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inquiryProduct informations Product Name 4-[[(4-Fluorophenyl)imino Methyl-phenol CAS No. 3382-63-6
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inquiry4-[[(4-Fluorophenyl)imino]methyl]-phenol CAS No.:3382-63-6 Name: 4-[[(4-Fluorophenyl)imino]methyl]-phenol Molecular Structure: Molecular Formula: C13H10FNO Molecular Weight: 215.23 CAS Re
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inquiryGood quality Good price Promptly delivery Appearance:white powder Storage:dry dondition Application:intermediate Port:shanghai
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inquiryCHENGDU YANXI is a comprehensive manufacturer and an international distribution of products throughout the world. Specialized in Scrap metal, Chemical raw materials, Paper products and color industry. We aim to become leading position in global dis
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inquiryTIANFUCHEM--3382-63-6-- 4-[[(4-Fluorophenyl)imino]methyl]-phenol in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stab
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inquiryLIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryProduct Name 4-[[(4-Fluorophenyl)imino]methyl]-phenol CAS 3382-63-6 MF C13H10FNO MW
Cas:3382-63-6
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White Crystalline Powder Storage:Store in sealed conta
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
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inquiry4-[[(4-Fluorophenyl)imino]methyl]-phenol CAS: 3382-63-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high
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Min.Order:1 Gram
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inquiry4-[[(4-Fluorophenyl)imino]methyl]-phenol CAS: 3382-63-6 Specification Product Name 4-[[(4-Fluorophenyl)imino Methyl-phenol CAS No. 3382-63-6 Appearance White or off
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiryTriumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis: Trading(Raw Mater
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryWe are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to provide excellence in researching, manufacturing and drug discovery process. Our research team of scientists co
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Min.Order:100 Gram
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inquiry3382-63-6 4-[[(4-Fluorophenyl)imino]methyl]-phenol Appearance:white powder Storage:room temperature Package:according to customers' requirements Application:Pharma intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FO
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inquiryWe are concentrating on APIs and pharmaceutical intermediates. It is made obtainable from us at the most reasonable rate. Our Service: 1. Rich experience: Our company is a professional production leading factory in China in pharmaceutical are
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inquiryChemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiry4-hydroxy-benzaldehyde
4-fluoroaniline
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
Conditions | Yield |
---|---|
In water at 20 - 85℃; for 5.5h; Large scale; | 97.5% |
In methanol at 20 - 30℃; Large scale; | 90% |
In isopropyl alcohol at 50℃; for 1h; | 88% |
ezetemibe
A
(-)-6-(4-fluorophenyl)tetrahydro-2H-pyran-2-one
B
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
Conditions | Yield |
---|---|
In water; acetonitrile UV-irradiation; |
p-azidofluorobenzene
trans-4-Hydroxystilbene
A
N-benzylidene-4-fluoroaniline
B
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
Conditions | Yield |
---|---|
With iron(II) chloride In acetonitrile at 100℃; Sealed tube; Inert atmosphere; |
4-fluoroaniline
A
N-benzylidene-4-fluoroaniline
B
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 - 5 °C / Inert atmosphere 1.2: 10 h / 20 °C / Inert atmosphere 2.1: iron(II) chloride / acetonitrile / 100 °C / Sealed tube; Inert atmosphere View Scheme |
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium acetate; palladium diacetate / 12 h / 20 °C / Inert atmosphere 2: iron(II) chloride / acetonitrile / 100 °C / Sealed tube; Inert atmosphere View Scheme |
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
tert-butyldimethylsilyl chloride
N-(4-((tert-butyldimethylsilyl)oxy)benzylidene)-4-fluoroaniline
Conditions | Yield |
---|---|
Stage #1: N-(4-hydroxybenzylidene)-4-fluorobenzenamine With dmap; triethylamine In dichloromethane at 0℃; for 0.166667h; Inert atmosphere; Stage #2: tert-butyldimethylsilyl chloride In dichloromethane at 0 - 20℃; Inert atmosphere; | 99% |
