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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

tert-butyl hypochlorite

Cas:507-40-4

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Hangzhou Dingyan Chem Co., Ltd

Analysis tests Standard Results Appearance Light yellow liquid conform Structure Nuclear mag

Top purity tert-butyl hypochlorite with high quality and best price cas:507-40-4

Cas:507-40-4

Min.Order:1 Gram

FOB Price: $2.0 / 5.0

Type:Trading Company

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply tert-butyl hypochlorite

Cas:507-40-4

Min.Order:1

Negotiable

Type:Other

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Large Stock 99.0% tert-butyl hypochlorite 507-40-4 Producer

Cas:507-40-4

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

tert-Butyl hypochlorite

Cas:507-40-4

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

TIANFUCHEM--507-40-4--tert-Butyl Hypochlorite factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business

TIANFUCHEM--507-40-4--tert-Butyl Hypochlorite factory price

Cas:507-40-4

Min.Order:1 Metric Ton

FOB Price: $2000.0

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

tert-Butyl Hypochlorite

Cas:507-40-4

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Wholesale price CAS 507-40-4 with best price

Cas:507-40-4

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Hypochlorous acid,1,1-dimethylethyl ester 507-40-4

Cas:507-40-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

tert-Butyl Hypochlorite CAS:507-40-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic int

tert-Butyl Hypochlorite CAS:507-40-4

Cas:507-40-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Hypochlorous acid,1,1-dimethylethyl ester

Cas:507-40-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

tert-Butyl Hypochlorite

Cas:507-40-4

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Send Pharmaceutical Technology Co., Ltd.

low price high quality high purity good sevice stock Appearance:white Storage:Preserve In Well-Closed, Light-Resistant and Tight Containers. Store In Cool & Dry Place Package:1g,5g,10g...1kg,5kg...more Application:Pharmaceutical intermediat

HYPOCHLOROUS ACID TERT-BUTYL ESTER

Cas:507-40-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

tert-Butyl Hypochlorite/High quality/Best price

Cas:507-40-4

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Tert-butyl Hypochlorite

Cas:507-40-4

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

We are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...)

tert-Butyl HypochloriteCAS NO.: 507-40-4

Cas:507-40-4

Min.Order:1 Kilogram

FOB Price: $5.0

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

tert-Butyl Hypochlorite Chemical Properties Boiling point 79.6℃ (750 Torr) density 0.96 refractive index 1.4010-1.4050 storage temp. Refrigerator Merck 14,1571 Stability: Unstable. Light-sensitive. Highly flammable. Incompatibl

Hypochlorous Acid tert-Butyl Ester

Cas:507-40-4

Min.Order:1 Gram

FOB Price: $66.0

Type:Lab/Research institutions

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

tert-Butyl Hypochlorite

Cas:507-40-4

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

tert-Butyl Hypochlorite

Cas:507-40-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Zhongqi chem Co.,Ltd.

Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an

Tert-butyl hypochlorite

Cas:507-40-4

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, in

Enke tert-Butyl hypochlorite

Cas:507-40-4

Min.Order:1 Kilogram

FOB Price: $300.0 / 400.0

Type:Lab/Research institutions

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

tert-Butyl hypochlorite

Cas:507-40-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Greenutra Resource Inc

tert-butyl hypochloriteAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air

tert-butyl hypochlorite

Cas:507-40-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

Tert-Butyl Hypochlorite

Cas:507-40-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

tert-butyl hypochlorite

Cas:507-40-4

Min.Order:0

Negotiable

Type:Other

inquiry

Shanghai Acmec Biochemical Technology Co., Ltd.

Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea

Acmec tert-Butyl Hypochlorite 500g

Cas:507-40-4

Min.Order:1 bottle

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

tert-Butyl Hypochlorite

Cas:507-40-4

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hubei Taiho Chemical Co.,LTD

TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

Tert-BUTYL HYPOCHLORITE

Cas:507-40-4

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Hypochlorous acid,1,1-diMethylethyl ester

Cas:507-40-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Circle Star Chem-medical Technology co.,Ltd.

good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:25kg,50kg,180kg,200kg,250kg,1000kg,customization Application:Pharma;Industry;Agricultural;chemical reaserch Tran

tert-Butyl Hypochlorite

Cas:507-40-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

tert-butyl alcohol
75-65-0

tert-butyl alcohol

tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

Conditions
ConditionsYield
With sodium hypochlorite; acetic acid In water at 0℃; for 0.166667h; Darkness;75%
With sodium hypochlorite; acetic acid at 20 - 25℃;72.2%
With acetic acid for 0.05h;66%
hypochloric acid
14989-30-1

hypochloric acid

tert-butyl alcohol
75-65-0

tert-butyl alcohol

tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

Conditions
ConditionsYield
In tetrachloromethane; water shaking a soln. of alcohol in CCl4 with an aq. soln. of HClO;; soln. of ester in CCl4 obtained;;
In tetrachloromethane; water shaking a soln. of alcohol in CCl4 with an aq. soln. of HClO;; soln. of ester in CCl4 obtained;;
sodium hypochlorite
7681-52-9

sodium hypochlorite

tert-butyl alcohol
75-65-0

tert-butyl alcohol

tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

Conditions
ConditionsYield
With acetic acid at 0℃; Darkness;
{bis(trimethylsilyl)amino}-(t-butylimino)phosphane
54760-90-6, 95792-83-9

{bis(trimethylsilyl)amino}-(t-butylimino)phosphane

tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

tert-butyl N-tert-butyl-N,N'-bis(trimethylsilyl)phosphoramidochloridimidate
79202-19-0

tert-butyl N-tert-butyl-N,N'-bis(trimethylsilyl)phosphoramidochloridimidate

Conditions
ConditionsYield
In benzene for 2h; Ambient temperature;100%
N-trimethylsilylimidophosphenous acid 2,2,6,6-tetramethylpiperidine
72821-01-3

N-trimethylsilylimidophosphenous acid 2,2,6,6-tetramethylpiperidine

tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

P-chloro-O-tert-butyl-2,2,6,6-tetramethylpiperidido-N-trimethylsilylimidophosphate

P-chloro-O-tert-butyl-2,2,6,6-tetramethylpiperidido-N-trimethylsilylimidophosphate

Conditions
ConditionsYield
In benzene at 0℃; for 1h; argon atmosphere;100%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

N-propylbenzohydroxamic acid
72805-06-2

N-propylbenzohydroxamic acid

N-chloro-N-propoxybenzamide

N-chloro-N-propoxybenzamide

Conditions
ConditionsYield
In dichloromethane for 3h; anhydrous;100%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

2-chloro-1-(4-isopropylphenyl)-2-methylpropan-1-one

2-chloro-1-(4-isopropylphenyl)-2-methylpropan-1-one

2-chloro-1-(4-(2-chloropropan-2-yl)phenyl)-2-methylpropan-1-one

2-chloro-1-(4-(2-chloropropan-2-yl)phenyl)-2-methylpropan-1-one

Conditions
ConditionsYield
In chlorobenzene at -10 - 20℃; Inert atmosphere;100%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

N,N,N'-tris(trimethylsilyl)phosphenimidous amide
50732-21-3, 65428-75-3

N,N,N'-tris(trimethylsilyl)phosphenimidous amide

tert-butyl tris(trimethylsilyl)phosphoramidochlorimidate
79202-16-7

tert-butyl tris(trimethylsilyl)phosphoramidochlorimidate

Conditions
ConditionsYield
In benzene for 2h; Ambient temperature;98%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

