Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryProduct Name: 2-(2-Bromoethyl)-1,3-dioxane Synonyms: 1,3-Dioxane, 2-(2-bromoethyl)-;2-(2-bromoethyl)-3-dioxane;3-BROMOPROPIONALDEHYDE TRIMETHYLENE ACETAL;2-(2-BROMOETHYL)-1,3-DIOXANE;LABOTEST-BB LT00233134;2-Bromopropanal 1,3-propanedi
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiry2-(2-Bromoethyl)-1,3-dioxane CAS:33884-43-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality orga
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
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inquiryProduct Name: 2-(2-Bromoethyl)-1,3-dioxane Synonyms: 1,3-Dioxane, 2-(2-bromoethyl)-;2-(2-bromoethyl)-3-dioxane;3-BROMOPROPIONALDEHYDE TRIMETHYLENE ACETAL;2-(2-BROMOETHYL)-1,3-DIOXANE;LABOTEST-BB LT00233134;2-Bromopropanal 1,3-propanediol acetal
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inquiryWe Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiryShanghai Massive Chemical Technology Co., Ltd. is engaged in development, production and marketing Specialty Chemicals to satisfy the changing needs of the chemical industry. We specialize in manufacturing high quality of Advanced Intermediates, Sp
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Hangzhou Dingyan Chem is a leading manufacturer and supplier of chemicals in China.We develop,produce and distribute high quality pharmaceuticals, intermediates, special chemicals and other fine chemicals.Appearance:A white or almost white crystallin
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inquiryhigh purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
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Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
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inquiryConditions | Yield |
---|---|
With hydrogen bromide In 1,4-dioxane at 5 - 20℃; for 0.5h; | 83% |
With hydrogen bromide for 1h; Ambient temperature; | 74% |
With hydrogen bromide at 5 - 10℃; | 50% |
2-(2-iodethyl)-[1,3]dioxane
ethylene dibromide
2-(2-Bromoethyl)-1,3-dioxane
Conditions | Yield |
---|---|
With tert.-butyl lithium 1) diethylether, -78 deg C, 5 min, r.t., 1h ; 2) -78 deg C; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In dichloromethane Ambient temperature; Yield given; | |
With toluene-4-sulfonic acid In dichloromethane at 20℃; for 8h; Inert atmosphere; | 252 g |
2-(2-Bromoethyl)-1,3-dioxane
bis(phenylsulfonyl)methane
5-(3,3-Bis-benzenesulfonyl-propyl)-[1,3]dioxane
Conditions | Yield |
---|---|
tetrabutylammomium bromide In sodium hydroxide at 25 - 30℃; for 3h; | 100% |
2-(2-Bromoethyl)-1,3-dioxane
(R,E)-2-methyl-N-(2-methylpropylidene)propane-2-sulfinamide
Conditions | Yield |
---|---|
Stage #1: 2-(2-Bromoethyl)-1,3-dioxane With iodine; magnesium In tetrahydrofuran at 20℃; for 1h; Stage #2: (R,E)-2-methyl-N-(2-methylpropylidene)propane-2-sulfinamide In tetrahydrofuran at -48℃; for 12h; Grignard addition; | 100% |
2-(2-Bromoethyl)-1,3-dioxane
Conditions | Yield |
---|---|
Stage #1: 2-(2-Bromoethyl)-1,3-dioxane With magnesium In tetrahydrofuran at 20 - 50℃; for 1h; Inert atmosphere; Stage #2: (R)-N-[(1Z)-[5-fluoro-2-(methylsulfanyl)phenyl]methylidene]-2-methylpropane-2-sulfinamide In tetrahydrofuran at -50 - 20℃; for 1h; Inert atmosphere; | 100% |
