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Cas:3143-02-0
Min.Order:1 Kilogram
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Type:Manufacturers
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inquiryUnique advantages for 3-Methyl-3-oxetanemethanol Cas 3143-02-0 Guaranteed the purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Clear colorless liquid Storage:cool dry place Package:25kg/drum;20
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Min.Order:1 Kilogram
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Type:Trading Company
inquiryProduct description: Product name 3-Methyl-3-oxetanemethanol CAS number 3143-02-0 Assay ≥98% Appearance Colorless to yellowish liquid Capacity 200mt/year Application Organic
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Min.Order:10 Gram
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Min.Order:1 Gram
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Type:Manufacturers
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developmen
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiry3-Methyl-3-oxetanemethanol CAS: 3143-02-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organi
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Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
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Min.Order:1 Kilogram
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Negotiable
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Cas:3143-02-0
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inquiryProduct Name: 3-Methyl-3-oxetanemethanol Synonyms: 3-METHYL-3-OXETANEMETHANOL;3-METHYL-3-OXETHANEMETHANOL;3-HYDROXYMETHYL-3-METHYLOXETANE;2-HYDROXYMETHYL-2-METHYL-1,3-EPOXYPROPANE;RARECHEM AK ML 0581;TIMTEC-BB SBB009078;3-METHYL-3-OXETANEMETHANO
Cas:3143-02-0
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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Min.Order:1 Gram
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Type:Trading Company
inquirytert-butyl[(3-methyloxetan-3-yl)methoxy]diphenylsilane
3-hydroxymethyl-3-methyloxethane
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at 20℃; for 2h; | 84% |
With tetrabutyl ammonium fluoride In tetrahydrofuran at 20℃; for 2h; | 84% |
Conditions | Yield |
---|---|
With potassium hydroxide; Diethyl carbonate at 115℃; for 1h; | 83.7% |
With potassium hydroxide; Diethyl carbonate In ethanol for 2h; Heating; | 81% |
Stage #1: 2-(hydroxymethyl)-2-methylpropane-1,3-diol With potassium hydroxide; carbonic acid dimethyl ester In methanol under 760.051 Torr; Heating; Stage #2: at 130 - 140℃; under 110 - 120 Torr; | 77% |
1,1,1-Trimethylolethane dinitrate
A
3-hydroxymethyl-3-methyloxethane
B
2-(hydroxymethyl)-2-methylpropane-1,3-diol
C
ethyl nitrate
D
1,1,1-Trimethylolethane mononitrate
E
3-methyl-3-(nitroxymethyl)oxetane
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water at 55℃; for 3.10833h; Product distribution; Rate constant; var. NaOH conc.; | A 13% B 0.7% C n/a D 24% E 66% F n/a |
trimethylolethane trinitrate
A
3-hydroxymethyl-3-methyloxethane
B
2-(hydroxymethyl)-2-methylpropane-1,3-diol
C
1,1,1-Trimethylolethane mononitrate
D
1,1,1-Trimethylolethane dinitrate
E
3-methyl-3-(nitroxymethyl)oxetane
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water at 55℃; for 86.1667h; Product distribution; Rate constant; Thermodynamic data; var. NaOH conc., var. solv., solv. effect, ΔH(excit.), ΔF(excit.), ΔS(excit.); | A 45.5% B 2.3% C 31.8% D 1.5% E 16.5% |
Conditions | Yield |
---|---|
With Ph4SbOMe In 1,2-dichloro-ethane at 60℃; for 24h; sealed ampule; | 82 % Chromat. |
2-(hydroxymethyl)-2-methylpropane-1,3-diol
Diethyl carbonate
3-hydroxymethyl-3-methyloxethane
Conditions | Yield |
---|---|
Erhitzen des Reaktionsprodukts unter vermindertem Druck bis auf 200grad; |
1,1,1-Trimethylolethane mononitrate
A
3-hydroxymethyl-3-methyloxethane
B
ethyl nitrate
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water at 55℃; for 21.9033h; Product distribution; Rate constant; var. NaOH conc.; |
3-methyl-3-(nitroxymethyl)oxetane
A
3-hydroxymethyl-3-methyloxethane
B
ethyl nitrate
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water at 55℃; for 11.38h; Product distribution; Rate constant; var. NaOH conc.; |
2-(hydroxymethyl)-2-methylpropane-1,3-diol