With 1H-imidazole In N,N-dimethyl-formamide at 60℃; for 4h; | 97.5% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 5h; | 98% |
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
trityl chloride
N-(4-trityloxybenzylidene)-4-fluoroaniline
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 10 - 20℃; for 1.08333h; | 97.8% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 10 - 20℃; | |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 10 - 20℃; |
chloro-trimethyl-silane
3-[5-(4-fluorophenyl)-1,5-dioxopentyl]-4-phenyl-2-oxazolidinone
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
3-{2-[3-(fluorophenyl)-3-(trimethyl silyloxy)-propyl]-3-(4-fluoro phenyl amino)-3-(4-trimethyl silyloxy phenyl)-1-oxo-propyl}-4-(S)-phenyl oxazolidin-2-one
Conditions | Yield |
---|---|
Stage #1: 3-[5-(4-fluorophenyl)-1,5-dioxopentyl]-4-phenyl-2-oxazolidinone With dimethylsulfide borane complex; ascorbic acid; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole In dichloromethane at -10 - 8℃; for 7.25h; Inert atmosphere; Large scale; Stage #2: With dihydrogen peroxide In methanol; dichloromethane at -5 - 20℃; for 0.5h; Inert atmosphere; Large scale; Stage #3: chloro-trimethyl-silane; N-(4-hydroxybenzylidene)-4-fluorobenzenamine Large scale; Further stages; | 96.3% |
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
2,2,2-Trichloroethyl chloroformate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 5℃; for 6h; | 95% |
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
pivaloyl chloride
2,2-dimethylpropionic acid 4-[(4-fluorophenylimino)methyl]phenyl ester
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 93% |
chloro-trimethyl-silane
methyl 5S-5-(4-fluorophenyl)-5-hydroxyvalerate
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
Conditions | Yield |
---|---|
Stage #1: chloro-trimethyl-silane; methyl 5S-5-(4-fluorophenyl)-5-hydroxyvalerate; N-(4-hydroxybenzylidene)-4-fluorobenzenamine With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at -10 - 0℃; Inert atmosphere; Stage #2: With (R,R)-(+)-N-benzyl-3,4-bis(diphenylphosphino)pyrrolidine; lithium diisopropyl amide In tetrahydrofuran; n-heptane; ethylbenzene at -10 - 0℃; Inert atmosphere; | 79% |
methyl 5S-5-(4-fluorophenyl)-5-hydroxyvalerate
triethylsilyl chloride
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
Conditions | Yield |
---|---|
Stage #1: methyl 5S-5-(4-fluorophenyl)-5-hydroxyvalerate; triethylsilyl chloride; N-(4-hydroxybenzylidene)-4-fluorobenzenamine With tributyl-amine In 2-methyltetrahydrofuran at -10 - 0℃; Inert atmosphere; Stage #2: With (R,R)-(+)-N-benzyl-3,4-bis(diphenylphosphino)pyrrolidine; lithium diisopropyl amide In tetrahydrofuran; n-heptane; ethylbenzene at -10 - 0℃; Inert atmosphere; | 78.3% |
methyl 5S-5-(4-fluorophenyl)-5-hydroxyvalerate
chlorotripropylsilane
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
Conditions | Yield |
---|---|
Stage #1: methyl 5S-5-(4-fluorophenyl)-5-hydroxyvalerate; chlorotripropylsilane; N-(4-hydroxybenzylidene)-4-fluorobenzenamine With triethylamine In 2-methyltetrahydrofuran at -20 - -10℃; Inert atmosphere; Stage #2: With (R,R)-(+)-N-benzyl-3,4-bis(diphenylphosphino)pyrrolidine; lithium diisopropyl amide In tetrahydrofuran; n-heptane; ethylbenzene at -20 - -10℃; Inert atmosphere; | 76.7% |
Conditions | Yield |
---|---|
Stage #1: chloro-trimethyl-silane; N-(4-hydroxybenzylidene)-4-fluorobenzenamine; C20H19ClFNO4 With N-ethyl-N,N-diisopropylamine for 1h; Stage #2: With titanium tetrachloride at -30 - -25℃; for 3h; | 71% |
chloro-trimethyl-silane
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
(4S)-3-[(5S)-5-(4-fluorophenyl)-5-hydroxypentanoyl]-4-phenyl-1,3-oxazolidine-2-one
(4S)-3-[(2R,5S)-5-(4-fluorophenyl)-2-[(S)-[(4-fluorophenyl)amino]({4-[(trimethylsilyl)oxy]phenyl})methyl]-5-[(trimethylsilyl)oxy]pentanoyl]-4-phenyl-1,3-oxazolidin-2-one
Conditions | Yield |
---|---|
Stage #1: chloro-trimethyl-silane; N-(4-hydroxybenzylidene)-4-fluorobenzenamine; (4S)-3-[(5S)-5-(4-fluorophenyl)-5-hydroxypentanoyl]-4-phenyl-1,3-oxazolidine-2-one With N-ethyl-N,N-diisopropylamine In dichloromethane at -10 - 0℃; Inert atmosphere; Stage #2: With titanium tetrachloride In dichloromethane at -30 - -25℃; Inert atmosphere; | 66.6% |
With triethylamine In dichloromethane at -20℃; Reagent/catalyst; Solvent; |
chloro-trimethyl-silane
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
(4S)-3-[(5S)-5-(4-fluorophenyl)-5-hydroxypentanoyl]-4-phenyl-1,3-oxazolidine-2-one
Conditions | Yield |
---|---|