Stage #1: 2-(2-Bromoethyl)-1,3-dioxane With magnesium In tetrahydrofuran at 20 - 50℃; for 1h; Inert atmosphere; Stage #2: (R)-N-[(1Z)-[5-fluoro-2-(methylsulfanyl)phenyl]methylidene]-2-methylpropane-2-sulfinamide In tetrahydrofuran at -50 - 20℃; | 100% |
Stage #1: 2-(2-Bromoethyl)-1,3-dioxane With magnesium In tetrahydrofuran at 20 - 50℃; for 1h; Inert atmosphere; Stage #2: (R)-N-[(1Z)-[5-fluoro-2-(methylsulfanyl)phenyl]methylidene]-2-methylpropane-2-sulfinamide In tetrahydrofuran at -50 - 20℃; for 1h; Inert atmosphere; | 100% |
2-(2-Bromoethyl)-1,3-dioxane
butyl magnesium bromide
2-hexyl-1,3-dioxolane
Conditions | Yield |
---|---|
With [((Me)NN2)NiCl] In tetrahydrofuran; ISOPROPYLAMIDE at -35 - 20℃; Inert atmosphere; | 99% |
With buta-1,3-diene; nickel dichloride In tetrahydrofuran at -78 - 0℃; for 1h; Inert atmosphere; | 86% |
With 1-Phenylprop-1-yne; copper In tetrahydrofuran at 25℃; for 3h; Schlenk technique; Glovebox; | 74% |
With buta-1,3-diene; copper dichloride In tetrahydrofuran at 25℃; for 24h; Schlenk technique; Inert atmosphere; | 73 %Chromat. |
2-(2-Bromoethyl)-1,3-dioxane
allylmagnesium bromide
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; Inert atmosphere; Reflux; | 99% |
2-(2-Bromoethyl)-1,3-dioxane
Conditions | Yield |
---|---|
Stage #1: 2-(2-Bromoethyl)-1,3-dioxane With iodine; magnesium In tetrahydrofuran at 20 - 50℃; for 1.5h; Inert atmosphere; Stage #2: (R)-N-[(1Z)-[3-fluoro-5-(methylsulfanyl)phenyl]methylidene]-2-methylpropane-2-sulfinamide In tetrahydrofuran at -70 - 20℃; for 2h; | 99% |
Conditions | Yield |
---|---|
With magnesium | 98% |
2-(2-Bromoethyl)-1,3-dioxane
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
Stage #1: 2-(2-Bromoethyl)-1,3-dioxane; meta-hydroxybenzaldehyde With potassium carbonate In acetonitrile at 80℃; for 18h; Stage #2: With sodium tetrahydroborate In methanol; dichloromethane at 0 - 20℃; for 2.25h; | 98% |
6-bromo-3,4-dihydroisoquinolin-1(2H)-one
2-(2-Bromoethyl)-1,3-dioxane
2-(2-(1,3-dioxan-2-yl)ethyl)-6-bromo-3,4-dihydroisoquinolin-1(2H)-one
Conditions | Yield |
---|---|
Stage #1: 6-bromo-3,4-dihydroisoquinolin-1(2H)-one With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.583333h; Stage #2: 2-(2-Bromoethyl)-1,3-dioxane In N,N-dimethyl-formamide for 16h; | 97% |
Stage #1: 6-bromo-3,4-dihydroisoquinolin-1(2H)-one With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 0.583333h; Inert atmosphere; Stage #2: 2-(2-Bromoethyl)-1,3-dioxane In N,N-dimethyl-formamide; mineral oil for 16h; Inert atmosphere; | 97% |
2-(2-Bromoethyl)-1,3-dioxane
Conditions | Yield |
---|---|
With magnesium In tetrahydrofuran; dichloromethane at -40 - 65℃; for 1h; Concentration; Reagent/catalyst; Temperature; Inert atmosphere; | 96.32% |
2-(2-Bromoethyl)-1,3-dioxane
1-indene
2-[2-(1H-inden-1-yl)ethyl]-1,3-dioxane
Conditions | Yield |
---|---|
With n-butyllithium In diethyl ether; hexane at -78 - 20℃; for 8.25h; Inert atmosphere; Schlenk technique; | 96% |
Stage #1: 1-indene With n-butyllithium In diethyl ether; hexane at 20℃; for 4h; Stage #2: 2-(2-Bromoethyl)-1,3-dioxane In diethyl ether; hexane at 20℃; for 16h; Further stages.; | 82% |
2-(2-Bromoethyl)-1,3-dioxane
phenylmagnesium chloride
2-(2-phenylethyl)-1,3-dioxane
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; [((Me)NN2)NiCl] In tetrahydrofuran at 20℃; for 2h; Kumada-Corriu-Tamao coupling reaction; Inert atmosphere; | 96% |
