Hangzhou DaAppearance:colourless liquid, clear Storage:Store in dry, dark and ventilated place. Package:according to the clients requirement Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Ag
Cas:111-44-4
Min.Order:1 Kilogram
FOB Price: $10.0 / 11.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:111-44-4
Min.Order:1 Kilogram
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Type:Manufacturers
inquiryChengdu and import and export trade co., LTD., registered capital of 10 million yuan, nearly $2 million, we have a production of pharmaceutical raw materials, pharmaceutical raw materials factory reagent r&d center, we are doing research and de
Cas:111-44-4
Min.Order:1 Metric Ton
FOB Price: $2200.0 / 2300.0
Type:Manufacturers
inquiry1.Hefei TNJ Chemical Industry Co.Limited(ISO9001:2008),are strong in the field of Pharmaceuticals,food additives,plant extract and fine chemical for more than 10 years. 2.Full experience of large numbers container loading in main Chinese seap
high quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:111-44-4
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiry2'-dichlorodiethylether 99% 111-44-4 Spec. Chemical Name: bis(2-chloroethyl) ether Chemical Formula C4H8Cl2O CAS Number: 111-44-4 Appearance: Colorless l
Cas:111-44-4
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryCAS 111-44-4 Name 2,2'-Dichlorodiethyl ether Appearance Clear colorless liquid Application Used as solvent in rubber, resin, etc
Appearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:By Sea/Air/Courier Port:Qingdao
Cas:111-44-4
Min.Order:100 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:111-44-4
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:111-44-4
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:111-44-4
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Interme
Cas:111-44-4
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryHigh quality 2 2'-Dichlorodiethyl ether/cas 111-44-4 from Wuxi TAA Chemical Industry Co.,Ltd. 1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index hav
Cas:111-44-4
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Other
inquiryProduct name: Dichloroethyl Ether CAS No.:111-44-4 Molecule Formula:C4H6Cl4O Molecule Weight:211.90 Purity: 99.0% Package: 200kg/drum Description:Colorless to light red transparent liquid Manufacture Standards:Enterprise Standard
Cas:111-44-4
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:111-44-4
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWe are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:111-44-4
Min.Order:1 Gram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home
Cas:111-44-4
Min.Order:240 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:111-44-4
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.High quality : the purity is 99% min . through multiple producing procedures. 2.Competitive price : low price because of our skilled production technolpgy ,save the production cost at most , and give big profit room to our customers489.Safe and fa
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:111-44-4