Diethyl carbonate
3-hydroxymethyl-3-methyloxethane
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol |
N-hexyl-3-methyloxetane-3-carboxamide
A
3-hydroxymethyl-3-methyloxethane
B
hexan-1-amine
Conditions | Yield |
---|---|
With [RuH(CO)(BPy-tPNN*)]; hydrogen In tetrahydrofuran at 110℃; under 7600.51 Torr; for 48h; Fischer-Porter tube; | A 74 %Chromat. B 74 %Chromat. |
2-(hydroxymethyl)-2-methylpropanedioic acid diethyl ester
3-hydroxymethyl-3-methyloxethane
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere 2.1: lithium borohydride / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere 3.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 °C 3.2: 1 h / Cooling with ice 3.3: 4.17 h / 0 - 60 °C 4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere 2.1: lithium borohydride / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere 3.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 °C 3.2: Cooling with ice 3.3: 4.17 h / 60 °C / Cooling with ice 4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C View Scheme |
diethyl 2-[(tert-butyldiphenylsilyloxy)methyl]-2-methylmalonate
3-hydroxymethyl-3-methyloxethane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: lithium borohydride / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 °C 2.2: 1 h / Cooling with ice 2.3: 4.17 h / 0 - 60 °C 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: lithium borohydride / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 °C 2.2: Cooling with ice 2.3: 4.17 h / 60 °C / Cooling with ice 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C View Scheme |
3-hydroxymethyl-3-methyloxethane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 °C 1.2: 1 h / Cooling with ice 1.3: 4.17 h / 0 - 60 °C 2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 °C 1.2: Cooling with ice 1.3: 4.17 h / 60 °C / Cooling with ice 2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C View Scheme |
3-hydroxymethyl-3-methyloxethane
4-nitro-benzoyl chloride
(3-methyloxetan-3-yl)methyl 4-nitrobenzoate
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 0.333333h; | 100% |
3-hydroxymethyl-3-methyloxethane
p-toluenesulfonyl chloride
(3-methyloxetan-3-yl)methyl 4-methylbenzenesulfonate
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; for 12h; Inert atmosphere; | 100% |
With pyridine for 1.5h; Inert atmosphere; Cooling with ice; | 96% |
With 1-methyl-1H-imidazole; triethylamine In dichloromethane at 25℃; for 2h; | 95% |
3-hydroxymethyl-3-methyloxethane
N-carbobenzyloxy-L-tryptophane
N-(benzyloxycarbonyl)-L-tryptophane (3-methyl-3-oxetanyl)methyl ester
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; | 100% |
With dmap; dicyclohexyl-carbodiimide In diethyl ether at 25℃; for 0.25h; | 84% |
3-hydroxymethyl-3-methyloxethane
2-amino-6-chloropyrazine
6-((3-methyloxetan-3-yl)methoxy)pyrazin-2-amine
Conditions | Yield |
---|---|
Stage #1: 3-hydroxymethyl-3-methyloxethane With sodium hydride In 1,4-dioxane; mineral oil at 20℃; for 2h; Stage #2: 2-amino-6-chloropyrazine for 16h; Reflux; | 100% |
Stage #1: 3-hydroxymethyl-3-methyloxethane With sodium hydride In 1,4-dioxane; mineral oil at 20℃; for 2h; Stage #2: 2-amino-6-chloropyrazine In 1,4-dioxane; mineral oil for 16h; Reflux; | 100% |
3-hydroxymethyl-3-methyloxethane
Conditions | Yield |
---|---|
With dipyridinium dichromate In N,N-dimethyl-formamide at 20℃; | 100% |
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene In water; acetonitrile at 20℃; | 14 g |
In water; acetonitrile at 20℃; Cooling with ice; | 14 g |
3-hydroxymethyl-3-methyloxethane
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; Inert atmosphere; | 100% |
3-hydroxymethyl-3-methyloxethane
3-bromomethyl-3-methyloxetane
Conditions | Yield |
---|---|
With carbon tetrabromide; triphenylphosphine In dichloromethane for 0.333333h; Ambient temperature; | 99% |
With carbon tetrabromide; triphenylphosphine In dichloromethane at 0 - 20℃; for 0.333333h; Product distribution / selectivity; | 95% |
With triphenyl phosphite; N-Bromosuccinimide In dichloromethane Ambient temperature; | 74% |
3-hydroxymethyl-3-methyloxethane
butyryl chloride
butyric acid 3-methyloxetan-3-ylmethyl ester
Conditions | Yield |
---|---|
With pyridine In dichloromethane | 99% |
3-hydroxymethyl-3-methyloxethane
4-Chlorobutanoyl chloride
