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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis

15-Crown-5

Cas:33100-27-5

Min.Order:1 Kilogram

FOB Price: $4.0

Type:Lab/Research institutions

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Chemlyte Solutions

Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff

Featured products 15-Crown-5(33100-27-5)

Cas:33100-27-5

Min.Order:100 Gram

Negotiable

Type:Other

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Wuhan Shengmao Corp

High Purity Appearance:Colorless and transparent viscous liquid Application:High-efficiency phase transfer catalyst; complexing agent

15-crown ether-5

Cas:33100-27-5

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

15-Crown-5

Cas:33100-27-5

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 15-Crown-5(1,4,7,10,13-Pentaoxacyclopentadecane) supplier in China

Cas:33100-27-5

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Hangzhou Dingyan Chem Co., Ltd

Items Standard Result Appearance Colorless to light yellow transparent liquid Conforms Assay

High purity 15-Crown-5-ether CAS:33100-27-5

Cas:33100-27-5

Min.Order:1 Gram

FOB Price: $100.0 / 500.0

Type:Manufacturers

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Hefei TNJ chemical industry co.,ltd

Product Product name 15-Crown-5 Synonyms 1,4,7,10,13-Pentaoxacyclopentadecane; Lead ionophore V CAS No.

15-Crown-5

Cas:33100-27-5

Min.Order:3 Metric Ton

Negotiable

Type:Trading Company

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Jinan Finer Chemical Co., Ltd

Product description: Product name 15-Crown-5 CAS number 33100-27-5 Assay ≥99% Appearance Colorless liquid Capacity 200mt/year Application Phase transfer catalysts used in or

15-Crown-5

Cas:33100-27-5

Min.Order:10 Gram

FOB Price: $12.0

Type:Lab/Research institutions

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Henan Allgreen Chemical Co.,Ltd

Good quality Good price Promptly delivery Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:intermediate Transportation:According to the demand o

33100-27-515-Crown-5

Cas:33100-27-5

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Chemwill Asia Co., Ltd.

15-Crown-5 Manufacturer Factory CAS 33100-27-5 15-Crown-5 Manufacturer High quality Best price In stock factory CAS 33100-27-5 15-Crown-5 COA TDS price MSDS highly quality and immedaite delivery 15-Crown-5 Chemical Properties Melting poi

15-Crown-5 Manufacturer Factory CAS 33100-27-5

Cas:33100-27-5

Min.Order:5 Kiloliter

FOB Price: $3.5 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

15-Crown-5 Basic information Product Name: 15-Crown-5 Synonyms: 1,4,10,13-Pentaoxacyclopentadecane;15-Crown-5,1,4,7,10,13-Pentaoxa-cyclo-pentadecane;Crownethers;Eth

TIANFU-CHEM 15-Crown-5 33100-27-5

Cas:33100-27-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

15-Crown-5

Cas:33100-27-5

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

New CAS 33100-27-5 with best quality

Cas:33100-27-5

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

Type:Trading Company

inquiry

Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developmen

15-crown ether-5 CAS NO.33100-27-5

Cas:33100-27-5

Min.Order:20 Kilogram

FOB Price: $10.0 / 100.0

Type:Trading Company

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after the dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available &diam

15-Crown-5 CAS33100-27-5

Cas:33100-27-5

Min.Order:1 Kilogram

FOB Price: $7.0 / 10.0

Type:Trading Company

inquiry

Henan Sinotech Import&Export Corporation

Chemical Name 15-Crown-5 Synonyms 1,4,7,10,13-Pentaoxacyclopentadecane; Lead ionophore V CAS No. 33100-27-5 Molecular formula C10H20O5

1,4,7,10,13-Pentaoxacyclopentadecane

Cas:33100-27-5

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

15-Crown-5 33100-27-5

Cas:33100-27-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Lower price 15-Crown-5 CAS33100-27-5

Cas:33100-27-5

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

15-Crown-5

Cas:33100-27-5

Min.Order:1 Kilogram

FOB Price: $85.0 / 100.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

15-Crown-5 CAS: 33100-27-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates

15-Crown-5 CAS: 33100-27-5

Cas:33100-27-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

15-Crown-5

Cas:33100-27-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Changchun Artel lmport and Export trade company

Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,

15-Crown-5 supplier in China CAS NO.33100-27-5

Cas:33100-27-5

Min.Order:10 Gram

Negotiable

Type:Trading Company

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:33100-27-5

Cas:33100-27-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fandachem Co.,Ltd

Hangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting 15-Crown-5 cas 33100-27-5 ;Please contact us by email freely. We are leading exporter in China. If you really need this cargo, pleas

15-Crown-5 cas 33100-27-5 from Fandachem

Cas:33100-27-5

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

15-Crown-5(1,4,7,10,13-Pentaoxacyclopentadecane)

Cas:33100-27-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

15-Crown-5

Cas:33100-27-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

15-Crown-5

Cas:33100-27-5

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 15-Crown-5

Cas:33100-27-5

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 15-Crown-5

Cas:33100-27-5

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

15-Crown-5

Cas:33100-27-5

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

Synthetic route

1,4,7,10,13-pentaoxacyclopentadecane-2,6-dione
63689-58-7

1,4,7,10,13-pentaoxacyclopentadecane-2,6-dione

15-crown-5
33100-27-5

15-crown-5

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 1.5h;79%
Pentaethylene glycol
4792-15-8

Pentaethylene glycol

15-crown-5
33100-27-5

15-crown-5

Conditions
ConditionsYield
With sodium hydroxide; p-toluenesulfonyl chloride In 1,4-dioxane at 80℃;75%
With sodium hydroxide; p-toluenesulfonyl chloride In 1,2-dimethoxyethane at 0℃; Product distribution; var. solvents, reagents, and temp.; other oligoethylene glycols;36 % Chromat.
Tetraethylene glycol
112-60-7

Tetraethylene glycol

ethylene glycol
107-21-1

ethylene glycol

15-crown-5
33100-27-5

15-crown-5

Conditions
ConditionsYield
With sodium carbonate; dicyclohexyl-carbodiimide In 1,4-dioxane at 70 - 75℃; for 6h; Concentration; Reagent/catalyst; Temperature; Solvent;70.2%
3-oxa-1,5-dichloropentane
111-44-4

3-oxa-1,5-dichloropentane

2,2'-[1,2-ethanediylbis(oxy)]bisethanol
112-27-6

2,2'-[1,2-ethanediylbis(oxy)]bisethanol

15-crown-5
33100-27-5

15-crown-5

Conditions
ConditionsYield
With sodium methylate In 1,4-dioxane for 24h; Heating; metal hydroxides, different bases as 'template' agents;66%
With sodium methylate In 1,4-dioxane for 24h; Heating;66%
1,4,7,10,13-Pentaoxacyclopentadecane-2,3-dithione
86309-76-4

1,4,7,10,13-Pentaoxacyclopentadecane-2,3-dithione

15-crown-5
33100-27-5

15-crown-5

Conditions
ConditionsYield
With nickel In diethyl ether; dichloromethane at 0℃; for 1h;52%
Pentaethylene glycol
4792-15-8

Pentaethylene glycol

A

15-crown-5
33100-27-5

15-crown-5

B

<60>crown-20
71092-63-2

<60>crown-20

C

<30>crown-10
52985-64-5

<30>crown-10

D

45-Crown-15
109635-67-8

45-Crown-15

Conditions
ConditionsYield
With potassium hydroxide; p-toluenesulfonyl chloride In 1,4-dioxane at 65℃;A 46%
B 0.7%
C 12%
D 3.4%
Pentaethylene glycol
4792-15-8

Pentaethylene glycol

A

15-crown-5
33100-27-5

15-crown-5

B

<30>crown-10
52985-64-5

<30>crown-10

C

45-Crown-15
109635-67-8

45-Crown-15

Conditions
ConditionsYield
With potassium hydroxide; p-toluenesulfonyl chloride In 1,4-dioxane at 65℃;A 46%
B 12%
C 3.4%
1,2-bis(2-chloroethoxy)ethane
112-26-5