N'-(1-adamantyl)-N,N-bis(trimethylsilyl)phosphorimidous amide
76889-11-7

N'-(1-adamantyl)-N,N-bis(trimethylsilyl)phosphorimidous amide

C20H42ClN2OPSi2
79202-21-4

C20H42ClN2OPSi2

Conditions
ConditionsYield
In benzene for 2h; Ambient temperature;95%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

(1,3-dimethylimidazol-2-ylidene)borane
1211417-77-4

(1,3-dimethylimidazol-2-ylidene)borane

(1,3-dimethyl-1H-imidazolium-2-yl)trichloroborate
1352941-55-9

(1,3-dimethyl-1H-imidazolium-2-yl)trichloroborate

Conditions
ConditionsYield
In dichloromethane at -78 - 20℃; for 1.05h; Schlenk technique; Inert atmosphere;94%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

N,N'-bis(t-butyl)-N-(trimethylsilyl)-phosphenimidous amide
53787-01-2, 87938-40-7

N,N'-bis(t-butyl)-N-(trimethylsilyl)-phosphenimidous amide

tert-butyl N,N'-di-tert-butyl-N-(trimethylsilyl)phosphoramidochloridimidate
79202-23-6

tert-butyl N,N'-di-tert-butyl-N-(trimethylsilyl)phosphoramidochloridimidate

Conditions
ConditionsYield
In benzene for 2h; Ambient temperature;93%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

LY 292223
130735-56-7

LY 292223

3-Chloro-2-(4-morpholinyl)-4H-1-benzopyran-4-one
130735-75-0

3-Chloro-2-(4-morpholinyl)-4H-1-benzopyran-4-one

Conditions
ConditionsYield
In dichloromethane; ethyl acetate91%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

2,4-dihydroxy-trifluoroacetophenone
182951-75-3

2,4-dihydroxy-trifluoroacetophenone

2,4-Dihydroxy-3-chloro-trifluoroacetophenone

2,4-Dihydroxy-3-chloro-trifluoroacetophenone

Conditions
ConditionsYield
In tetrachloromethane90%
tetrachloromethane
56-23-5

tetrachloromethane

(H3)triosmiumnonacarbonyl(μ3-CH)

(H3)triosmiumnonacarbonyl(μ3-CH)

tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

(H3)triosmiumnonacarbonyl(μ3-CCl)

(H3)triosmiumnonacarbonyl(μ3-CCl)

Conditions
ConditionsYield
Heating H3Os3(CO)9(μ3-CH) at 45°C in CO-saturated CCl4 with excess t-BuOCl.; TLC on fluorescent silica (pentane);90%
(H3)triosmiumnonacarbonyl(μ3-CH)

(H3)triosmiumnonacarbonyl(μ3-CH)

tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

Bromotrichloromethane
75-62-7

Bromotrichloromethane

(H3)triosmiumnonacarbonyl(μ3-CBr)

(H3)triosmiumnonacarbonyl(μ3-CBr)

Conditions
ConditionsYield
Heating H3Os3(CO)9(μ3-CH) at 45°C in CO-saturated BrCCl3 with excess t-BuOCl.; TLC on fluorescent silica (pentane);90%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

phenylacetylene
536-74-3

phenylacetylene

benzoic acid
65-85-0

benzoic acid

1-(tert-butoxy)-2,2-dichloro-2-phenylethyl benzoate

1-(tert-butoxy)-2,2-dichloro-2-phenylethyl benzoate

Conditions
ConditionsYield
With tetrachloromethane at 30℃; for 2h; Schlenk technique;90%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

(C4H9)2(C6H5)SnCH(CH3)CH(CH3)OH

(C4H9)2(C6H5)SnCH(CH3)CH(CH3)OH

threo-iodo{3-(pivaloyloxy)but-2-yl}dibutylstannane

threo-iodo{3-(pivaloyloxy)but-2-yl}dibutylstannane

Conditions
ConditionsYield
With pyridine In diethyl ether byproducts: HCl; for 1 h at 0°C;; filtn.; washing with satd. CuSO4 soln. and NaHCO3 soln.; drying;;89%
3-(3-Acetaminophenyl)methyl-2,3,3a4,5,9b-hexahydro-1H-oxo-benz[e]isoindole

