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N~2~-methyl-L-glutamine CAS NO.3081-62-7 Application:N~2~-methyl-L-glutamine CAS NO.3081-62-7
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Conditions | Yield |
---|---|
In methanol at 70℃; for 168h; | 26% |
N2-benzyloxycarbonyl-N5-methyl-L-glutamine
N-(γ-glutamyl)methylamine
Conditions | Yield |
---|---|
With palladium Hydrogenation; |
L-glutamic acid-5-ethyl ester; hydrochloride
methylamine
N-(γ-glutamyl)methylamine
Conditions | Yield |
---|---|
With ethanol |
Conditions | Yield |
---|---|
(i) CS2, MeOH, (ii) AcOH; Multistep reaction; |
methylamine hydrochloride
monosodium glutamate
N-(γ-glutamyl)methylamine
Conditions | Yield |
---|---|
In water at 30℃; for 0.166667h; γ-glutamylmethylamide synthetase from Methylophaga sp. AA-30, 0.5 M Tris HCl buffer pH 7.5, 2.5 M 2-mercaptoethanol, 0.1 M MnCl2, 0.1 M ATP; | |
In water at 30℃; for 0.166667h; γ-glutamylmethylamide synthetase from Methylophaga sp. AA-30, 0.5 M Tris HCl buffer pH 7.5, 2.5 M 2-mercaptoethanol, 0.1 M MnCl2, 0.1 M ATP; relative enzyme activity, Km, effect of pH, temperature, metal ions; |
L-glutamine
methylamine
A
L-glutamic acid
B
N-(γ-glutamyl)methylamine
Conditions | Yield |
---|---|
With glutaminase from Pseudomonas nitroreducens IFO 12694; imidazole buffer In water at 30℃; for 1h; Product distribution; other reagent, pH dependence; |
Conditions | Yield |
---|---|
With glutaminase from Pseudomonas nitroreducens IFO 12694; imidazole buffer In water at 30℃; relative rate of glutamyl transfer; | |
With recombinant Pseudomonas nitroreducens IFO12694 γ-glutamyltranspeptidase at 30℃; for 0.333333h; pH=10.5; aq. buffer; Enzymatic reaction; |
Conditions | Yield |
---|---|
With glutaminase from Pseudomonas nitroreducens IFO 12694; imidazole buffer In water at 30℃; relative rate of glutamyl transfer; |
Conditions | Yield |
---|---|
With water at 37℃; |
Conditions | Yield |
---|---|
With imidazole buffer; Pseudomonas taetrolens Y-30 glutamine synthetase EC 6.3.1.2; magnesium chloride; ATP at 30℃; pH=8.5; Enzyme kinetics; Further Variations:; pH-values; Reagents; |
methylamine hydrochloride
monosodium L-glutamate
N-(γ-glutamyl)methylamine
Conditions | Yield |
---|---|
With 1H-imidazole; ATP; magnesium chloride; Methylovorus mays No. 9 theanine-forming enzyme In water at 30℃; pH=7.75; Enzyme kinetics; |
Conditions | Yield |
---|---|
With recombinant (His)6-tagged Escherichia coli K12 W3110 γ-glutamylcysteine synthetase; magnesium sulfate; ATP In water at 37℃; for 1h; pH=8.5; aq. buffer; Enzymatic reaction; |
γ-L-glutamyl-L-glutamine
N-(γ-glutamyl)methylamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: recombinant Pseudomonas nitroreducens IFO12694 γ-glutamyltranspeptidase / 0.03 h / 30 °C / pH 10.5 / aq. buffer; Enzymatic reaction 2: recombinant Pseudomonas nitroreducens IFO12694 γ-glutamyltranspeptidase / 0.33 h / 30 °C / pH 10.5 / aq. buffer; Enzymatic reaction View Scheme |
A
N-(γ-glutamyl)methylamine
B
(R)-(-)-α-methylamino phenylacetic acid
C
L-proline
Conditions | Yield |
---|---|
With hydrogenchloride In water at 110℃; for 24h; |
Conditions | Yield |
---|---|
With lithium hydroxide In methanol ligand was reacted with LiOH; soln. of ZnCl2 in methanol was added at room temp.; washed (methanol); elem. anal.; | 63% |
N-(γ-glutamyl)methylamine
2-oxo-glutaric acid-5-methylamide
Conditions | Yield |
---|---|
With enzyme from the toxin of crotalus adamanteus; catalase |
Conditions | Yield |
---|---|
With recombinant Pseudomonas nitroreducens IFO12694 γ-glutamyltranspeptidase at 30℃; for 0.0333333h; pH=10.5; aq. buffer; Enzymatic reaction; |
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