1,2-bis(2-chloroethoxy)ethane

diethylene glycol
111-46-6

diethylene glycol

15-crown-5
33100-27-5

15-crown-5

Conditions
ConditionsYield
With potassium hydroxide for 0.133333h; microwave irradiation;40%
diethylene glycol ditosylate
7460-82-4

diethylene glycol ditosylate

2,2'-[1,2-ethanediylbis(oxy)]bisethanol
112-27-6

2,2'-[1,2-ethanediylbis(oxy)]bisethanol

15-crown-5
33100-27-5

15-crown-5

Conditions
ConditionsYield
With aluminum oxide; potassium fluoride In acetonitrile for 24h; Ambient temperature;25%
18-crown-6 ether
17455-13-9

18-crown-6 ether

C14H14Mg*C10H20O5

C14H14Mg*C10H20O5

A

15-crown-5
33100-27-5

15-crown-5

B

C14H14Mg*C12H24O6

C14H14Mg*C12H24O6

Conditions
ConditionsYield
In benzene at 25℃; Equilibrium constant;
complex of 15-crown-5 with K+
61060-13-7

complex of 15-crown-5 with K+

15-crown-5
33100-27-5

15-crown-5

Conditions
ConditionsYield
In methanol at 25℃; Equilibrium constant;
In acetone at 25℃; Equilibrium constant; complexation of alkali metal cations (Li+, Na+, K+, Rb+, Cs+) with crown ethers, diaza crown ethers and cryptands in acetone, stability constants of complexes formed; influence of ion-pair formation on stability constants;
complex of 15-crown-5 with Na+
59890-71-0

complex of 15-crown-5 with Na+

15-crown-5
33100-27-5

15-crown-5

Conditions
ConditionsYield
In methanol at 25℃; Equilibrium constant;
complex of 15-crown-5 with Na+
59890-71-0

complex of 15-crown-5 with Na+

A

15-crown-5
33100-27-5

15-crown-5

B

sodium cation
17341-25-2

sodium cation

Conditions
ConditionsYield
In methanol; water at 25℃; Equilibrium constant; var. MeOH/H2O ratio;
C10H20O5*C6H2N3O7(1-)*K(1+)

C10H20O5*C6H2N3O7(1-)*K(1+)

A

15-crown-5
33100-27-5

15-crown-5

B

potassium picrate
573-83-1

potassium picrate

Conditions
ConditionsYield
In dichloromethane; water at 25℃; for 0.666667h; Equilibrium constant;
C10H20O5*C6H2N3O7(1-)*Cs(1+)

C10H20O5*C6H2N3O7(1-)*Cs(1+)

A

15-crown-5
33100-27-5

15-crown-5

B

cesium picrate
3638-61-7

cesium picrate

Conditions
ConditionsYield
In dichloromethane; water at 25℃; for 0.666667h; Equilibrium constant;
C10H20O5*C6H2N3O7(1-)*Na(1+)

C10H20O5*C6H2N3O7(1-)*Na(1+)

A

15-crown-5
33100-27-5

15-crown-5

B

sodium picrate
3324-58-1

sodium picrate

Conditions
ConditionsYield
In dichloromethane; water at 25℃; for 0.666667h; Equilibrium constant;
C10H20O5*C6H2N3O7(1-)*Rb(1+)

C10H20O5*C6H2N3O7(1-)*Rb(1+)

A

15-crown-5
33100-27-5

15-crown-5

B

rubidium picrate
23296-29-9

rubidium picrate

Conditions
ConditionsYield
In dichloromethane; water at 25℃; for 0.666667h; Equilibrium constant;
C10H20O5*C7H7N2(1+)*BF4(1-)

C10H20O5*C7H7N2(1+)*BF4(1-)

A

15-crown-5
33100-27-5

15-crown-5

B

2-methylchlorobenzene
95-49-8

2-methylchlorobenzene

Conditions
ConditionsYield
In 1,2-dichloro-ethane at 20℃; Rate constant; Kinetics; Thermodynamic data; var. crown ethers, ΔH(excit.), ΔS(excit.);
C10H20O5*C8H9N2(1+)*BF4(1-)

C10H20O5*C8H9N2(1+)*BF4(1-)

