As a leading and professional manufacturer of APIs and API intermediates in China,Anhui Dexinjia Biopharm Co., Ltd founded in 2006, Except for the R&D center, our company has built a close cooperation relation with Chinese Academy of Sciences,
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inquiryUnique advantages for L(-)-Pipecolinic acid Cas3105-95-1 Guaranteed the purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White crystalline powder Package:1kg/foil bag;25kg/drum Applicati
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inquiryProduct description: Product name L(-)-Pipecolinic acid CAS number 3105-95-1 Assay ≥98% Appearance White crystalline powder Capacity 200mt/year Application Pharmaceutical int
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inquiryHigh purity CAS 3105-95-1 L(-)-Pipecolinic acid in stock Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediates (Fluo
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inquiryEnglish Name L(-)-Pipecolinic acid CAS Number 3105-95-1 Molec
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inquiryProduct Name: L-PIPECOLINIC ACID Synonyms: RARECHEM BK PT F201;(S)-(-)-2-PIPERIDINECARBOXYLIC ACID;(S)-2-PIPERIDINECARBOXYLIC ACID;S-(-)-PIPECOLINIC ACID;(S)-(-)-PIPECOLI
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Product Name: L(-)-Pipecolinic acid Synonyms: RARECHEM BK PT F201;(S)-(-)-2-PIPERIDINECARBOXYLIC ACID;(S)-2-PIPERIDINECARBOXYLIC ACID;S-(-)-PIPECOLINIC ACID;(S)-(-)-PIPECOLIC ACID;(S)-PIPECOLIC ACID;(S)-PIPERIDINE-2-CARBOXYLIC ACID;PIP-OH CAS:
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inquiryConditions | Yield |
---|---|
With porcine kidney D-amino acid oxidase; Pseudomonas putida N-methyl-L-amino acid dehydrogenase; Tris buffer; flavin adenine dinucleotide; catalase In various solvent(s) at 30℃; for 24h; pH=5.1 - 7.6; | 100% |
(S)-(-)-2-piperidinecarboxylic acid ethyl ester hydrochloride
pipecolinic acid
Conditions | Yield |
---|---|
With hydrogenchloride; water at 90℃; for 6h; | 100% |
(S)-1-(carbobenzyloxy)-2-piperidinecarboxylic acid
pipecolinic acid
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In methanol under 2327.2 Torr; for 6h; Ambient temperature; | 94% |
pipecolinic acid
Conditions | Yield |
---|---|
With lithium hydroxide In tetrahydrofuran at 0℃; for 3h; Reagent/catalyst; | 93.2% |
(4S,9aS)-4-phenylhexahydropyrido[2,1-c][1,4]oxazin-1-one
pipecolinic acid
Conditions | Yield |
---|---|
With hydrogen; palladium dihydroxide In ethanol for 2h; Catalytic hydrogenation; | 91% |
methyl (S)-pipecolinate
pipecolinic acid
Conditions | Yield |
---|---|
With sodium hydroxide at 120℃; for 3h; | 91% |
Conditions | Yield |
---|---|
With bovine liver catalase; D-glucose; NADP In water at 30℃; for 17h; pH=7.5; | 90% |
platinum(IV) oxide; Pt/titania In water for 44h; Irradiation; pH 9.7; | 33% |
With lysine aminotransferase expressed by Escherichia coli JM109 |
pipecolinic acid
Conditions | Yield |
---|---|
With water; hydrogen bromide at 70℃; for 5h; Reagent/catalyst; Temperature; | 90% |
(2S)-1-(4-methylphenylsulfonyl)piperidine-2-carboxylic acid
pipecolinic acid
Conditions | Yield |