3-methyl-3-oxetanylmethyl 4-chlorobutanoate
Conditions | Yield |
---|---|
With triethylamine In diethyl ether for 1h; Ambient temperature; | 98% |
With pyridine In dichloromethane at 0℃; for 48h; | 92% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; Inert atmosphere; | 98% |
3-hydroxymethyl-3-methyloxethane
7-bromoheptanoyl chloride
1-methyl-3-oxacyclobutanecarbinyl 7-bromoheptanoate
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0℃; for 1.5h; | 97% |
With pyridine In tetrahydrofuran at 5℃; for 1.5h; | 89% |
3-hydroxymethyl-3-methyloxethane
acetyl chloride
(3-Methyloxetan-3-yl)methyl acetate
Conditions | Yield |
---|---|
With pyridine In dichloromethane | 97% |
3-hydroxymethyl-3-methyloxethane
5-bromo-2,3-dimethoxybenzoic acid chloride
3-methyloxetane-3-methyl 2,3-dimethoxy-5-bromobenzoate
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; | 97% |
3-hydroxymethyl-3-methyloxethane
hex-5-ynoic acid
(3-methyloxyethan-3-yl)methyl-5-hexynoate
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0℃; for 1h; Cooling with ice; | 97% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 0.75h; |
3-hydroxymethyl-3-methyloxethane
phenyldimethylsilyl chloride
3-methyl-3-[(phenyldimethylsilyl)oxymethyl]oxetane
Conditions | Yield |
---|---|
Stage #1: 3-hydroxymethyl-3-methyloxethane With sodium hydride In tetrahydrofuran at 0 - 20℃; for 2h; Inert atmosphere; Stage #2: phenyldimethylsilyl chloride In tetrahydrofuran at 0 - 20℃; for 2h; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
With hydrogen bromide In tetrahydrofuran; water at 20℃; for 17.5h; Inert atmosphere; Cooling with ice; | 96.1% |
With hydrogen bromide In tetrahydrofuran at 0 - 20℃; for 5h; | 96% |
With hydrogen bromide In tetrahydrofuran at 0℃; for 4h; | 93.7% |
3-hydroxymethyl-3-methyloxethane
5-ketohexanoic acid
3-methyloxetan-3-yl-carbinyl 5-oxohexanoate
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 12h; | 96% |
3-hydroxymethyl-3-methyloxethane
tert-butyldimethylsilyl chloride
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 0 - 20℃; for 6h; | 96% |
With 1H-imidazole In N,N-dimethyl-formamide at 20 - 25℃; for 12h; | 84% |
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; for 1.5h; Inert atmosphere; | 96% |
3-hydroxymethyl-3-methyloxethane
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 0.25h; | 96% |
1,4-dioxane
3-hydroxymethyl-3-methyloxethane
hydrogen bromide
2-(bromomethyl)-2-methylpropane-1,3-diol
Conditions | Yield |
---|---|
In water for 3.5h; Inert atmosphere; Schlenk technique; Reflux; | 96% |
3-hydroxymethyl-3-methyloxethane
benzoic acid
(3-Methyloxetan-3-yl)methyl benzoate
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; Inert atmosphere; | 96% |
3-hydroxymethyl-3-methyloxethane
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 0.25h; Inert atmosphere; | 96% |
3-hydroxymethyl-3-methyloxethane
benzyloxyacetic acid
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 25℃; for 18h; Inert atmosphere; | 96% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; Inert atmosphere; | 94% |
3-hydroxymethyl-3-methyloxethane
4-(N-tert-butoxycarbonyl)aminobenzoic acid
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; Inert atmosphere; | 96% |
3-hydroxymethyl-3-methyloxethane
(Z)-3-iodoprop-2-enoic acid
(3-methyl-3-oxetanyl)methyl (Z)-3-iodo-2-propenoate
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; | 95% |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 1h; | 95% |
3-hydroxymethyl-3-methyloxethane
3-[(2,4,6-triisopropylphenyl)sulfenyl]propionic acid
(3-methyl-3-oxethanyl)methyl 3-[(2,4,6-triisopropylphenyl)sulfenyl]propionate
Conditions | Yield |
---|---|
With 1,1'-carbonyldiimidazole In dichloromethane at 20℃; for 36h; | 95% |
3-hydroxymethyl-3-methyloxethane
(S)-3-((tert-butyldimethylsilyl)oxy)-4,4-dimethyl-5-oxoheptanoic acid
(-)-(3S)-3-(tert-butyldimethylsilyloxy)-4,4-dimethyl-5-oxoheptanoic acid 3-methyloxetan-3-ylmethyl ester
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 1h; | 95% |
3-hydroxymethyl-3-methyloxethane
3-methyl-3-(nitroxymethyl)oxetane
Conditions | Yield |
---|---|
With carbon dioxide; dinitrogen pentoxide at 0℃; under 45004.5 - 60006 Torr; for 0.5h; Autoclave; | 95% |
Conditions | Yield |
---|---|
at 150℃; for 48h; | 95% |
at 150℃; for 48h; | 95% |
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