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiry2,2'-Dichlorodiethyl etherAppearance:colourless liquid Package:in drums Application:A clear colorless liquid with a sweet pleasant or nauseating odor. Flash point 131°F. Denser than water and insoluble in water. Toxic by inhalation and skin absorptio
Cas:111-44-4
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With 2-chloro-1,3-dimethylimidazolinium chloride; triethylamine In dichloromethane at 20℃; for 17h; Chlorination; | 92% |
With hydrogenchloride; sulfuric acid; zinc(II) chloride at 95℃; |
Conditions | Yield |
---|---|
With hexabutylguanidinium chloride at 120℃; for 4h; | 91% |
Conditions | Yield |
---|---|
With thionyl chloride Reflux; | 86% |
With thionyl chloride at 110℃; | 84% |
With pyridine; thionyl chloride In benzene for 20h; Heating; | 35% |
Conditions | Yield |
---|---|
With hydrogenchloride In water at 30℃; for 12h; Temperature; | 81.3% |
Conditions | Yield |
---|---|
With 2-chloro-ethanol |
2-chloroethyl nitrite
3-oxa-1,5-dichloropentane
Conditions | Yield |
---|---|
With sulfuryl dichloride at 165℃; |
Conditions | Yield |
---|---|
With chlorine; 2-chloro-ethanol | |
With oxirane; chlorine | |
With oxirane; chlorine; 2-chloro-ethanol |
tert-butylhypochlorite
ethene
2-chloro-ethanol
3-oxa-1,5-dichloropentane
Conditions | Yield |
---|---|
With sulfuric acid Entfernen das entstehende Wasser; | |
With sulfuryl dichloride at 165℃; | |
With sulfuric acid at 200 - 250℃; |
1,4-dioxane
A
1,11-dichloro-3,6,9-trioxaundecane
B
1,2-bis(2-chloroethoxy)ethane
C
3-oxa-1,5-dichloropentane
Conditions | Yield |
---|---|
With titanium tetrachloride 1.) 20 deg C, 2.) 160 deg C, 5 d; Yield given. Multistep reaction. Yields of byproduct given; |
methanol
ethene
A
2-chloroethyl methyl ether
B
1,2-dichloro-ethane
C
3-oxa-1,5-dichloropentane
D
1,4-dichlorobutane
Conditions | Yield |
---|---|
With hydrogenchloride at 5 - 10℃; under 45003.6 Torr; electrolysis; | A 47 % Chromat. B 31 % Chromat. C 17 % Chromat. D 6 % Chromat. |
ethene
A
1,2-dichloro-ethane
B
3-oxa-1,5-dichloropentane
C
1,4-dichlorobutane
Conditions | Yield |
---|---|
With hydrogenchloride In water; acetonitrile at 5 - 10℃; under 45003.6 Torr; electrolysis, further solvent methanol; | A 82 % Chromat. B 17 % Chromat. C 6 % Chromat. |
ethene
A
2-chloroethyl methyl ether
B
1,2-dichloro-ethane
C
3-oxa-1,5-dichloropentane
D
1,4-dichlorobutane
Conditions | Yield |
---|---|
With hydrogenchloride In methanol at 5 - 10℃; under 45003.6 Torr; electrolysis, further solvent aq. acetonitrile; | A 47 % Chromat. B 31 % Chromat. C 17 % Chromat. D 6 % Chromat. |
ethene
A
1,2-dichloro-ethane
B
3-oxa-1,5-dichloropentane
C
2-chloro-ethanol
Conditions | Yield |
---|---|
With hypochloric acid; chlorine In various solvent(s) at 25℃; for 0.00883333h; in tributyl phosphate, in a rotor-pulsation apparatus; Title compound not separated from byproducts; | A 11.9 % Spectr. B 14.4 % Spectr. C 42.1 % Spectr. |
With hypochloric acid; chlorine In various solvent(s) at 25℃; for 0.00883333h; in tributyl phosphate, in a rotor pulsation apparatus; Title compound not separated from byproducts; | A 11.9 % Spectr. B 14.4 % Spectr. C 42.1 % Spectr. |
With hypochloric acid; chlorine In various solvent(s) at 25℃; for 0.00883333h; Product distribution; dependence of yield of products on time of reaction in tributyl phosphate in a rotor-pulsation apparatus; | A 11.9 % Spectr. B 14.4 % Spectr. C 42.1 % Spectr. |