---|---|
With sodium amalgam; sodium phosphate In methanol at 20℃; for 5h; | 80% |
(4R)-4-Phenylhexahydropyrido<2,1-c><1,4>oxazin-1-one
pipecolinic acid
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol; acetic acid for 1h; | 70% |
(2S)-2-piperidinecarboxylic acid L-tartrate
pipecolinic acid
Conditions | Yield |
---|---|
With Amberlite IR-120 In water | 59% |
Conditions | Yield |
---|---|
With porcine kidney D-amino acid oxidase; Pseudomonas putida N-methyl-L-amino acid dehydrogenase; Tris buffer; flavin adenine dinucleotide; catalase In various solvent(s) at 30℃; for 24h; pH=8.0; | 50% |
With D-tartaric acid |
(3S,5S)-2,3,5,6-tetrahydro-3-(4-bromobutyl)-5-phenyl-N-(benzyloxycarbonyl)-4H-1,4-oxazine-2-one
A
L-Norleucine
B
pipecolinic acid
Conditions | Yield |
---|---|
With hydrogen; trifluoroacetic acid; palladium on activated charcoal In methanol under 2844.31 Torr; for 24h; | A 12% B 45% |
N-acetyl-DL-2-amino-6-bromohexanoic acid
A
pipecolinic acid
B
N-acetyl-D-2-amino-6-bromohexanoic acid
Conditions | Yield |
---|---|
With sodium hydroxide; Aspergillus L-aminoacylase; cobalt(II) chloride In water at 38℃; for 24h; pH=7; | A 35% B n/a C n/a |
(RS)-piperidine-2-carboxamide
pipecolinic acid
Conditions | Yield |
---|---|
With air; D-glucose; Pseudomonas fluorescens DSM 9924 cells; yeast extract at 30℃; | 20% |
(2S,3'S,5'R,6'R)-6'-(3-Carboxy-propyl)-[2,3']bipiperidinyl-5'-carboxylic acid
A
pipecolinic acid
B
3-amino propanoic acid
C
4-amino-n-butyric acid
Conditions | Yield |
---|---|
With chromium(VI) oxide In sulfuric acid at 100℃; for 6h; | A 9% B n/a C n/a |
(2S)-1,2,3,6-tetrahydropyridine-2-carboxylic acid
pipecolinic acid
Conditions | Yield |
---|---|
With methanol; platinum Hydrogenation; |
Conditions | Yield |
---|---|
With hydrogen |
Conditions | Yield |
---|---|
platinum(IV) oxide; Pt/titania In water for 24h; Irradiation; pH 5.8; | 17 % Chromat. |
Conditions | Yield |
---|---|
platinum(IV) oxide; Pt/titania In water for 24h; Irradiation; pH 5.7; | 43 % Chromat. |
N-6-(aminocarbonyl)-L-lysine
pipecolinic acid
Conditions | Yield |
---|---|
platinum(IV) oxide; Pt/titania In water for 17h; Irradiation; pH 7.3; | 38 % Chromat. |
Conditions | Yield |
---|---|
platinum(IV) oxide; Pt/titania In water for 41h; Irradiation; pH 4.6; | 11 % Chromat. |
Conditions | Yield |
---|---|
platinum(IV) oxide; Pt/titania In water for 47h; Irradiation; pH 6.6; | 8 % Chromat. |
L-Lysine hydrochloride
pipecolinic acid
Conditions | Yield |
---|---|
With sodium nitroprusside; sodium hydroxide In water at 60℃; for 4h; pH=9.5; Yield given; | |
at 37℃; for 20h; pH=7; Enzymatic reaction; | n/a |
Tacrolimus
pipecolinic acid
Conditions | Yield |
---|---|
With hydrogenchloride Heating; |
(22E,24E,26E,27E,29R,30S,31R,32R,34S,36S,38S,39S,40S,41R,50R)-40,50-dihydroxy-39-[(1R)-2-[(1S,3R,4R)-4-hydroxy-3-methoxy-cyclohexyl]-1-methyl-ethyl]-38,41-dimethoxy-29,30,31,32,42,43-hexamethyl-60,61-dioxa-51-azatricyclohexatriaconta-22,24,26(42),27(43)-tetraene-44,45,46,47,48-pentone
pipecolinic acid
Conditions | Yield |
---|---|
With hydrogenchloride In methanol for 32h; |
methyl piperidine-2-carboxylate hydrochloride