A

15-crown-5
33100-27-5

15-crown-5

B

1-chloro-2-ethylbenzene
89-96-3

1-chloro-2-ethylbenzene

Conditions
ConditionsYield
In 1,2-dichloro-ethane at 20℃; Rate constant; Kinetics; Thermodynamic data; var. crown ethers, ΔH(excit.), ΔS(excit.);
o-acetylbenzenediazonium tetrafluoroborate

o-acetylbenzenediazonium tetrafluoroborate

A

15-crown-5
33100-27-5

15-crown-5

B

1-(2-chlorophenyl)ethanone
2142-68-9

1-(2-chlorophenyl)ethanone

Conditions
ConditionsYield
In 1,2-dichloro-ethane at 20℃; Rate constant; Kinetics; Thermodynamic data; var. crown ethers, ΔH(excit.), ΔS(excit.);
C10H20O5*C3H9N*H(1+)

C10H20O5*C3H9N*H(1+)

A

15-crown-5
33100-27-5

15-crown-5

B

trimethylammonium
145384-53-8

trimethylammonium

Conditions
ConditionsYield
Thermodynamic data; enthalpy and entropy changes for the complex dissociation reaction: ΔH0D, ΔS0D;
C10H20O5*C6H13N*H(1+)

C10H20O5*C6H13N*H(1+)

A

cyclohexyl-ammonium cation
29384-28-9

cyclohexyl-ammonium cation

B

15-crown-5
33100-27-5

15-crown-5

Conditions
ConditionsYield
Thermodynamic data; enthalpy and entropy changes for the complex dissociation reaction: ΔH0D, ΔS0D;
C10H20O5*C5H5N*H(1+)

C10H20O5*C5H5N*H(1+)

A

pyridin-1-ium
16969-45-2

pyridin-1-ium

B

15-crown-5
33100-27-5

15-crown-5

Conditions
ConditionsYield
Thermodynamic data; enthalpy and entropy changes for the complex dissociation reaction: ΔH0D, ΔS0D;
triethylene glycol di-(p-toluenesulfonate)
19249-03-7

triethylene glycol di-(p-toluenesulfonate)

diethylene glycol
111-46-6

diethylene glycol

15-crown-5
33100-27-5

15-crown-5

Conditions
ConditionsYield
With aluminum oxide; potassium fluoride In acetonitrile for 24h; Ambient temperature;33 % Chromat.
C10H20O5*ClO4(1-)*Li(1+)

C10H20O5*ClO4(1-)*Li(1+)

15-crown-5
33100-27-5

15-crown-5

Conditions
ConditionsYield
In acetone Equilibrium constant; various solvents (MeNO2, MeCN, propylene carbonate, MeOH, pyridine), complex formation between crown ethers and lithim ion, effect of solvent of the stability of complexes, 7Li NMR study;
In acetone Equilibrium constant; various solvents (MeNO2, MeCN, MeOh H2O etc.), complex formation between crown ethers and lithim ion, effect of solvent of the stability of complexes;
1,4,7,10,13-Pentaoxa-cyclopentadecane; compound with GENERIC INORGANIC NEUTRAL COMPONENT

1,4,7,10,13-Pentaoxa-cyclopentadecane; compound with GENERIC INORGANIC NEUTRAL COMPONENT

15-crown-5
33100-27-5

15-crown-5

Conditions
ConditionsYield
With Iodine monochloride In benzene at 24.9℃; Equilibrium constant;
complex of 15-crown-5 with K+
61060-13-7

complex of 15-crown-5 with K+

cryptand 211
31250-06-3

cryptand 211

A

15-crown-5
33100-27-5

15-crown-5

B

C14H28N2O4*K(1+)

C14H28N2O4*K(1+)

Conditions
ConditionsYield
In gas at 76.9℃; Equilibrium constant; Thermodynamic data; ΔG0;
complex of 15-crown-5 with Na+
59890-71-0

complex of 15-crown-5 with Na+

cryptand 211
31250-06-3

cryptand 211

A

15-crown-5
33100-27-5

15-crown-5

B

C14H28N2O4*Na(1+)

C14H28N2O4*Na(1+)

Conditions
ConditionsYield
In gas at 76.9℃; Equilibrium constant; Thermodynamic data; ΔG0;
C10H20O5*Li(1+)
74060-72-3