sulfuryl dichloride
2-chloro-ethanol
A
sulfuric acid bis-(2-chloroethyl) ester
B
3-oxa-1,5-dichloropentane
Conditions | Yield |
---|---|
at 165℃; |
ethene
chlorine
2-chloro-ethanol
A
1,2-dichloro-ethane
B
3-oxa-1,5-dichloropentane
Conditions | Yield |
---|---|
at 15 - 20℃; Kinetics; unter Lichtausschluss; |
Conditions | Yield |
---|---|
With chlorine; sodium sulfate at 60℃; | |
With chlorine; sodium sulfate at 60℃; |
Conditions | Yield |
---|---|
With 1,4-dioxane; polyethylene glycol chlorohydrin; chlorine; 2-chloro-ethanol at 25 - 35℃; | |
With 1,4-dioxane; chlorine at 20 - 25℃; | |
With polyethylene glycol mixture; chlorine |
2-chloro-ethanol
A
1,4-dioxane
B
2-[2-(chloroethoxy)ethoxy]ethanol
C
2-(2-Chloroethoxy)ethanol
D
1,2-dichloro-ethane
E
3-oxa-1,5-dichloropentane
Conditions | Yield |
---|---|
at 150℃; for 5h; Product distribution; Kinetics; Rate constant; dependence of the products of ECH decomposition on temperature in sealed tube at 115, 130, 140, 150, 160 deg C; |
sulfuryl dichloride
2-chloroethyl nitrite
A
chloroethyl chlorosulfate
B
sulfuric acid bis-(2-chloroethyl) ester
C
3-oxa-1,5-dichloropentane
ethene
chlorine
A
1,2-dichloro-ethane
B
3-oxa-1,5-dichloropentane
Conditions | Yield |
---|---|
at 15 - 20℃; unter Lichtausschluss; |
1,4-dioxane
ethene
chlorine
A
1,2-bis(2-chloroethoxy)ethane
B
1,2-dichloro-ethane
C
3-oxa-1,5-dichloropentane
Conditions | Yield |
---|---|
at 20 - 25℃; weniger als 1 Mol Chlor; | |
at 20 - 25℃; weniger als 1 Mol Chlor; |
ethene
water
chlorine
A
1,2-dichloro-ethane
B
3-oxa-1,5-dichloropentane
C
2-chloro-ethanol
ethanol
ethene
chlorine
A
2-chloroethyl ethyl ether
B
1,2-dichloro-ethane
C
3-oxa-1,5-dichloropentane
D
2-chloro-ethanol
1,3-DIOXOLANE
A
bis(2-chloromethyl)ether
B
2-chloroethyl chloromethyl ether
C
3-oxa-1,5-dichloropentane
Conditions | Yield |
---|---|
Stage #1: 1,3-DIOXOLANE With dichloromethane; tungsten(VI) chloride In Chloroform-D at 20℃; for 192h; Stage #2: With water In Chloroform-D at -20℃; |
2-Methoxyethoxymethyl chloride
A
bis(2-chloromethyl)ether
B
methylene chloride
C
Dimethyl ether
D
chloromethyl methyl ether
E
1,2-dichloro-ethane
F
3-oxa-1,5-dichloropentane
Conditions | Yield |
---|---|
Stage #1: 2-Methoxyethoxymethyl chloride With dichloromethane; tungsten(VI) chloride In Chloroform-D at 20℃; for 12h; Stage #2: With water In Chloroform-D at -20℃; |
3-oxa-1,5-dichloropentane
2,2'-diiodoethyl ether
Conditions | Yield |
---|---|
With sodium iodide In acetone for 120h; Heating / reflux; | 100% |
With sodium iodide In acetone for 72h; Heating; | 81% |
With sodium iodide In acetone for 72h; Reflux; Darkness; | 81% |
ditosylethylenediamine
3-oxa-1,5-dichloropentane
N,N',N'',N'''-tetrakis(tolyl-p-sulphonyl)-1,10-dioxa-4,7,13,16-tetra-azacyclo-octadecane
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide 170 deg C, 5 h; cool, 12 h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide for 5h; Heating; | 78% |
With potassium carbonate In N,N-dimethyl-formamide at 5 - 170℃; for 30h; | 15% |
With potassium carbonate In N,N-dimethyl-formamide at 170℃; for 12h; | 14.3% |
With potassium carbonate In N,N-dimethyl-formamide at 170℃; for 5h; Yield given; |