A
pipecolinic acid
B
(R)-(+)-pipecolic acid
Conditions | Yield |
---|---|
With Aspergillus niger lipase Product distribution; enantioselectivity, different pH, enzyme assay, other pipecolate esters; |
(2R,3R)-3-hydroxypiperidine-1-carboxylic acis
pipecolinic acid
Conditions | Yield |
---|---|
With phosphorus; hydrogen iodide at 140℃; for 5h; |
B
pipecolinic acid
Conditions | Yield |
---|---|
Aspergillus niger lipase for 3h; |
formaldehyd
pipecolinic acid
(-)-(2S)-1-methylpiperidine-2-carboxylic acid
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In methanol under 836.056 Torr; for 24h; | 100% |
With hydrogen; palladium on activated charcoal In methanol; water for 42h; |
1-benzylisatin
ethyl (2E)-(1-benzyl-2-oxo-1,2-dihydro-3H-indol-3-ylidene)acetate
pipecolinic acid
Conditions | Yield |
---|---|
In ethanol at 20℃; for 2h; diastereoselective reaction; | 99% |
di-tert-butyl dicarbonate
pipecolinic acid
(S)-(-)-1-(tert-butoxycarbonyl)-2-piperidinecarboxylic acid
Conditions | Yield |
---|---|
With TEA In methanol a) 50 deg C, 5 min, b) RT, 1 h; | 98% |
95% | |
With sodium hydrogencarbonate In tetrahydrofuran; water at 25℃; Inert atmosphere; | 95.8% |
Conditions | Yield |
---|---|
With thionyl chloride at 20℃; for 48h; | 97.5% |
With thionyl chloride at 0 - 20℃; for 10.58h; | 95% |
With thionyl chloride at 0 - 20℃; | 92% |
methyl chloroformate
pipecolinic acid
(S)-(-)-[(N-methoxycarbonyl)piperidine]-2-carboxylic acid
Conditions | Yield |
---|---|
With sodium hydroxide In water at 20℃; pH=8 - 9; Acylation; | 97% |
With sodium hydroxide In water | 66% |
With sodium hydroxide In water | 66% |
Conditions | Yield |
---|---|
With 5%-palladium/activated carbon; hydrogen In ethanol at 20℃; Solvent; Reagent/catalyst; | 96.8% |
Stage #1: butyraldehyde; pipecolinic acid With trifluoroacetic acid In methanol at 20℃; for 1h; Stage #2: With sodium cyanoborohydride In methanol at 30 - 40℃; for 6h; Reagent/catalyst; Concentration; | 65% |
pipecolinic acid
(S)-Piperidine-2-carbonyl chloride
Conditions | Yield |
---|---|
With thionyl chloride In ethanol | 95% |
Multi-step reaction with 2 steps 1: NaOH / H2O / 0 °C 2: SOCl2 / CH2Cl2 / 24 h / Ambient temperature View Scheme | |
Stage #1: pipecolinic acid With thionyl chloride In methanol at -20℃; Reflux; Stage #2: With triethylamine In ethyl acetate at 20℃; | |
With thionyl chloride In dichloromethane at 20℃; |
pipecolinic acid
(S)-pipecolinol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 14h; Reflux; Inert atmosphere; | 95% |
With lithium aluminium tetrahydride In tetrahydrofuran for 8h; Reflux; | 90% |
Stage #1: pipecolinic acid With dimethylsulfide borane complex; boron trifluoride diethyl etherate In tetrahydrofuran at 0℃; Reflux; Stage #2: With hydrogenchloride; methanol In water at 0℃; Reflux; | 80% |
Conditions | Yield |
---|---|
Stage #1: pipecolinic acid With thionyl chloride at 20 - 23℃; for 16h; Inert atmosphere; Stage #2: ethanol for 6h; Inert atmosphere; | 95% |
With thionyl chloride for 4h; Reflux; | 90% |
With thionyl chloride at 70℃; for 12h; |
Conditions | Yield |
---|---|
In water at 20℃; for 336h; Inert atmosphere; | 95% |