C10H20O5*Li(1+)

cryptand 211
31250-06-3

cryptand 211

A

15-crown-5
33100-27-5

15-crown-5

B

C14H28N2O4*Li(1+)

C14H28N2O4*Li(1+)

Conditions
ConditionsYield
In gas at 76.9℃; Equilibrium constant; Thermodynamic data; ΔG0;
15-crown-5
33100-27-5

15-crown-5

[W(carbonyl)5([bis(trimethylsilyl)methyl]cyanophosphane)]
851576-85-7

[W(carbonyl)5([bis(trimethylsilyl)methyl]cyanophosphane)]

sodium hexamethyldisilazane
1070-89-9

sodium hexamethyldisilazane

[(OC)5WP(CH(SiMe3)2)CNNa(15-crown-5)]
947333-62-2

[(OC)5WP(CH(SiMe3)2)CNNa(15-crown-5)]

Conditions
ConditionsYield
In tetrahydrofuran under Ar; cooled (-80°C) soln. of NaN(SiMe3)2 in THF added dropwise to stirred soln. of W complex in THF and 15-crown-5; warmed slowly toroom temp. for 3.5 h; solvent removed under vac.; washed with Et2O and n-pentane; dried under reduced pressure; elem. anal.;100%
15-crown-5
33100-27-5

15-crown-5

Br(1-)*C10H20NaO5

Br(1-)*C10H20NaO5

Conditions
ConditionsYield
With sodium bromide In water at 20℃; for 12h;100%
15-crown-5
33100-27-5

15-crown-5

C10H20NaO5*HO(1-)

C10H20NaO5*HO(1-)

Conditions
ConditionsYield
With sodium hydroxide In water at 20℃; for 12h;100%
15-crown-5
33100-27-5

15-crown-5

C10H20NaO5*IO3(1-)

C10H20NaO5*IO3(1-)

Conditions
ConditionsYield
With sodium iodate In water at 20℃; for 12h;100%
15-crown-5
33100-27-5

15-crown-5

sodium acetate
127-09-3

sodium acetate

C2H3O2(1-)*C10H20NaO5

C2H3O2(1-)*C10H20NaO5

Conditions
ConditionsYield
In water at 20℃; for 12h;100%
15-crown-5
33100-27-5

15-crown-5

sodium oxalate
62-76-0

sodium oxalate

C2O4(2-)*2C10H20NaO5

C2O4(2-)*2C10H20NaO5

Conditions
ConditionsYield
In water at 20℃; for 12h;100%
15-crown-5
33100-27-5

15-crown-5

potassium hydrogen phthalate
877-24-7

potassium hydrogen phthalate

C8H5O4(1-)*C12H24KO6

C8H5O4(1-)*C12H24KO6

Conditions
ConditionsYield
In water at 20℃; for 12h;100%
15-crown-5
33100-27-5

15-crown-5

sodium chloride
7647-14-5

sodium chloride

zinc(II) chloride
7646-85-7

zinc(II) chloride

C10H20NaO5(1+)*Cl3Zn(1-)

C10H20NaO5(1+)*Cl3Zn(1-)

Conditions
ConditionsYield
Stage #1: 15-crown-5; sodium chloride In water at 20℃; for 12h;
Stage #2: zinc(II) chloride In ethanol for 12h; Reflux;
100%
15-crown-5
33100-27-5

15-crown-5

iron(III) chloride hexahydrate

iron(III) chloride hexahydrate

sodium chloride
7647-14-5

sodium chloride

Cl4Fe(1-)*C10H20NaO5(1+)

Cl4Fe(1-)*C10H20NaO5(1+)

Conditions
ConditionsYield
Stage #1: 15-crown-5; sodium chloride In water at 20℃; for 12h;
Stage #2: iron(III) chloride hexahydrate In ethanol for 12h; Reflux;
100%
hydrogenchloride
7647-01-0

hydrogenchloride

15-crown-5
33100-27-5

15-crown-5

uranyl acetate dihydrate

uranyl acetate dihydrate

sodium acetate
127-09-3

sodium acetate

2Na(1+)*2(CH2)10O5*UO2Cl4(2-)=[Na(CH2)10O5]2UO2Cl4

2Na(1+)*2(CH2)10O5*UO2Cl4(2-)=[Na(CH2)10O5]2UO2Cl4

Conditions
ConditionsYield
In water UO2OAc2*2H2O, NaCH3COO, ligand and HCl were combined in water with stirring, evapd. slowly at room temp. for 1 wks; isolated; elem. anal.;99.9%
15-crown-5
33100-27-5