3-(3-Acetaminophenyl)methyl-2,3,3a4,5,9b-hexahydro-1H-oxo-benz[e]isoindole

3-(3-acetaminophenyl)methyl-2,3,3a,4,5,9b-hexahydro-1H-oxo-benz[e]isoindole
140378-02-5

3-(3-acetaminophenyl)methyl-2,3,3a,4,5,9b-hexahydro-1H-oxo-benz[e]isoindole

tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

3-(5-Acetamino-2-chlorophenyl)methyl-2,3,3a,4,5,9b-hexahydro-1H-oxo-benz[e]isoindole
140378-03-6

3-(5-Acetamino-2-chlorophenyl)methyl-2,3,3a,4,5,9b-hexahydro-1H-oxo-benz[e]isoindole

Conditions
ConditionsYield
In chloroform86%
3-(3-acetaminophenyl)methyl-2,3,3a,4,5,9b-hexahydro-1H-oxo-benz[e]isoindole
140378-02-5

3-(3-acetaminophenyl)methyl-2,3,3a,4,5,9b-hexahydro-1H-oxo-benz[e]isoindole

tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

3-(5-Acetamino-2-chlorophenyl)methyl-2,3,3a,4,5,9b-hexahydro-1H-oxo-benz[e]isoindole
140378-03-6

3-(5-Acetamino-2-chlorophenyl)methyl-2,3,3a,4,5,9b-hexahydro-1H-oxo-benz[e]isoindole

Conditions
ConditionsYield
In chloroform86%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

6α-bromopenicillanic acid pivalolyloxymethyl ester
76468-87-6

6α-bromopenicillanic acid pivalolyloxymethyl ester

(pivaloyloxy)methyl 2-<(2'S,3'R)-2'-tert-butoxy-3'-bromo-4'-oxoazetidin-1'-yl>-3-methylbut-2-enoate
122348-01-0

(pivaloyloxy)methyl 2-<(2'S,3'R)-2'-tert-butoxy-3'-bromo-4'-oxoazetidin-1'-yl>-3-methylbut-2-enoate

Conditions
ConditionsYield
With 1-methyl-piperazine In chloroform for 0.166667h; Ambient temperature;85%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

methoxy-1 trimethylsiloxy-2 styrene
81699-72-1

methoxy-1 trimethylsiloxy-2 styrene

2-tert-Butoxy-2-methoxy-1-phenyl-ethanone
81699-78-7

2-tert-Butoxy-2-methoxy-1-phenyl-ethanone

Conditions
ConditionsYield
With mercury(II) oxide; tetrakis(triphenylphosphine) palladium(0) In toluene at -78℃; for 1h;85%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

(C4H9)2(C6H5)SnCH(CH3)CH(CH3)OH

(C4H9)2(C6H5)SnCH(CH3)CH(CH3)OH

erythro-iodo-{3-(pivaloyloxy)but-2-yl}dibutylstannane

erythro-iodo-{3-(pivaloyloxy)but-2-yl}dibutylstannane

Conditions
ConditionsYield
With pyridine In diethyl ether byproducts: HCl; for 1 h at 0°C;; filtn.; washing with satd. CuSO4 soln. and NaHCO3 soln.; drying;;85%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

water
7732-18-5

water

2-(1-chloro-2-hydroxy-2-phenylethyl)-6-methyl-1,3,6,2-dioxazaborocane-4,8-dione

2-(1-chloro-2-hydroxy-2-phenylethyl)-6-methyl-1,3,6,2-dioxazaborocane-4,8-dione

C13H15BClNO5

C13H15BClNO5

Conditions
ConditionsYield
With pyridine-4-carboxylic acid In acetone at -15℃;A 85%
B 6%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

ammonia
7664-41-7

ammonia

chloroamine
12190-75-9

chloroamine

Conditions
ConditionsYield
In methanol; tert-butyl alcohol at -40℃;80%
In neat (no solvent) equimolar amounts;; detection by spectroscopy;;
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