pipecolinic acid
Conditions | Yield |
---|---|
In methanol mixed, stirred for 2 h, filtered, evaptd.(vac.), redissolved, pptd.(diethylether), filtered off, washed(diethylether), dried(vac.); elem. anal.; | 94% |
(E)-4-Ethoxy-1,1,1-trifluoro-3-buten-2-one
pipecolinic acid
Conditions | Yield |
---|---|
Stage #1: (E)-4-Ethoxy-1,1,1-trifluoro-3-buten-2-one; pipecolinic acid With sodium hydrogencarbonate In water Stage #2: Acidic conditions; | 91% |
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In dichloromethane | 90% |
benzyl chloroformate
pipecolinic acid
(S)-1-(carbobenzyloxy)-2-piperidinecarboxylic acid
Conditions | Yield |
---|---|
With sodium carbonate In 1,3-dioxane; water | 89% |
With sodium carbonate In 1,4-dioxane; water | 89% |
With sodium hydroxide for 6h; Ambient temperature; | |
With sodium hydroxide In tetrahydrofuran; water at 20℃; for 4h; | |
With sodium hydroxide In water at 0℃; for 4h; |
6,8-dichloro-3-nitro-2-phenyl-2H-chromene
indole-2,3-dione
pipecolinic acid
Conditions | Yield |
---|---|
In ethanol for 2h; Reflux; stereoselective reaction; | 89% |
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile
pipecolinic acid
(S)-(-)-1-(tert-butoxycarbonyl)-2-piperidinecarboxylic acid
Conditions | Yield |
---|---|
With triethylamine In water; acetone | 88% |
Conditions | Yield |
---|---|
With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide In dichloromethane at 20℃; for 12h; | 88% |
Stage #1: pipecolinic acid With hydrogenchloride; thionyl chloride In N,N-dimethyl-formamide; toluene at 55℃; for 3h; Stage #2: 2,6-dimethylaniline With hydrogenchloride In N,N-dimethyl-formamide; toluene at 55℃; for 3h; | 88% |
Stage #1: pipecolinic acid With hydrogenchloride In 1,4-dioxane; toluene for 1h; Stage #2: 2,6-dimethylaniline With trichlorophosphate In 1,4-dioxane; toluene at 20℃; Stage #3: With sodium hydroxide In 1,4-dioxane; water; toluene pH=6 - 11; | 60% |
Stage #1: 2,6-dimethylaniline; pipecolinic acid With methanesulfonyl chloride In tetrahydrofuran at 50℃; Stage #2: With sodium hydroxide In tetrahydrofuran; water pH=4 - 9; | 42% |
Stage #1: pipecolinic acid With hydrogenchloride; thionyl chloride In chloroform; water; N,N-dimethyl-formamide; toluene at 40℃; for 3h; pH=2; Sonication; Inert atmosphere; Stage #2: 2,6-dimethylaniline In chloroform; N,N-dimethyl-formamide; toluene at 45℃; for 1.2h; pH-value; Temperature; Wavelength; Sonication; |
Conditions | Yield |
---|---|
In ethanol for 2h; Reflux; stereoselective reaction; | 88% |
6-chloro-3-nitro-2-phenyl-2H-chromene
indole-2,3-dione
pipecolinic acid
Conditions | Yield |
---|---|
In ethanol for 2h; Reflux; stereoselective reaction; | 88% |
4-benzylidene-3-methyl-1-phenylpyrazolone
benzaldehyde
pipecolinic acid
Conditions | Yield |
---|---|
In chloroform at 75℃; for 1h; Sealed tube; Inert atmosphere; Molecular sieve; | 88% |
9-bromo-2-(1-isopropyl-1H-1,2,4-triazol-5-yl)-5,6-dihydrobenzo-[f ]imidazo[1,2-d][1,4]oxazepine
pipecolinic acid
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; methyl pyridine-2-carboxylate In dimethyl sulfoxide at 80℃; for 24h; | 87% |
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