15-crown-5

[NaU(bis(trimethylsilyl)amide)(CH2SiMe2N(SiMe3))2]
1242245-34-6

[NaU(bis(trimethylsilyl)amide)(CH2SiMe2N(SiMe3))2]

[Na(15-crown-5)][U(bis(trimethylsilyl)amide)(CH2SiMe2N(SiMe3))2]

[Na(15-crown-5)][U(bis(trimethylsilyl)amide)(CH2SiMe2N(SiMe3))2]

Conditions
ConditionsYield
In pentane under Ar; a NMR tube was charged with U-contg. compd. (0.027 mmol) in pentane, and 15-crown-5 (0.032 mmol) was added; the suspn. was heated for 3 d at 60°C; elem. anal.;99%
15-crown-5
33100-27-5

15-crown-5

1,1,1-trimethyl-2,2,2-triphenyldisilane
1450-18-6

1,1,1-trimethyl-2,2,2-triphenyldisilane

[Na(15-crown-5)SiPh3]·(thf )0.5

[Na(15-crown-5)SiPh3]·(thf )0.5

Conditions
ConditionsYield
With sodium t-butanolate In tetrahydrofuran at 20℃; for 2h; Inert atmosphere; Schlenk technique;99%
sodium amalgam

sodium amalgam

15-crown-5
33100-27-5

15-crown-5

C60H51B3N12(1-)

C60H51B3N12(1-)

C60H51B3N12(1-)*C10H20NaO5(1+)

C60H51B3N12(1-)*C10H20NaO5(1+)

Conditions
ConditionsYield
In tetrahydrofuran; hexane99%
15-crown-5
33100-27-5

15-crown-5

zirconium(IV) chloride
10026-11-6

zirconium(IV) chloride

sodium fluoride

sodium fluoride

{Na-15-crown-5}2-cis-{ZrF2Cl4}

{Na-15-crown-5}2-cis-{ZrF2Cl4}

Conditions
ConditionsYield
In acetonitrile soln. of ZrCl4 and 15-crown-5 prepared under cooling; addn. of NaF; stirred for 12 h at 25°C; filtration; solvent removed until beginning of crystn.; cooled down to 5°C; crystn.; filtration; washed (cold acetonitrile); dried under vac.; elem. anal.; IR;98.3%
15-crown-5
33100-27-5

15-crown-5

niobium pentachloride

niobium pentachloride

(NbCl4)2(15-crown-5)

(NbCl4)2(15-crown-5)

Conditions
ConditionsYield
In tetrachloromethane Ar-atmosphere; room temp.; elem. anal.;98%
15-crown-5
33100-27-5

15-crown-5

Na[U(N(SiMe3)2)(OC(=CH2)SiMe2NSiMe3)2(N3)]
1331740-29-4

Na[U(N(SiMe3)2)(OC(=CH2)SiMe2NSiMe3)2(N3)]

pentane
109-66-0

pentane

Na(C10H20O5)[U(N3)(NSi2C6H18)(COCH2Si(CH3)2N(Si(CH3)3))2]*0.5C5H12

Na(C10H20O5)[U(N3)(NSi2C6H18)(COCH2Si(CH3)2N(Si(CH3)3))2]*0.5C5H12

Conditions
ConditionsYield
In pentane Ar; U compd. and ligand (1:1 molar ratio), stirred for 12 at 20°C; filtered, evapd., elem. anal.;98%
iron(II) bis(trimethylsilyl)amide
14760-22-6

iron(II) bis(trimethylsilyl)amide

15-crown-5
33100-27-5

15-crown-5

sodium hexamethyldisilazane
1070-89-9

sodium hexamethyldisilazane

[Na(15-crown-5)2]+[Fe(N{SiMe3}2)3]−

[Na(15-crown-5)2]+[Fe(N{SiMe3}2)3]−

Conditions
ConditionsYield
Stage #1: iron(II) bis(trimethylsilyl)amide; sodium hexamethyldisilazane In toluene for 1h; Reflux; Inert atmosphere; Glovebox; Schlenk technique;
Stage #2: 15-crown-5 In toluene for 1h; Reflux; Inert atmosphere; Glovebox; Schlenk technique;
97.74%
15-crown-5
33100-27-5