2-amino-5-bromo-3-methylbenzonitrile
1093966-37-0

2-amino-5-bromo-3-methylbenzonitrile

2,2'-(diazene-1,2-diyl)bis(5-bromo-3-methylbenzonitrile)

2,2'-(diazene-1,2-diyl)bis(5-bromo-3-methylbenzonitrile)

Conditions
ConditionsYield
With potassium iodide In acetonitrile at -10℃; Temperature; Inert atmosphere;80%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

1-ethyl-3-methylimidazolium dicyanodihydridoborate

1-ethyl-3-methylimidazolium dicyanodihydridoborate

C2BCl2N2(1-)*C6H11N2(1+)

C2BCl2N2(1-)*C6H11N2(1+)

Conditions
ConditionsYield
In dichloromethane at 0 - 20℃; for 12h; Darkness;79%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

C14H15BFNO4

C14H15BFNO4

water
7732-18-5

water

C14H16BClFNO5

C14H16BClFNO5

Conditions
ConditionsYield
With pyridine-4-carboxylic acid In acetone at -15℃; Reagent/catalyst; Solvent; Temperature;78%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

(2S,3S)-3-(tert-butyldiphenylsilyloxy)-2-methylbutanal oxime
1132969-93-7

(2S,3S)-3-(tert-butyldiphenylsilyloxy)-2-methylbutanal oxime

(S,Z)-1-(trityloxy)pent-3-en-2-ol
1132969-94-8

(S,Z)-1-(trityloxy)pent-3-en-2-ol

(R)-1-((4S,5R)-3-((2S,3S)-3-(tert-butyldiphenylsilyloxy)butan-2-yl)-4-methyl-4,5-dihydroisoxazol-5-yl)-2-(trityloxy)ethanol
1132969-95-9

(R)-1-((4S,5R)-3-((2S,3S)-3-(tert-butyldiphenylsilyloxy)butan-2-yl)-4-methyl-4,5-dihydroisoxazol-5-yl)-2-(trityloxy)ethanol

Conditions
ConditionsYield
Stage #1: tert-butylhypochlorite; (2S,3S)-3-(tert-butyldiphenylsilyloxy)-2-methylbutanal oxime In dichloromethane at -78℃; Inert atmosphere;
Stage #2: (S,Z)-1-(trityloxy)pent-3-en-2-ol With ethylmagnesium bromide In diethyl ether; dichloromethane; isopropyl alcohol at 0 - 20℃; Inert atmosphere;
76%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

phenylacetylene
536-74-3

phenylacetylene

Trimethylacetic acid
75-98-9

Trimethylacetic acid

1-(tert-butoxy)-2,2-dichloro-2-phenylethyl pivalate

1-(tert-butoxy)-2,2-dichloro-2-phenylethyl pivalate

Conditions
ConditionsYield
With tetrachloromethane at 60℃; for 1h; Schlenk technique;76%
2-Picolinic acid
98-98-6

2-Picolinic acid

tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

phenylacetylene
536-74-3

phenylacetylene

1-(tert-butoxy)-2,2-dichloro-2-phenylethyl picolinate

1-(tert-butoxy)-2,2-dichloro-2-phenylethyl picolinate

Conditions
ConditionsYield
With tetrachloromethane at 30℃; for 1h; Schlenk technique;76%
tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

o-toluidine
95-53-4

o-toluidine

2-methyl-6-(thiomethoxymethyl)-aniline

2-methyl-6-(thiomethoxymethyl)-aniline

Conditions
ConditionsYield
With sodium methylate In methanol; dichloromethane; water75%
With sodium methylate In methanol; dichloromethane; water75%

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