With 1-Phenylprop-1-yne; copper In tetrahydrofuran at 80℃; for 12h; Schlenk technique; Glovebox; | 75% |
5-Norbornene-2-carboxaldehyde
2-(2-Bromoethyl)-1,3-dioxane
3-(1,3-dioxan-2-yl)-1-(5-norbornen-2-yl)-1-propanol
Conditions | Yield |
---|---|
With ammonium chloride In tetrahydrofuran | 95% |
2-(2-Bromoethyl)-1,3-dioxane
(2S,4aR,4bS,6aS,7aS,8aS,8bS,8cR,8dR,9aR,9bR)-2,9b-dihydroxy-4a,6a-dimethyloctadecahydro-7H-cyclopropa[4,5]cyclopenta[1,2-a]cyclopropa[l]phenanthren-7-one
17α-(2-[1,3]dioxan-2-ylethyl)-6β,7β,15β,16β-dimethylen-5β-androstane-3β,5,17β-triol
Conditions | Yield |
---|---|
Stage #1: 2-(2-Bromoethyl)-1,3-dioxane With magnesium; iodine In tetrahydrofuran at 55 - 60℃; for 1h; Stage #2: (2S,4aR,4bS,6aS,7aS,8aS,8bS,8cR,8dR,9aR,9bR)-2,9b-dihydroxy-4a,6a-dimethyloctadecahydro-7H-cyclopropa[4,5]cyclopenta[1,2-a]cyclopropa[l]phenanthren-7-one In tetrahydrofuran for 3.5h; Product distribution / selectivity; | 95% |
Stage #1: (2S,4aR,4bS,6aS,7aS,8aS,8bS,8cR,8dR,9aR,9bR)-2,9b-dihydroxy-4a,6a-dimethyloctadecahydro-7H-cyclopropa[4,5]cyclopenta[1,2-a]cyclopropa[l]phenanthren-7-one With lithium In tetrahydrofuran at -20℃; for 0.333333 - 0.5h; Stage #2: 2-(2-Bromoethyl)-1,3-dioxane In tetrahydrofuran at -20 - 0℃; for 2h; Product distribution / selectivity; | 74% |
2-(2-Bromoethyl)-1,3-dioxane
1,5-bis[(4R)-4-phenyl-3-(2,4,6-trimethoxybenzyl)-1,3-oxazolidin-2-yl]pentane
(2R,2'R)-2,2'-[1,9-bis(1,3-dioxan-2-yl)nonane-3(S),7(S)-diamino]bis(2-phenylethanol)
Conditions | Yield |
---|---|
Stage #1: 2-(2-Bromoethyl)-1,3-dioxane With magnesium In tetrahydrofuran Stage #2: 1,5-bis[(4R)-4-phenyl-3-(2,4,6-trimethoxybenzyl)-1,3-oxazolidin-2-yl]pentane In tetrahydrofuran at 60℃; for 48h; Stage #3: With water; ammonium chloride In tetrahydrofuran at 20℃; diastereoselective reaction; | 95% |
2-(2-Bromoethyl)-1,3-dioxane
2-(2-iodethyl)-[1,3]dioxane
Conditions | Yield |
---|---|
With sodium iodide In acetone Reflux; | 95% |
With sodium iodide In acetone | |
With sodium iodide In acetone |
2-(2-Bromoethyl)-1,3-dioxane
benzyl {4-[methoxy(methyl)amino]-4-oxobutyl}methylcarbamate
benzyl [6-(1,3-dioxan-2-yl)-4-oxohexyl]methylcarbamate
Conditions | Yield |
---|---|
Stage #1: 2-(2-Bromoethyl)-1,3-dioxane With iodine; magnesium In tetrahydrofuran at 65℃; Stage #2: benzyl {4-[methoxy(methyl)amino]-4-oxobutyl}methylcarbamate In tetrahydrofuran at 4 - 65℃; for 2h; | 95% |
Conditions | Yield |
---|---|
Stage #1: 2-(2-Bromoethyl)-1,3-dioxane With magnesium; iodine In tetrahydrofuran at 20℃; for 2h; Inert atmosphere; Stage #2: C27H26F3NO4S In tetrahydrofuran at -78℃; for 1.66667h; Stage #3: With ammonium chloride In tetrahydrofuran; water at -48℃; | 95% |
2-(2-Bromoethyl)-1,3-dioxane
Conditions | Yield |
---|---|
Stage #1: 2-(2-Bromoethyl)-1,3-dioxane With iodine; magnesium In tetrahydrofuran Inert atmosphere; Stage #2: phenyl 6-(benzyloxy)-2-methyl-4-[(1E)-{[(S)-2-methylpropane-2-sulfinyl]imino}methyl]-3-(trifluoromethyl)benzoate In tetrahydrofuran at -78℃; for 1.66667h; diastereoselective reaction; | 95% |
2-(2-Bromoethyl)-1,3-dioxane
zinc
Conditions | Yield |
---|---|
In tetrahydrofuran at 50℃; Inert atmosphere; Schlenk technique; | 95% |
2-(2-Bromoethyl)-1,3-dioxane
3,5,5-trimethylcyclopenten-2-one