15-crown-5

dihydroxy-anthraquinone-C60

dihydroxy-anthraquinone-C60

bis(sodium-15-crown-5)dioxoanthraquinone-C60

bis(sodium-15-crown-5)dioxoanthraquinone-C60

Conditions
ConditionsYield
With sodium t-butanolate In tetrahydrofuran; toluene Ambient temperature;97%
ammonium dichromate(VI)

ammonium dichromate(VI)

15-crown-5
33100-27-5

15-crown-5

NH4CrO3Cl(15-crown-5)2

NH4CrO3Cl(15-crown-5)2

Conditions
ConditionsYield
With hydrogenchloride In water addn. of org. ligand to soln. of ammonium dichromate and concd. hydrochloric acid (stirring, 20°C); ppt. filtered off, washed (water) and dried at 40-50°C; elem. anal.;97%
15-crown-5
33100-27-5

15-crown-5

Ni(1,3-imidazolidinyl-N,N'-bis(benzene-2-thiolate)2) * DMF

Ni(1,3-imidazolidinyl-N,N'-bis(benzene-2-thiolate)2) * DMF

sodium thiophenolate
930-69-8

sodium thiophenolate

[Na(1,4,7,10,13-pentaoxacyclopentadecane)][Ni(SPh)(1,3-imidazolidinyl-N,N'-bis(benzene-2-thiolate))]

[Na(1,4,7,10,13-pentaoxacyclopentadecane)][Ni(SPh)(1,3-imidazolidinyl-N,N'-bis(benzene-2-thiolate))]

Conditions
ConditionsYield
In tetrahydrofuran N2-atmosphere; mixing Ni-complex with excess NaSPh, addn. of MeOH, stirring for 1 d, filtration, addn. of excess of crown; crystn. (-30°C, 3 d), collection (filtration), washing (THF, hexane), drying (vac., 2 h); elem. anal.;97%
2,6-dimesitylphenyl-trifluorosilane

2,6-dimesitylphenyl-trifluorosilane

15-crown-5
33100-27-5

15-crown-5

C10H20O5*C24H25F4Si(1-)*Na(1+)
1195787-45-1

C10H20O5*C24H25F4Si(1-)*Na(1+)

Conditions
ConditionsYield
With sodium fluoride In toluene for 648h; Inert atmosphere;97%
tin(II) trifluoromethanesulfonate

tin(II) trifluoromethanesulfonate

15-crown-5
33100-27-5

15-crown-5

[tin(II)([15]crown-5)2](trifluoromethanesulfonate)2

[tin(II)([15]crown-5)2](trifluoromethanesulfonate)2

Conditions
ConditionsYield
In tetrahydrofuran standard inert-atmosphere techniques; soln. of (15)crown-5 (0.972 mmol) added to soln. of Sn(OTf)2 (0.480 mmol), stiired for 2 h; solvent removed (in vac.), washed with pentane; elem. anal.;97%
15-crown-5
33100-27-5

15-crown-5

magnesium bis(tetrahydroborate) tris(tetrahydrofuran)

magnesium bis(tetrahydroborate) tris(tetrahydrofuran)

magnesium bis(tetrahydroborate) bis(15-crown-5)

magnesium bis(tetrahydroborate) bis(15-crown-5)

Conditions
ConditionsYield
In tetrahydrofuran96.1%
In tetrahydrofuran byproducts: THF; under N2 15-crown-5 was added dropwise to THF soln. of Mg-compd.; ppt. was centrifuged off, dried in vac., elem. anal.;96.1%
15-crown-5
33100-27-5

15-crown-5

MoF4(NCl)
113236-05-8

MoF4(NCl)

sodium fluoride

sodium fluoride

sodium-15-crown-5-pentafluoro-N-chloronitreno-molybdate(IV)

sodium-15-crown-5-pentafluoro-N-chloronitreno-molybdate(IV)

