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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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Benzeneethanamine,2-nitro-Appearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
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2-nitro-benzeneacetonitrile
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
Stage #1: 2-nitro-benzeneacetonitrile With dimethylsulfide borane complex In tetrahydrofuran at 0℃; for 8h; Heating / reflux; Stage #2: With methanol for 1h; Heating / reflux; | 100% |
With borane-THF at 0 - 20℃; Inert atmosphere; | 82% |
With dimethylsulfide borane complex In tetrahydrofuran at 0 - 70℃; for 8h; Inert atmosphere; | 82% |
With borane-THF |
3-(2-nitrophenyl)propionic acid
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
With hydrogen azide; chloroform; sulfuric acid |
N-(2-nitro-phenethyl)-acetamide
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
With hydrogen bromide |
phenethylamine
A
2-(p-nitrophenyl)ethylamine
B
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid |
(2-bromoethyl)-2-nitrobenzene
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
(i) aq. NaN3, DMSO, (ii) Ph3P, benzene, (iii) aq. HBr, AcOH; Multistep reaction; | |
Stage #1: (2-bromoethyl)-2-nitrobenzene With sodium azide In water; acetonitrile for 20h; Heating / reflux; Stage #2: With triphenylphosphine In toluene at 20℃; for 16h; Stage #3: With sodium hydroxide; hydrogen bromide; acetic acid more than 3 stages; |
2-(2-nitrophenyl)acetamide
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
With borane In 1,4-dioxane | |
With borane |
2-nitro-benzeneethanol
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
With dmap; trifluoromethylsulfonic anhydride; ammonia 1.) CH2Cl2, from -30 deg C to RT, 2.) THF, from -30 deg C to RT; Multistep reaction; | |
Multi-step reaction with 2 steps 1: aq. HBr 2: (i) aq. NaN3, DMSO, (ii) Ph3P, benzene, (iii) aq. HBr, AcOH View Scheme |
phenethylamine
A
2-(p-nitrophenyl)ethylamine
B
2-(2-aminoethyl)nitrobenzene
nitric acid
phenethylamine
A
2-(p-nitrophenyl)ethylamine
B
2-(2-aminoethyl)nitrobenzene
C
2-(3-nitrophenyl)ethylamine
Conditions | Yield |
---|---|
at -10℃; |
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
With potassium hydroxide at 80 - 90℃; |
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
at 80 - 90℃; |
methyl-N-(benzyl-methyl)-formamide
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: nitric acid / 0 °C 2: hydrobromic acid View Scheme |
phenethylamine
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 210 - 220 °C / durch Erhitzen zuletzt auf 290grad 2: nitric acid / 0 °C 3: hydrobromic acid View Scheme |
ethyl 2-nitrophenylacetate
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: NaBH4, AlCl3 2: aq. HBr 3: (i) aq. NaN3, DMSO, (ii) Ph3P, benzene, (iii) aq. HBr, AcOH View Scheme |
2-nitrophenethyl azide
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
Stage #1: 2-nitrophenethyl azide With triphenylphosphine; calcium carbonate In benzene at 20℃; Stage #2: With hydrogen bromide In water; acetic acid at 100℃; for 1h; | |
Stage #1: 2-nitrophenethyl azide With triphenylphosphine; calcium carbonate In benzene at 20℃; Stage #2: With hydrogen bromide; acetic acid In water at 100℃; for 1h; Stage #3: With sodium hydroxide In water | |
Stage #1: 2-nitrophenethyl azide With triphenylphosphine; calcium carbonate In benzene at 20℃; Stage #2: With hydrogen bromide; acetic acid In water at 100℃; for 1h; Stage #3: With sodium hydroxide In water |
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
With sodium hydroxide; water | |
With sodium hydroxide In tetrahydrofuran; water pH=8 - 9; |
phenylacetonitrile
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: nitric acid; acetic acid / 0 - 40 °C 2: dimethylsulfide borane complex / tetrahydrofuran / 8 h / 0 - 70 °C / Inert atmosphere View Scheme |
2-(2-aminoethyl)nitrobenzene
β-(o-aminophenyl)ethylamine
Conditions | Yield |
---|---|
With hydrogen; palladium 10% on activated carbon In ethanol under 2068.65 Torr; for 18h; | 99% |
With palladium 10% on activated carbon; hydrogen In ethanol at 20℃; under 2280.15 Torr; | 99% |
With phosphorus; hydrogen iodide | |
With ethanol; nickel Hydrogenation; | |
With hydrogen; palladium 10% on activated carbon In methanol for 18.0833h; |
di-tert-butyl dicarbonate
2-(2-aminoethyl)nitrobenzene
[2-(2-nitrophenyl)ethyl]carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In 1,4-dioxane; water at 0 - 20℃; | 92% |
2-(2-aminoethyl)nitrobenzene
propyl N-cyano-3-pyridinecarboximidate
Conditions | Yield |
---|---|
In methanol Ambient temperature; | 64% |
2-(2-aminoethyl)nitrobenzene
1,4-dihydrocinnoline
Conditions | Yield |
---|---|
With acetate buffer; acetic acid In methanol; water redox electrolysis; | 45% |
2-(2-aminoethyl)nitrobenzene
ortho-nitrobenzoic acid
Conditions | Yield |
---|---|
bei der Oxydation; |
2-(2-aminoethyl)nitrobenzene
2-amino-N-methylbenzylamine
Conditions | Yield |
---|---|
With hydrogenchloride; tin | |
With phosphorus; hydrogen iodide |
2-(2-aminoethyl)nitrobenzene
benzenesulfonyl chloride
N-Benzolsulfonyl-2-(2-nitrophenyl)-ethylamin
Conditions | Yield |
---|---|
With pyridine |
2-(2-aminoethyl)nitrobenzene
methylamine
methyl-(2-nitro-phenethyl)-amine
Conditions | Yield |
---|---|
In acetonitrile |
2-(2-aminoethyl)nitrobenzene
(R)-Pantolacton
2-(2-aminoethyl)nitrobenzene
N-(2-nitro-phenethyl)-acetamide
Conditions | Yield |
---|---|
With acetylation reagent |
2-(2-aminoethyl)nitrobenzene
N-(thiazol-2-yl)-1H-imidazole-1-carbothioamide
Conditions | Yield |
---|---|
In acetonitrile at 100℃; for 1h; |
2-(2-aminoethyl)nitrobenzene
4-<5-(acetamidomethyl)furan-2-yl>-2-<<(2-nitrophenyl)ethyl>guanidino>thiazole
Conditions | Yield |
---|---|
In ethanol for 72h; Heating; Yield given; |
2-(2-aminoethyl)nitrobenzene
4-<5-(acetamidomethyl)furan-2-yl>-2-<<(2-aminophenyl)ethyl>guanidino>thiazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ethanol / 72 h / Heating 2: 73 percent / H2 / 10 percent Pd/C / methanol / 760 Torr / Ambient temperature View Scheme |
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: ethanol / 72 h / Heating 2: 73 percent / H2 / 10 percent Pd/C / methanol / 760 Torr / Ambient temperature 3: 57 percent / Et3N / CH2Cl2; dimethylformamide / 1 h / Ambient temperature View Scheme |
2-(2-aminoethyl)nitrobenzene
N-[2-(2-aminophenyl)ethyl]acetamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: acetylation reagent 2: reduction View Scheme |
2-(2-aminoethyl)nitrobenzene
o-ethoxycarbonylimino-N-acetylphenethylamine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: acetylation reagent 2: reduction View Scheme |
2-(2-aminoethyl)nitrobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Raney nickel; ethanol / Hydrogenation View Scheme |
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