / toluene; water / 20 °C / Inert atmosphere View Scheme |
(E)-3-phenylacrylic acid
fesoterodine
Conditions | Yield |
---|---|
Multi-step reaction with 12 steps 1.1: sulfuric acid / 120 - 125 °C 2.1: potassium carbonate; sodium iodide / acetone / Reflux 3.1: sodium tetrahydroborate / 1,2-dimethoxyethane / 0.17 h 3.2: 3 h / 10 °C 4.1: triethylamine / dichloromethane / 12 h / 25 - 30 °C 5.1: acetonitrile / 30 h / 95 - 100 °C / autoclave; Sealed tube 6.1: isopropyl alcohol / 15 h / 25 - 86 °C 7.1: sodium hydroxide / water 8.1: ethyl bromide; iodine; magnesium / tetrahydrofuran / 1 h / 55 °C / Reflux 8.2: 1 h / -65 - -60 °C 9.1: thionyl chloride / 10 °C / Reflux 10.1: lithium aluminium tetrahydride / tetrahydrofuran / 14 h / 25 - 30 °C 11.1: hydrogen / 5% Pd(II)/C(eggshell) / methanol / 50 - 55 °C 12.1: dichloromethane / 1.5 h / 0 - 5 °C 12.2: 1 h / 0 - 5 °C View Scheme | |
Multi-step reaction with 10 steps 1.1: sulfuric acid / 120 - 125 °C / Inert atmosphere 2.1: potassium carbonate / acetone / Reflux 3.1: potassium hydroxide; water / methanol / Inert atmosphere; Reflux 3.2: pH 1 - 2 4.1: toluene / 0 - 10 °C 4.2: 50 - 60 °C 5.1: sodium tetrahydroborate; boron trifluoride diethyl etherate / tetrahydrofuran / 31 - 35 °C 5.2: 30 - 65 °C 6.1: isopropyl alcohol; water / Reflux 7.1: sodium carbonate / dichloromethane; water 7.2: 14 - 20 °C 8.1: hydrogenchloride; sodium tetrahydroborate / water / 32 - 38 °C 8.2: Reflux 9.1: sodium hydroxide; sodium carbonate / dichloromethane; water 9.2: Raney nickel 10.1: triethylamine / dichloromethane / 0.75 h / 0 - 20 °C View Scheme |
methyl 4-(benzyloxy)-3-[(1R)-3-(dipropan-2-ylamino)-1-phenylpropyl]benzoate
fesoterodine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: lithium aluminium tetrahydride / tetrahydrofuran / 14 h / 25 - 30 °C 2.1: hydrogen / 5% Pd(II)/C(eggshell) / methanol / 50 - 55 °C 3.1: dichloromethane / 1.5 h / 0 - 5 °C 3.2: 1 h / 0 - 5 °C View Scheme | |
Multi-step reaction with 3 steps 1: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 3 h / Inert atmosphere 2: hydrogen / Raney nickel / methanol / 20 °C 3: triethylamine / acetonitrile / -10 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 5 h / 0 - 20 °C / Inert atmosphere 1.2: 0 - 5 °C 2.1: hydrogen / 5%-palladium/activated carbon / methanol / 2 h / 25 - 35 °C / Autoclave 2.2: 25 - 35 °C 3.1: dichloromethane / 1.5 h / 0 - 5 °C 3.2: 0.5 h / 0 - 5 °C View Scheme |
R-(-)-[3-(2-benzyloxy-5-bromophenyl)-3-phenylpropyl]diisopropylamine
fesoterodine
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: ethyl bromide; iodine; magnesium / tetrahydrofuran / 1 h / 55 °C / Reflux 1.2: 1 h / -65 - -60 °C 2.1: thionyl chloride / 10 °C / Reflux 3.1: lithium aluminium tetrahydride / tetrahydrofuran / 14 h / 25 - 30 °C 4.1: hydrogen / 5% Pd(II)/C(eggshell) / methanol / 50 - 55 °C 5.1: dichloromethane / 1.5 h / 0 - 5 °C 5.2: 1 h / 0 - 5 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: magnesium / iodine / tetrahydrofuran / 1 h / -70 - 70 °C 1.2: -5 - 35 °C 1.3: pH 1 - 2 2.1: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 0.25 h / 0 - 5 °C 3.1: hydrogen / 5%-palladium/activated carbon / methanol / 2 h / 25 - 35 °C / Autoclave 3.2: 25 - 35 °C 4.1: dichloromethane / 1.5 h / 0 - 5 °C 4.2: 0.5 h / 0 - 5 °C View Scheme | |
Multi-step reaction with 5 steps 1.1: iodine; magnesium; ethyl bromide / tetrahydrofuran / 2 h / 60 - 65 °C / Inert atmosphere 1.2: 1 h / -70 - -50 °C 2.1: thionyl chloride / 0 - 65 °C 3.1: lithium aluminium tetrahydride / tetrahydrofuran / 30 °C 4.1: hydrogen; palladium 10% on activated carbon / isopropyl alcohol / 25 - 30 °C / 2068.65 - 2585.81 Torr / Autoclave 5.1: sodium hydrogencarbonate / dichloromethane / 3 h / -2 - 3 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 9 steps 1.1: triethylamine / dichloromethane / 12 h / 25 - 30 °C 2.1: acetonitrile / 30 h / 95 - 100 °C / autoclave; Sealed tube 3.1: isopropyl alcohol / 15 h / 25 - 86 °C 4.1: sodium hydroxide / water 5.1: ethyl bromide; iodine; magnesium / tetrahydrofuran / 1 h / 55 °C / Reflux 5.2: 1 h / -65 - -60 °C 6.1: thionyl chloride / 10 °C / Reflux 7.1: lithium aluminium tetrahydride / tetrahydrofuran / 14 h / 25 - 30 °C 8.1: hydrogen / 5% Pd(II)/C(eggshell) / methanol / 50 - 55 °C 9.1: dichloromethane / 1.5 h / 0 - 5 °C 9.2: 1 h / 0 - 5 °C View Scheme | |
Multi-step reaction with 8 steps 1.1: pyridine / dichloromethane / 5 - 30 °C / Industry scale 2.1: water / 75 - 78 °C / Industry scale 3.1: ethyl bromide; iodine; magnesium / tetrahydrofuran / 50 - 60 °C 3.2: -70 - -60 °C 3.3: -50 °C 4.1: borane-dimethyl sulfide complex / tetrahydrofuran / 25 - 50 °C 4.2: 0.5 h / 10 - 15 °C / Industry scale 5.1: raney nickel / methanol / 30 - 35 °C / Autoclave 6.1: tetrahydrofuran / 10 - 55 °C 7.1: potassium carbonate / toluene; water / 50 - 55 °C 8.1: dichloromethane / -25 - -20 °C View Scheme | |
Multi-step reaction with 8 steps 1.1: pyridine / dichloromethane / 5 - 30 °C / Industry scale 1.2: 5 - 30 °C / Industry scale 2.1: water / 75 - 78 °C / Industry scale 3.1: ethyl bromide; magnesium / iodine / tetrahydrofuran / 50 - 60 °C 3.2: -70 - -60 °C 4.1: dimethylsulfide borane complex / tetrahydrofuran / 25 - 50 °C 5.1: methanol / 30 - 35 °C 6.1: tetrahydrofuran / 10 - 55 °C 7.1: potassium carbonate / toluene; water / 50 - 55 °C 8.1: dichloromethane / -25 - -20 °C View Scheme |
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