3-oxa-1,5-dichloropentane
Conditions | Yield |
---|---|
With boron trichloride at -78 - 0℃; | 100% |
p-methoxybenzylnitrile
3-oxa-1,5-dichloropentane
4-(4-methoxyphenyl)tetrahydro-2H-pyran-4-carbonitrile
Conditions | Yield |
---|---|
Stage #1: p-methoxybenzylnitrile With sodium hydride In DMF (N,N-dimethyl-formamide) at 0 - 20℃; for 0.5h; Stage #2: 3-oxa-1,5-dichloropentane In DMF (N,N-dimethyl-formamide) at 0 - 20℃; for 2.33333h; | 100% |
Stage #1: p-methoxybenzylnitrile With sodium hydroxide In N,N-dimethyl-formamide for 0.5h; Stage #2: 3-oxa-1,5-dichloropentane In N,N-dimethyl-formamide at 80 - 100℃; for 5h; | 69% |
With sodium hydride In N,N-dimethyl-formamide; mineral oil Cooling with ice; | 64% |
With NaH In dimethyl sulfoxide |
phenylacetonitrile
3-oxa-1,5-dichloropentane
4-phenyltetrahydro-2H-pyran-4-carbonitrile
Conditions | Yield |
---|---|
With sodium hydride; sodium iodide In dimethyl sulfoxide; mineral oil at 20℃; for 12h; Inert atmosphere; Sealed tube; | 99% |
With sodium amide; toluene |
3,5-dihydroxy-4-(phenylmethoxy)benzoic acid methyl ester
3-oxa-1,5-dichloropentane
methyl 4-O-benzyl-3,5-di-O-methoxymethylgallate
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 1h; Inert atmosphere; | 99% |
3,5-dimethyl-1H-pyrazole
3-oxa-1,5-dichloropentane
1,1'-(2,2'-oxybis(ethane-2,1-diyl))bis(3,5-dimethyl-1H-pyrazole)
Conditions | Yield |
---|---|
Stage #1: 3,5-dimethyl-1H-pyrazole With potassium hydroxide In dimethyl sulfoxide at 80℃; for 1h; Stage #2: 3-oxa-1,5-dichloropentane In dimethyl sulfoxide at 80℃; Further stages.; | 98% |
1,2-bis(t-butyloxycarbonyl)hydrazine
3-oxa-1,5-dichloropentane
1,4,5-oxadiazepane-4,5-dicarboxylic acid di-tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: 1,2-bis(t-butyloxycarbonyl)hydrazine With sodium hydride In N,N-dimethyl-formamide at -3 - 20℃; for 2.13333h; Stage #2: 3-oxa-1,5-dichloropentane In N,N-dimethyl-formamide at -3 - 20℃; Temperature; | 97.1% |
Conditions | Yield |
---|---|
In acetonitrile at 60℃; for 24h; | 97% |
4-methoxy-aniline
3-oxa-1,5-dichloropentane
4-(4-methoxyhenyl)morpholine nitric acid salt
Conditions | Yield |
---|---|
Stage #1: 4-methoxy-aniline; 3-oxa-1,5-dichloropentane With tetrabutylammomium bromide; sodium hydroxide for 8h; Heating; Stage #2: With nitric acid at 0 - 5℃; for 12h; | 97% |
Conditions | Yield |
---|---|
With sodium hydroxide In dimethyl sulfoxide at 90℃; for 24h; | 96% |
(4-fluoromethyl-phenyl)-acetonitrile
3-oxa-1,5-dichloropentane
4-(4-fluorophenyl)tetrahydro-2H-pyran-4-carbonitrile
Conditions | Yield |
---|---|
With sodium hydride In diethyl ether; dimethyl sulfoxide at 5 - 30℃; | 96% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 120℃; for 3h; | 96% |
In acetonitrile at 100℃; for 48h; Inert atmosphere; | 90% |
1,3-dihydroxy-4-iodo-2-nitrobenzene
3-oxa-1,5-dichloropentane
1-iodo-2,4-bis(methoxymethoxy)-3-nitrobenzene
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 0 - 20℃; for 1.5h; | 96% |
Conditions | Yield |
---|---|
With cesium iodide In ethanol; water at 90℃; under 8250.83 Torr; Temperature; Pressure; | 95.9% |
3-oxa-1,5-dichloropentane
2-hydroxynitrobenzene
1,5-bis(o-nitrophenoxy)-3-oxapentane
Conditions | Yield |
---|---|