Conditions
ConditionsYield
In acetonitrile stirring (room temp., 2 h); crystn. on cooling (-18°C), sepn. (filtration off), washing (acetonitrile), drying (vac.); elem. anal.;96%
15-crown-5
33100-27-5

15-crown-5

niobium pentachloride

niobium pentachloride

(NbCl4)3(15-crown-5)

(NbCl4)3(15-crown-5)

Conditions
ConditionsYield
In tetrachloromethane Ar-atmosphere; molar ratio Nb2Cl10:crown=1:2, room temp.; elem. anal.;96%
2-(3-methoxymethoxyphenyl)butane-1,2-diol
131481-05-5

2-(3-methoxymethoxyphenyl)butane-1,2-diol

15-crown-5
33100-27-5

15-crown-5

methyl iodide
74-88-4

methyl iodide

2-methoxy-2-(3-methoxymethoxyphenyl)but-1-yl methyl ether
131480-48-3

2-methoxy-2-(3-methoxymethoxyphenyl)but-1-yl methyl ether

Conditions
ConditionsYield
In N-methyl-acetamide; mineral oil95%
15-crown-5
33100-27-5

15-crown-5

2Mo(6+)*2(N3S2)(3-)*6Cl(1-)={MoCl3(N3S2)}2

2Mo(6+)*2(N3S2)(3-)*6Cl(1-)={MoCl3(N3S2)}2

sodium fluoride

sodium fluoride

{Na-15-crown-5}{MoF2Cl2(N3S2)}

{Na-15-crown-5}{MoF2Cl2(N3S2)}

Conditions
ConditionsYield
In acetonitrile byproducts: NaCl; addn. of NaF to suspn. of Mo-complex, addn. of 15-crown-5 (dropwise), stirring (12 h), sepn. of ppt. (filtration); crystn. on cooling (-20°C), sepn. (filtration off), washing (acetonitrile), drying (vac.); elem. anal.;95%
15-crown-5
33100-27-5

15-crown-5

{ReCl3(NO)2}2

{ReCl3(NO)2}2

sodium fluoride

sodium fluoride

acetonitrile
75-05-8

acetonitrile

{Na(15-crown-5)}{ReFCl3(NO)(CH3CN)}

{Na(15-crown-5)}{ReFCl3(NO)(CH3CN)}

Conditions
ConditionsYield
In acetonitrile heating of 1.8mmol (ReCl3(NO)2)2 in 30ml acetonitrile (formation of sol. (ReCl3(NO)2(CH3CN)), addn. of 3.6mmol NaF amd 0.715ml 15 crown-5; 2h refluxing;; cooling down and concg. of soln.; single crystal;filtn., concgn. of filtrate (20ml); elem. anal.;;95%
aluminium trichloride
7446-70-0

aluminium trichloride

15-crown-5
33100-27-5

15-crown-5

{AlCl2((CH2CH2O)5)}(1+)*AlCl4(1-)={AlCl2((CH2CH2O)5)}{AlCl4}
111523-29-6

{AlCl2((CH2CH2O)5)}(1+)*AlCl4(1-)={AlCl2((CH2CH2O)5)}{AlCl4}

Conditions
ConditionsYield
In tetrahydrofuran all manipulations under dry N2; slowly dissolving AlCl3 in THF, adding 15-crown-5 with stirring, color change from light green to dark green, crystn. (after 30 min); sepg. crystals from the mother soln., drying (vac., 25°C); elem. anal.;95%
15-crown-5
33100-27-5

15-crown-5

scandium chloride * 3 acetonitrile

scandium chloride * 3 acetonitrile

(ScCl2(C10H20O5))(1+)*Cl(1-)=(ScCl2(C10H20O5))Cl
147631-11-6

(ScCl2(C10H20O5))(1+)*Cl(1-)=(ScCl2(C10H20O5))Cl

Conditions
ConditionsYield
In acetonitrile Sc-compd. was dissolved in MeCN (under dry inert gas), addn. of crown ether; sepn. of precipitate, washing with MeCN, vac. drying at 30°C, elem. anal.;95%
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