Stage #1: N-(4-hydroxybenzylidene)-4-fluorobenzenamine; (4S)-3-[(5S)-5-(4-fluorophenyl)-5-hydroxypentanoyl]-4-phenyl-1,3-oxazolidine-2-one With N-ethyl-N,N-diisopropylamine In dichloromethane at -10 - -5℃; Stage #2: chloro-trimethyl-silane In dichloromethane at -5℃; for 1.5h; Stage #3: With N,O-bis-(trimethylsilyl)-acetamide; titanium tetrachloride more than 3 stages; | 65% |
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
chloromethyl methyl ether
(4S)-3-[(5S)-5-(4-fluorophenyl)-5-hydroxypentanoyl]-4-phenyl-1,3-oxazolidine-2-one
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at -20 - -10℃; for 1h; Temperature; Reagent/catalyst; | 64.5% |
chloro-trimethyl-silane
N,O-bis-(trimethylsilyl)-acetamide
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
(4S)-3-[(5S)-5-(4-fluorophenyl)-5-hydroxypentanoyl]-4-phenyl-1,3-oxazolidine-2-one
(4S)-3-[(2R,5S)-5-(4-fluorophenyl)-2-[(S)-[(4-fluorophenyl)amino]({4-[(trimethylsilyl)oxy]phenyl})methyl]-5-[(trimethylsilyl)oxy]pentanoyl]-4-phenyl-1,3-oxazolidin-2-one
Conditions | Yield |
---|---|
Stage #1: chloro-trimethyl-silane; N-(4-hydroxybenzylidene)-4-fluorobenzenamine; (4S)-3-[(5S)-5-(4-fluorophenyl)-5-hydroxypentanoyl]-4-phenyl-1,3-oxazolidine-2-one With N-ethyl-N,N-diisopropylamine In dichloromethane at -10 - -5℃; for 1h; Stage #2: With titanium tetrachloride In dichloromethane at -30℃; for 20h; Stage #3: N,O-bis-(trimethylsilyl)-acetamide | 60% |
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 20 - 30℃; Large scale; | 59% |
(S)-3-(5-(4-fluorophenyl)-5,5-dimethoxypentanoyl)-4-phenyloxazolidin-2-one
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
benzyl chloroformate
C41H34F2N2O7
Conditions | Yield |
---|---|
Stage #1: N-(4-hydroxybenzylidene)-4-fluorobenzenamine; benzyl chloroformate With N-ethyl-N,N-diisopropylamine In dichloromethane; toluene at 0 - 20℃; for 1.66667h; Stage #2: (S)-3-(5-(4-fluorophenyl)-5,5-dimethoxypentanoyl)-4-phenyloxazolidin-2-one With titanium(IV) trichloride isopropoxide In dichloromethane; toluene at -35 - -30℃; for 3.33333h; | 51.76% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran for 6h; | 45% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran for 6h; | 44% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran for 6h; | 41% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran for 6h; | 41% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran for 6h; | 38% |
Conditions | Yield |
---|---|
Stage #1: N-(4-hydroxybenzylidene)-4-fluorobenzenamine With potassium carbonate In acetone for 0.166667h; Inert atmosphere; Stage #2: N-(2-chloroethyl)-pyrrolidine In acetone Inert atmosphere; Reflux; | 37% |
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
Conditions | Yield |
---|---|
Stage #1: 3-[(5S)-5-(4-fluorophenyl)-5-hydroxy-1-oxopentyl]-4-phenyl-2-oxazolidinone; N-(4-hydroxybenzylidene)-4-fluorobenzenamine With chloro-trimethyl-silane; N-ethyl-N,N-diisopropylamine; titanium tetrachloride In n-heptane; toluene at -35 - -10℃; for 4.75h; Stage #2: With bistrimethylsilylacetamide In n-heptane; toluene for 0.5h; Heating / reflux; |
(S)-3-{4-[2-(4-fluorophenyl)dioxolan-2-yl]butanoyl}-4-phenyl-oxazolidin-2-one
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
(S)-3-{(R)-2-[(S)-(4-fluorophenylamino)-(4-hydroxyphenyl)methyl]-4-[2-(4-fluorophenyl)-[1,3]-dioxolan-2-yl]butyryl}-4-phenyloxazolidin-2-one
Conditions | Yield |
---|---|
Stage #1: (S)-3-{4-[2-(4-fluorophenyl)dioxolan-2-yl]butanoyl}-4-phenyl-oxazolidin-2-one; N-(4-hydroxybenzylidene)-4-fluorobenzenamine With chloro-trimethyl-silane; N-ethyl-N,N-diisopropylamine In dichloromethane at -10℃; for 1.5h; Stage #2: With titanium tetrachloride In dichloromethane at -15℃; |
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
benzyl chloroformate
benzyl-[4-(4-fluorophenyliminomethyl)phenyl]-carbonate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane; toluene at 5 - 10℃; | |
With N-ethyl-N,N-diisopropylamine In dichloromethane; toluene at 5 - 10℃; for 1.08333h; |
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
(4S)-3-[(5S)-5-(4-fluorophenyl)-5-hydroxypentanoyl]-4-phenyl-1,3-oxazolidine-2-one
Conditions | Yield |
---|---|
With titanium tetrachloride; N-ethyl-N,N-diisopropylamine In dichloromethane |
N-(4-hydroxybenzylidene)-4-fluorobenzenamine
Conditions | Yield |
---|---|
Stage #1: (S)-3-(5-(4-fluorophenyl)-5-(hydroxyimino)pentanoyl)-4-phenyloxazolidin-2-one; N-(4-hydroxybenzylidene)-4-fluorobenzenamine With chloro-trimethyl-silane; N-ethyl-N,N-diisopropylamine In dichloromethane at -10 - -5℃; Stage #2: titanium tetrachloride In dichloromethane at -30 - -25℃; for 3 - 6h; |
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