With 15-crown-5; sodium carbonate In N,N-dimethyl-formamide at 140℃; for 5h; | 95% |
With potassium carbonate In dimethyl sulfoxide at 130℃; for 6h; | 85% |
With potassium carbonate In N,N-dimethyl-formamide |
Conditions | Yield |
---|---|
With sodium carbonate In acetonitrile for 24h; Heating; | 95% |
Conditions | Yield |
---|---|
In acetonitrile at 60℃; for 24h; | 95% |
2-Benzoyl-hydrazin-1-carbonsaeuremethylester
3-oxa-1,5-dichloropentane
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl acetamide; N,N-dimethyl-formamide at 0 - 20℃; | 95% |
2,4-diamino-6-(4-nitrophenyl)-1,3,5-triazine
3-oxa-1,5-dichloropentane
Conditions | Yield |
---|---|
Stage #1: 2,4-diamino-6-(4-nitrophenyl)-1,3,5-triazine With sodium hydride In N,N-dimethyl acetamide at 55 - 60℃; for 0.166667h; Inert atmosphere; Stage #2: 3-oxa-1,5-dichloropentane In N,N-dimethyl acetamide for 4.5h; Reagent/catalyst; Temperature; Inert atmosphere; | 94.6% |
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 65℃; Thermodynamic data; Solvent; Reagent/catalyst; Concentration; Temperature; Inert atmosphere; Green chemistry; | 77% |
para-tert-butylphenol
3-oxa-1,5-dichloropentane
1,5-Bis(4-t-butylphenoxy)-3-oxapentane
Conditions | Yield |
---|---|
With potassium hydroxide In butan-1-ol for 18h; Heating; | 94% |
With sodium hydroxide at 180 - 190℃; |
ethyl 4,6-O-benzylidene-α-D-glucopyranoside
3-oxa-1,5-dichloropentane
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide In water at 20℃; for 9h; | 94% |
3-oxa-1,5-dichloropentane
1,5-diazido-3-oxapentane
Conditions | Yield |
---|---|
With sodium azide; tetra-(n-butyl)ammonium iodide In N,N-dimethyl-formamide at 90℃; for 48h; | 93% |
With sodium azide In N,N-dimethyl-formamide for 17h; Heating; | 62.8% |
With sodium azide; choline chloride In N,N-dimethyl-formamide at 95℃; Rate constant; var. phase transfer catalysts; | |
With sodium azide; cetyltributylphosphonium bromide; potassium iodide for 17h; Heating; Yield given; | |
With sodium azide; cetylpyridinium chloride; potassium iodide In water for 20h; Heating / reflux; |
3-oxa-1,5-dichloropentane
2,2,2-trichloro-1-fluoroethyl 2-chloroethyl ether
Conditions | Yield |
---|---|
With sulfur tetrafluoride; hydrogen fluoride; chlorine at 80℃; for 5h; Product distribution; other temperature, stainless-steel autoclave, other ratio of reagents; | 93% |
With sulfur tetrafluoride; hydrogen fluoride; chlorine at 80℃; for 5h; stainless-steel autoclave; | 93% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 60℃; Cycloaddition; | 93% |
endo-N-hydroxy-5-norbornene-2,3-dicarboxyimide
3-oxa-1,5-dichloropentane
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 2h; | 92% |
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 22h; Gabriel Amine Synthesis; | 64.5 g |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 24h; | 92% |
Conditions | Yield |
---|---|
In acetonitrile for 24h; Menshutkin Reaction; Heating; | 92% |
With sodium carbonate In isopropyl alcohol at 55 - 83℃; for 8h; |
3-oxa-1,5-dichloropentane
2-(4-phenylthiazol-2-yl)acetonitrile
4-(4-phenylthiazol-2-yl)tetrahydro-2H-pyran-4-carbonitrile
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide; mineral oil Cooling with ice; | 92% |
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