4-<2-(1,3-Dioxan-2-yl)ethyl>-2,2,4-trimethylcyclopentanone
Conditions | Yield |
---|---|
Stage #1: 2-(2-Bromoethyl)-1,3-dioxane With iodine; magnesium; ethylene dibromide In tetrahydrofuran for 0.666667h; Heating; Stage #2: With copper(I) bromide dimethylsulfide complex In tetrahydrofuran at 5℃; for 0.166667h; Stage #3: 3,5,5-trimethylcyclopenten-2-one In tetrahydrofuran at 0 - 20℃; for 5.66667h; | 93% |
2-(2-Bromoethyl)-1,3-dioxane
Conditions | Yield |
---|---|
Stage #1: 2-(2-Bromoethyl)-1,3-dioxane With magnesium In tetrahydrofuran at -15 - 50℃; for 5h; Inert atmosphere; Stage #2: N-(3-pyridinemethylidene)-2-methylpropane-2-sulfinamide In tetrahydrofuran at -15 - 25℃; for 6h; | 92.7% |
2-(2-Bromoethyl)-1,3-dioxane
Conditions | Yield |
---|---|
With magnesium In tetrahydrofuran at 60℃; for 8h; | 92% |
2-(2-Bromoethyl)-1,3-dioxane
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 80℃; for 13h; | 92% |
2-(2-Bromoethyl)-1,3-dioxane
Conditions | Yield |
---|---|
With dichloro bis(acetonitrile) palladium(II); dipotassium hydrogenphosphate; norbornene In N,N-dimethyl acetamide at 90℃; for 22h; regioselective reaction; | 91% |
With dichloro bis(acetonitrile) palladium(II); dipotassium hydrogenphosphate; norbornene In N,N-dimethyl acetamide at 90℃; for 22h; regioselective reaction; | 91% |
Conditions | Yield |
---|---|
Stage #1: 2-(2-Bromoethyl)-1,3-dioxane With magnesium; ethylene dibromide In tetrahydrofuran at 23℃; for 1.5h; Inert atmosphere; Schlenk technique; Stage #2: With copper(l) cyanide; lithium chloride In tetrahydrofuran at -45 - 23℃; for 0.666667h; Inert atmosphere; Schlenk technique; Stage #3: (+)-(R)-6-methylcyclohex-2-en-1-one Further stages; | 91% |
Stage #1: 2-(2-Bromoethyl)-1,3-dioxane With magnesium; ethylene dibromide In tetrahydrofuran for 1.5h; Inert atmosphere; Stage #2: With copper(l) cyanide; lithium chloride In tetrahydrofuran at -45℃; for 0.666667h; Inert atmosphere; Stage #3: (+)-(R)-6-methylcyclohex-2-en-1-one Further stages; | 91% |
1-butylbenzimidazole
2-(2-Bromoethyl)-1,3-dioxane
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20 - 80℃; for 5h; | 91% |
2-(2-Bromoethyl)-1,3-dioxane
Br(1-)*C23H29N2O5(1+)
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 25 - 80℃; for 10h; Inert atmosphere; | 90% |
2-(2-Bromoethyl)-1,3-dioxane
bis(pinacol)diborane
2-(2-(1,3-dioxan-2-yl)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Conditions | Yield |
---|---|
With lithium tert-butoxide In N,N-dimethyl-formamide at 25℃; for 16h; Inert atmosphere; Schlenk technique; | 90% |
With potassium tert-butylate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; copper(l) chloride In tetrahydrofuran at 20℃; for 5h; Inert atmosphere; | 86% |
Stage #1: bis(pinacol)diborane With potassium tert-butylate; [1,3-bis(2,4,6-trimethylphenyl)imidazol]-2-ylidene; zinc(II) chloride In tert-butyl methyl ether for 0.5h; Inert atmosphere; Schlenk technique; Glovebox; Stage #2: 2-(2-Bromoethyl)-1,3-dioxane In tert-butyl methyl ether at 20℃; for 2h; Inert atmosphere; Schlenk technique; Glovebox; | 84% |
2-(2-Bromoethyl)-1,3-dioxane
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 5h; Inert atmosphere; Schlenk technique; | 90% |
In N,N-dimethyl-formamide at 20 - 80℃; for 5h; |
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